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31.
Bruno Jasse  Jack L. Koenig 《Polymer》1981,22(8):1040-1044
Fourier transform infra-red measurements have been made of the orientation in isotactic polystyrene as a function of draw ratio. Based on these results, new band assignments are made and orientation functions calculated.  相似文献   
32.
Although some patterns of physical behavior are common in the glass transition and in the properties of supercooled liquids and glasses (characteristic viscoelasticity, temperature dependence of viscosity and relaxation times, property evolution through “physical aging”, difficulties in performing equilibrium measurements or simulations, etc.), it is difficult to arrive at a definition of the glass transition which distinguishes it from other phenomena exhibiting similar features. The present paper addresses this problem by defining a dynamical measure of order involving the average “shape” of particle trajectories in supercooled liquids. This dynamic order parameter should provide a measure of “closeness” to the glass transition and some indirect insights into the physical nature of supercooled liquids and glasses. Arguments are given that the proposed dynamic measure of order [“generalized capacity”, C(T)] is related to the temperature-dependent “effective hydrodynamic radius” RH(T) measured in supercooled liquids and model numerical calculations are given to support this view. Some consequences of the intermittent particle motion at low temperatures for stress relaxation are also discussed.  相似文献   
33.
Abstract. A vector time series model of the form A(L)y(t) + B(L)x(t) =ε(t) is known as a vector autoregressive model with exogenous variables (VARX model) and involves a regressand vector y(t) and a regressor vector x(t). This paper provides a method for the recursive fitting of subset VARX models. It suggests the use of ascending recursions in conjunction with an order selection criterion to choose an 'optimum' subset VARX model.  相似文献   
34.
The differences between ITS-90 and IPTS-68 above 1235 K are described. It is shown that none of the following CIE definitions or recommendations require revision because of the introduction of the ITS-90: International Lighting Vocabulary definitions; CIE Standard Illuminants A, D65, other illuminants; and sources for realizing CIE Illuminants. The effect of the ITS-90 on previously calibrated sources for realizing CIE illuminants is negligibly small.2  相似文献   
35.
To make media resources a prime citizen on the Web, we have to go beyond simply replicating digital media files. The Web is based on hyperlinks between Web resources, and that includes hyperlinking out of resources (e.g., from a word or an image within a Web page) as well as hyperlinking into resources (e.g., fragment URIs into Web pages). To turn video and audio into hypervideo and hyperaudio, we need to enable hyperlinking into and out of them. The W3C Media Fragments Working Group is taking on the challenge to further embrace W3C??s mission to lead the World Wide Web to its full potential by developing a Media Fragment protocol and guidelines that ensure the long-term growth of the Web. The major contribution of this paper is the introduction of Media Fragments as a media-format independent, standard means of addressing media resources using URIs. Moreover, we explain how the HTTP protocol can be used and extended to serve Media Fragments and what the impact is for current Web-enabled media formats.  相似文献   
36.
A popular conception of the evolution of remote manipulation is a progression from teleoperation to telerobotics and then to robotics. This is logical because in going from teleoperation to robotics there would appear to be a continuous decrease in manned workload, an increase in system complexity, and an increase in the amount of intelligence in the automated system. During the past 10 years NASA Langley Research Center (LaRC) has been involved in all three areas. The decision on which system is most suitable for a task depends not only on the task, but on the allocation of responsibility for intelligence or high level control. The operator may be responsible for all intelligence and control functions, they may be shared between the operator and the automated system, or they may be performed by an autonomous system. This paper discusses some of the experiences in each area in applications related to possible space tasks and some of the lessons learned.  相似文献   
37.
38.
Failure mechanisms of an alumina, tested at 1200°C under static and various cyclic loading conditions, were examined. Slow crack growth of a single crack is the dominant mechanism for the failure in specimens under cyclic loading with a short duration of maximum stress at all applied stress levels, as well as at high applied loads for static loading and cyclic loading with a longer hold time at maximum stress. At low stress levels, failure of static loading and cyclic loading with a longer hold time at maximum stress might occur by formation and/or growth of multiple macrocracks. More importantly, for all the given loading conditions. The viscous glassy phase behind the crack tip could have a bridging effect on the crack surfaces. A simplified model for calculating effective stress intensity factor at the crack tip under static and various cyclic loading demonstrated a trend consistent with the stress–life data.  相似文献   
39.
The MAS-NMR spectra of adsorbed trimethylphosphine (TMP) were used to determine the concentration of Brønsted and Lewis acid sites on pure and chlorinated-Al2O3 samples. Chlorination with CHCl3,CCl4 or AlCl3 promoted the formation of Brønsted acid centers, which are characterized by the protonated adduct of TMP. This adduct has a31P chemical shift of ca. –3.8 ppm and a JP–H scalar coupling of 517 Hz. Additional resonances in the –44 to –54 ppm range are attributed to Lewis acid-base pairs. In some cases a partially resolved JP–Al coupling is observed, which confirms the assignment. Upon thermal treatment of a chlorinated sample at temperatures > 200°C, the concentration of Brønsted acid centers decreased; the concentration of one type of Lewis acid increased and another remained almost constant. In a parallel set of experiments the initial conversion ofn-hexane at 150°C and the yields of cracking and isomerization products were determined. Comparable functional relationships were observed between the loss of Brønsted acid sites and the decrease in yields of both cracking and isomerization products. These results suggest that Bransted acidity is responsible for the cracking and isomerization ofn-hexane over chlorided aluminas at 150°C.  相似文献   
40.
Abstract. Conventional methods to determine the forgetting factors in autoregressive (AR) models are mostly based on arbitrary or personal choices. In this paper, we present two procedures which can be used to select the forgetting factor in subset AR modelling. The first procedure uses the bootstrap to determine the value of a fixed forgetting factor. The second procedure starts from this base and applies the time-recursive maximum likelihood estimation to a variable forgetting factor. In one illustration using real exchange rates, we demonstrate the effect of the forgetting factor in subset AR modelling on ex ante forecasting of non-stationary time series. In a second illustration, these two procedures are applied to time-update forecasts for a stock market index. Subset AR models not including a forgetting factor act as a set of benchmarks for assessing ex ante forecasting performance, and consistently improved forecasting performance is demonstrated for these proposed procedures.  相似文献   
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