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171.
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为优化2,6-二氟苯甲酸(DFBA)的合成工艺,以2,6-二氯苯腈(DCBN)和氟化钾为原料,N,N-二甲基酰胺(DMF)为溶剂,在聚醚类催化剂A的催化下氟代合成中间体2,6-二氟苯腈,然后中间体在碱性条件下水解制得(DFBA).试验结果表明,合成DFBN的最佳条件为:DCBN在DMF中的质量浓度为0.38g/mL,KF的量为DCBN的量的2.3~2.4倍,反应时间10 h,最高收率93.5%;合成DFBA时,以质量分数为20%的NaOH为介质,反应时间9 h,收率≥92%.收率93.5%,纯度99.7%.该工艺收率高、三废排放少,可节省成本,有望工业推广. 相似文献
173.
In this paper we introduce VideoGraph, a novel non-linear representation for scene structure of a video. Unlike classical linear sequential organization, VideoGraph concentrates the video content across the time line by structuring scenes and materializes with two-dimensional graph, which enables non-linear exploration on the scenes and their transitions. To construct VideoGraph, we adopt a sub-shot induced method to evaluate the spatio-temporal similarity between shot segments of video. Then, scene structure is derived by grouping similar shots and identifying the valid transitions between scenes. The final stage is to represent the scene structure using a graph with respect to scene transition topology. Our VideoGraph can provide a condensed representation in the scene level and facilitate a non-linear manner to browse videos. Experimental results are presented to demonstrate the effectiveness and efficiency by using VideoGraph to explore and access the video content. 相似文献
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论文对多媒体技术在英语教学中的应用了做了分析,比较了多媒体技术使用和传统模式的英语教学的不同特点,突出了多媒体技术的使用给英语教学改革带来了巨大的推动作用,并且根据教学经验,提出了多媒体技术在英语教学中使用要注意的一些问题。 相似文献
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Despite the successes in the last two decades, the state-of-the-art face detectors still have problems in dealing with images in the wild due to large appearance variations. Instead of leaving appearance variations directly to statistical learning algorithms, we propose a hierarchical part based structural model to explicitly capture them. The model enables part subtype option to handle local appearance variations such as closed and open month, and part deformation to capture the global appearance variations such as pose and expression. In detection, candidate window is fitted to the structural model to infer the part location and part subtype, and detection score is then computed based on the fitted configuration. In this way, the influence of appearance variation is reduced. Besides the face model, we exploit the co-occurrence between face and body, which helps to handle large variations, such as heavy occlusions, to further boost the face detection performance. We present a phrase based representation for body detection, and propose a structural context model to jointly encode the outputs of face detector and body detector. Benefit from the rich structural face and body information, as well as the discriminative structural learning algorithm, our method achieves state-of-the-art performance on FDDB, AFW and a self-annotated dataset, under wide comparisons with commercial and academic methods. 相似文献
179.
Extracting significant features from high-dimension and small sample size biological data is a challenging problem. Recently, Micha? Draminski proposed the Monte Carlo feature selection (MC) algorithm, which was able to search over large feature spaces and achieved better classification accuracies. However in MC the information of feature rank variations is not utilized and the ranks of features are not dynamically updated. Here, we propose a novel feature selection algorithm which integrates the ideas of the professional tennis players ranking, such as seed players and dynamic ranking, into Monte Carlo simulation. Seed players make the feature selection game more competitive and selective. The strategy of dynamic ranking ensures that it is always the current best players to take part in each competition. The proposed algorithm is tested on 8 biological datasets. Results demonstrate that the proposed method is computationally efficient, stable and has favorable performance in classification. 相似文献
180.