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101.
Weixin Guan Xiaochen Yang Chenyuan Dong Xiaoming Yan Wenji Zheng Yuan Xi Xuehua Ruan Yan Dai Gaohong He 《应用聚合物科学杂志》2021,138(8):49895
The packing pattern of two-dimensional (2D) sheet-like fillers in membranes is relatively random, leading to the unfavorable permeability from tortuous diffusion pathway. A new strategy that using prestructured materials with uniform channels as fillers was proposed. In this work, Ti3AlC2 is etched to prepare multilayered MXene (m-MXene), the channels aggregate as a whole unit, ensure the impossibility of ineffective packing compared with traditional individual sheets, largely facilitating the selective permeation. Then, the m-MXene/Poly (amide-6-b-ethylene oxide) (Pebax) MMMs are synthesized. SEM images demonstrate the accordion shaped structure of filler, which is the multi-channels laminates. Furthermore, the results of gas permeation test exhibit enhanced performance of m-MXene/Pebax MMMs. MMM with 0.5 wt.% m-MXene behaved best, CO2 permeability of 86.22 Barrer as well as CO2/N2 selectivity of 104.85, transcending the Robeson upper bound (2008). Having distinct enhancement for CO2 separation, the m-MXene/Pebax MMMs in this work offer prospective practical applications. 相似文献
102.
Jianping Shi Wei Zeng Zhiwang Yang Ju Li Pufang Zhao Hongtao Li Xingxing Yan Na Wen Ziqiang Lei Denglong Chen Jie Guan 《应用聚合物科学杂志》2021,138(21):50500
Organic–inorganic hybrid flame retardant was obtained by modifying aluminum hydroxide with different particle size with 1-hydroxyethylidene-1,1-diphosphonic acid. The structure of the organic–inorganic hybrid flame retardant is characterized by Fourier transform infrared spectroscopy, X-ray diffraction, and scanning electron microscopy, while 1H-NMR spectroscopy only characterizes specific samples. The thermal stability and flame retardancy of the samples were analyzed by thermogravimetric analysis, limiting oxygen index (LOI), vertical combustion of UL-94 and cone calorimeter. The results show that the modified 10 μm aluminum hydroxide has a better effect than the 25 μm aluminum hydroxide and 100 nm aluminum hydroxide. Compared with pure polyethylene terephthalate (PET), the LOI value of the best sample is increased by 24.4%, and UL-94 V reaches V-0 level. Heat release rate, total heat release rate, and carbon monoxide production rate decreased by 45.8%, 33.2%, and 41.5%, respectively, compared to pure PET. The results showed that the aluminum hydroxide with a particle size of 10 μm exhibited the best flame retardant effect, which could be attributed to the decomposition of organic phosphoric acid and the dehydration of aluminum hydroxide, yielding a higher amount of residual carbon. 相似文献
103.
104.
从塑性力学应力Lode参数着手,深入研究了应力Lode参数与各应力参量之间的内在联系,并对塑性理论中屈服准则进行了合理推广。对塑性理论及其应用具有重要意义。 相似文献
105.
Effect of rhenium addition on isothermal oxidation behavior of single-crystal Ni-based superalloy 总被引:1,自引:0,他引:1
The isothermal oxidation behavior of a nickel-based superalloy, which we designate as DD32, containing 4 wt.% rhenium and another alloy (DD32M) without rhenium were investigated at 900, 1000 and 1100 °C. Oxidized alloys were characterized by SEM, EDX, EPMA and XRD. The two alloys revealed similar oxidation rates at 900 °C, while the DD32 alloy showed a slightly higher mass gain than that of the DD32M alloy during 1000 and 1100 °C exposure. Surface and cross-sectional examination indicated that DD32 alloy showed nonuniform oxidation between dendritic and interdendritic areas at all temperatures. Similar different oxidation behavior between dendritic and interdendritic regions was also observed in the DD32M alloy at 900 °C. However, DD32M showed relatively uniform oxidation at 1000 and 1100 °C exposure. Therefore, Re addition clearly induced the nonuniform oxidation of the alloy. 相似文献
106.
