Synthesis of TiO<Subscript>2</Subscript> Hybrid Molecular Imprinted Polymer for Ethofumesate Linked by Silane Coupling Agent

TiO₂ hybrid molecular imprinted polymer (MIP) for ethofumesate using methacrylic acid (MAA) as the functional monomer and silane coupling agent 3-(trimethoxysilyl) propylmethacrylate (KH570) as organic–inorganic connective bridge was synthesized via photo-excitation method. Hydrogen bond was proved to act between MAA and ethofumesate for pre- and post-polymerization binding properties as testified by UV spectrometric method. KH570 modified TiO₂ nanoparticles were prepared via sonochemical reaction, which can accelerate hydrolysis, increase collision chance for the reactive system and improve the dispersion of the nanoparticles. Scanning electron microscope (SEM), transmission electron microscope (TEM), binding and the adsorption kinetics experiments as well as thermogravimetric analysis (TGA) were employed for characterization. The results indicated that the hybrid MIP revealed a larger surface area and more ordered imprinting cavities with improved thermal stability compared to organic-only MIP. Furthermore, faster adsorption kinetics and enhancive adsorption capacity were achieved, which made it promising in chemical sensor applications.     

Growth of highly orientated strontium barium niobate thin films on Si substrates through the sol–gel process using a K: SBN template layer

We report the growth of highly C-axis orientation of Sr _x Ba_1−x Nb₂O₆ (SBN) thin films on p-type (100) Si substrates by using a potassium-substituted SBN template layer with the sol–gel method. The crystallization of SBN thin films was found closely related to the potassium ion doping concentration and the postannealing temperature of the K-SBN template layer. Secondary ion mass spectrometry analysis showed that potassium elements were accumulated at the interface of the template layer and silicon substrate. SBN films postannealed at 750 °C with K-SBN template layer has a smaller full width at half maximum of X-ray rocking curve of 2.45° than that of 5.40° for the pure SBN films. By introducing a template layer, the surface morphologies of SBN films fabricated on silicon substrate were greatly improved.     

广州地铁二号线民用移动通信工程简介

简单介绍了广州地铁二号线民用移动通信工程概况，并就地铁民用移动通信系统引入地铁的主要技术难点进行了论述。     

Free-Edge and Ply Cracking Effect in Angle-Ply Laminated Composites Subjected to In-Plane Loads

This paper presents a semianalytical method for the prediction of interlaminar stresses and displacements near the free edges and ply cracks in general angle-ply laminates subjected to biaxial extensions and/or in plane shear deformation. The method is based on a state space representation of the three-dimensional equations of elasticity. Numerical solutions are obtained by using layer refinement in the through thickness direction and Fourier series expansion in the other directions. By this approach, an angle-ply laminate may be composed of an arbitrary number of monoclinic layers and each layer may have different material property and thickness. This method guarantees continuous fields of all interlaminar stresses across interfaces between material layers. Numerical results are compared with those obtained from other methods. It is found that the theory provides a satisfactory approximation to the stress singularities near the free edges and ply cracks. Numerical solutions for antisymmetric laminates under extension and general laminates under shearing are new in the literature and can be used as benchmarks for validating new models.     

链烷烃的表面张力与内压

对Ｄａｖｉｓ和Ｒｏｓｓｅｉｎｓｋｙ提出的关系检验表明，液体的表面张力σ与Ｐ１Ｖｍ１／３之比不仅取决于温度，还与液体的种类有关，据此，建立了一个能由链烷烃的分子结构准确预测其表面张力的方法。     

用Promax处理LD22-l“模糊带”地震资料

通过LD22-l构造地震资料目标处理,搞清了“模糊带”,引进交互处理系统是成功的.     

铁钴钒软磁合金损耗谱的分形结构

研究了铁钴钒软磁合金的铁芯损耗，发现铁芯损耗谱具有分形结构。讨论了带材厚度和磁感应强度对分形维数Ｄｆ的影响。     

室温下Ho∶YAG激光器输出3J的2．1μm激光

根据对２．１μｍ波长Ｃｒ，Ｔｍ，Ｈｏ∶ＹＡＧ激光器的实验研究，详细分析了冷却温度、放电脉冲半宽度和输出镜透过率等因素对激光器的输出的影响     

Testing of multi-output circuits by means of signature analyzer

Let a circuit havem outputs,m>1. There are two ways to test this circuit by means of a signature analyzer: use a single input analyzer for each output or use anm-input analyzer to test all outputs simultaneously. The main goal of this letter is to demonstrate that for fault output sequences with small multiplicity of errors and long length the second approach is more effective.