裂解汽油加氢装置二段反应器缺陷分析

对中国石油吉林石化公司300 kt/a乙烯装置汽油加氢二段反应器接管与筒体焊接接头的缺陷进行详细分析。阐明了缺陷的产生是由于在焊接过程中焊缝熔合区内形成马氏体、增碳层并伴有δ-铁素体的分解而使熔合区内及焊缝处的材质脆化。由于选用焊接材料的错误,产生较高的焊接残余应力致使焊缝开裂。分析了焊缝马氏体、增碳层及δ-铁素体分解的原因。     

Surface and interfacial FTIR spectroscopic studies of latexes. IX. The effect of homopolymer and copolymer structures on surfactant mobility in Sty/BA latices

The effects of homopolymer and copolymer compositions and structures in styrene/n-butyl acrylate (Sty/BA) latices on sodium dioctyl sulfosuccinate (SDOSS) surfactant mobility and its preferential concentration at the film–air (F–A) and film–substrate (F–S) interfaces were examined using attenuated total reflectance Fourier transform infrared (ATR FTIR) spectroscopy. It appears that the SDOSS concentration at the F–S interface is highest when the Sty/BA feed ratio is 50/50, and the excess of Sty results in migration of SDOSS surfactant to the F–A interface. This behavior is attributed to the increased glass transition temperature and diminished compatibility between surfactant molecules and copolymer latex. This study also shows that the primary factors that influence exudation to either F–A or F–S interfaces are surface tension of the substrate, glass transition temperature, water flux during coalescence, and compatibility between latex components. © 1995 John Wiley & Sons, Inc.     

乙烯二聚制高纯丁烯－1技术经济评价

本文对生产高纯度丁烯－１的Ａｌｐｈａｂｎｔｏｌ工艺进行了技术经济评价，认为该工艺条件简单、反应条件温和，而且投资少，所以很适合事在发展中国家应用。     

Formation of novel polymeric nanoparticles

We have found that not only block copolymers but also ionomers can self-assemble in a selective solvent to form surfactant-free nanoparticles. The self-assembly can be induced by chemical reaction, polymer-polymer complexation, and microphase inversion in addition to the temperature. A recently developed microwave method for the preparation of uniform surfactant-free polymeric nanoparticles is also reviewed. Our results have revealed that for a given dispersion, the particle surface area occupied per stabilizer (surfactant, polymer chains, and ionic groups) is close to a constant.     

多路输出反激式开关电源的改进与实现

针对传统开关电源存在的控制芯片供电方式耗能较大、反馈电路光耦有效输入电流范围窄两个问题,对传统电源电路进行了改进,设计并实现了一款性能优良的48V转+5V、±15V,输出功率25W的三路输出反激式开关电源。样机输出电压精度为0.2%(+5V)、0.53%(+15V)、0.6%(-15V),输出电压纹波为20mV(+5V)、50mV(+15V)、60mV(-15V),电压精度和纹波率均满足小于1%的要求;测试表明:该电源性能优良,具有效率高,稳压精度高,负载调整率高等优点,有很高的生产应用价值。     

高校智慧实验室综合管理平台建设研究

提出智慧实验室综合管理平台应能改善甚至解决高校实验室存在的人工管理、智慧化建设缓慢、开放共享不足等问题.分析智慧实验室管理平台的架构,描述了管理平台中实验教学管理与实验室开放管理应具备的主要功能与管理流程,为智慧实验室的管理与建设提供一定的参考.     

高性能MCU的FPGA原型验证系统研究与平台实现

本文研究并实现了一种基于Cortex-A7核的高性能MCU在FPGA原型阶段的验证平台。该设计研究可以针对高性能MCU芯片或其FPGA原型验证阶段的软硬件验证环境快速搭建,通过交互式、软硬件协同的方式对MCU芯片各个模块功能进行实时、可靠的功能验证。高效的FPGA原型验证可以提高MCU研发速度、缩短验证时间、提高验证效率、及时发现芯片设计的缺陷、缩短芯片研发周期。     

A low‐profile antenna with circularly polarized reconfigurable and omnidirectional radiation patterns

A low profile circularly polarized (CP) antenna with reconfigurable polarization is designed and presented, which can radiate omnidirectional patterns that can be switched between left‐hand circularly polarized (LHCP) and right‐hand circularly polarized (RHCP). A pair of arc‐shaped complementary dipoles is acted as reconfigurable elements by bridging four pin diodes at the dipole arced arms. A meander phase shift line is employed to connected the arc dipole arms and plate cavity to adjust the phase relationship of two sources. The proposed antenna exhibits the omnidirectional radiation pattern by combining six identical elements placed in a circular array configuration. 24 p‐i‐n diodes are exploited to six elements, by manipulating the dc bias voltage across the diodes, the polarization state of the antenna can be switched. The patterns of the antenna are similar to that of a dipole, but its size is only about Φ0.87 × 0.029λ₀ at 5.8 GHz. The overlapped bandwidth of measured 3‐dB axial ratio (AR) and 10‐dB return loss is 5.724‐5.87 and 5.738‐5.91 GHz for two polarization states, which are right on the target of ISM band. It can be well adapted to medical diagnosis systems.     

基于MEMS电容式加速度计的闭环读出电路设计

设计了面向圆片级封装的一种闭环加速度计读出电路.在基于电容式微加速度计结构的读出电路设计中考虑了寄生电容对整个系统的影响.用MATLAB SIMULINK对所设计的读出电路进行了建模仿真.在仿真过程中分析了噪声、圆片级封装与普通封装的寄生参数及实际工艺中流水结构的不对称性的影响并进行了比较.结果表明,所设计传感器及读出电路的非线性误差在量程±20 gn范围内小于0.5％;圆片级封装的稳定时间在2 ms,小于普通封装的稳定时间;基于圆片级封装的对称性梳齿结构的输出电压灵敏度为328 mV/gn.     

基于稳健设计的SGNS算法的超参数调优方法

通常给定超参数的若干取值选取性能最大的为最优组合(称为直接选优法),但是此方法的稳健性差。为此,提出了一种基于稳健设计的超参数调优方法(称为稳健调优法)。具体地,以SGNS算法中的超参数调优为例,在词语推断任务上实验并得出:经方差分析得到SGNS算法中的七个超参数中的五个对算法预测性能有显著影响,确定为主控因子,其余两个确定为噪声因子,且主控因子中有三个对性能估计的方差有显著影响,因此,调优中仅从期望最大来直接选优是不合理的;稳健调优法与直接选优法两者在预测性能上没有显著差异,但稳健调优法对噪声因子具有较好的稳健性。稳健调优法对一般的深度神经网络的调参有实际的借鉴意义。