采用自行设计的连续流变挤压成形设备成功制备出声10mm的AZ61镁合金线材。合金从辊靴型腔人口到出口的过程中,受到轧辊的剪切作用,枝晶臂不断受到剪切破碎,合金从浇注口到挤压区,逐渐由发达的枝晶状组织演化为细小的破碎晶、等轴晶和球形晶。在挤压成形时,中心部位固相变形小,边部大,在圆弧流动区产生了优良的超细晶组织。在合理的技术条件下,制备的AZ61合金线材断面组织优良,呈现两相塑性流动的特征。 相似文献
107.
Effects of distance between arc and heat sink on stress and distortion in DC-LSND welding technology
The characteristics of temperatures, stresses and strains fields have been studied numerically for a titanium alloy sheet welded with an improved gas tungsten arc welding method, in which a trailing spot heat sink is introduced to control the welding stress and distortion. The impinging jet model is employed to describe the internee heat transfer between the cooling media and the top suufuce of the workpiece. The influcnee of the distance between arc and heat sink is investigated. Results show that there is an ideal range of distance. Using the ideal distance, a low stress and no distortion welding structure can be derived. 相似文献
108.
Ni-15Cr-6W-3Mo-2Al-2Ti变形高温合金的室温抗张强度、塑性和冲击性能,随着合金中Si含量的变化呈现马鞍型的变化,即在0.4—0.6%Si范围内出现一个低塑性、低拉伸强度和低冲击韧性区。造成这种现象的本质原因是由于Si含量变化改变了晶界碳化物沉淀析出顺序、析出类型、析出量和析出形态。该合金晶界碳化物析出可分为四个阶段:第一阶段,<0.1%Si时,只有单一的M_(23)C_6析出;第二阶段,>0.1%Si以后,除M_(23)C_6外,M_6C开始析出,一直到0.4%Si时增加2缓慢;第三阶段,0.4—0.6%Si时,M_6C大量析出逐渐取代M_(23)C_6;第四阶段,>0.6%Si以后,M_6C量占绝对优势,但增加幅度比第三阶段小得多。从晶界形态来看,第一、二、四阶段皆属不连续的链状形式,只有第三阶段晶界呈现连续膜状。因此,造成性能下降的原因不是因为析出M_6C,而是它的形态,当它以颗粒状分布在晶界上时是一个很好的强化相。第三阶段的不正常析出是性能下降的本质因素。本研究结果打破了只要镍基合金中MO+1/2>W>6%(重量百分比)就形成M_6C的经验判据,“Si”才是该合金碳化物沉淀析出过程的控制因素。本文还对比了冶炼工艺差别对碳化物析出过程的影响。 相似文献
109.
高温高压CO2多相介质腐蚀研究及应用的新进展 总被引:4,自引:1,他引:4
CO2腐蚀是油气生产中所遇到的重大腐蚀难题之一。本文论述了腐蚀产物膜在 CO2多相流动介质中的作用,腐蚀产物膜力学性能测试和表征方法研究的进展及存在问题, CO2腐蚀形貌的类型及特征。 相似文献
110.
1 INTRODUCTIONMagnesiumchlorideisabasicmaterialforchem icalindustry ,andithaswideapplicationsinmetallur gy,architecturalmaterialandtextileindustry .Itisalsoamaterialforfire resistantproducts ,cryogenandcompoundfertilizerproductions[1] .Thefullydehy dratedmagnesiumchlorideisagoodmaterialforelec trolyticmetalmagnesium production .Becausemag nesiumchloridehasastrongadsorptiveability ,itisalsousedasadryingagent .Manysuccessfulworkshavebeendoneonthedehydrationofbischophite[2 10 ] .Butinfact,… 相似文献