Synthesis of carbon nanocapsules containing Fe, Ni or Co by arc discharge in aqueous solution

A simple, inexpensive and one-step synthesis method of metal-containing carbon nanocapsules using an arc discharge in aqueous solution is reported. It was found that Ni, Co and Fe nanoparticles could be in situ encapsulated in carbon shells when the arc was performed respectively in aqueous solutions of NiSO₄, CoSO₄ and FeSO₄. Transmission electron microscopy, energy dispersive X-ray spectroscopy and electron diffraction patterns of selected areas were used to determine the crystalline phase of the metal cores. To explain the formation mechanism of metal-containing carbon nanocapsules, a model of discharge in solution is proposed. This result presents a simply controllable way to synthesize metal-containing carbon nanocapsules.     

建筑电气设计中消防防火审核探讨

防火审核是建筑电气设计审核中的一个重要组成部分,要严格按照相关的防火规范设计和审核其设计,为建筑安全打下坚实的基础。分析、探讨了电气系统设计中防火审核的方法和相关技术,并提出了相关的设计对策和建议,以期能为相关人员提供参考。     

计算机网络安全威胁的技术特征与防范措施

目前,在计算机网络中存在许多不安全因素,这些因素不仅会对计算机的正常运行造成影响,还会对社会发展造成较大的影响.因此,我们要结合具体情况,采取有针对性的防范措施.简要分析了计算机网络安全威胁的特征和防范措施,希望可以为相关单位提供一些有价值的参考意见.     

浅析加快300 MW机组启动速度的方法及措施

随着电网的装机容量日益增大,机组的启动次数也在逐日增多。从保证机组安全经济运行的角度出发,结合笔者直接或间接参与制定的技术措施,简要分析了影响机组启动速度的因素和改善措施,以期为其他发电厂在机组启动方面提供一些参考和建议。     

服务于教学实践和创业实训的校园电子商务模式研究

将电子商务引入校园生活,可以很好地突破时间和空间的限制,最大限度地发挥其优势,给校园师生提供方便。我国的校园电子商务目前只处于起步阶段,这方面的研究也比较少。本文在分析国内高校电子商务教学和创业教育存在的主要问题基础上,对我国高校的校园电子商务常见模式进行归纳、分析和比较,并结合我校的实际优势,提出一种服务于教学实践和创业实训的校园电子商务模式并加以介绍。     

Automating fluid delivery in a capillary microfluidic device using low-voltage electrowetting valves

A multilayer capillary polymeric microfluidic device integrated with three normally closed electrowetting valves for timed fluidic delivery was developed. The microfluidic channel consisted two flexible layers of poly (ethylene terephthalate) bonded by a pressure-sensitive adhesive spacer tape. Channels were patterned in the spacer tape using laser ablation. Each valve contained two inkjet-printed silver electrodes in series. Capillary flow within the microchannel was stopped at the second electrode which was modified with a hydrophobic monolayer (valve closed). When a potential was applied across the electrodes, the hydrophobic monolayer became hydrophilic and allowed flow to continue (valve opened). The relationship between the actuation voltage, the actuation time, and the distance between two electrodes was performed using a microfluidic chip containing a single microchannel design. The results showed that a low voltage (4.5 V) was able to open the valve within 1 s when the distance between two electrodes was 1 mm. Increased voltages were needed to open the valves when the distance between two electrodes was increased. Additionally, the actuation time required to open the valve increased when voltage was decreased. A multichannel device was fabricated to demonstrate timed fluid delivery between three solutions. Our electrowetting valve system was fabricated using low-cost materials and techniques, can be actuated by a battery, and can be integrated into portable microfluidic devices suitable for point-of-care analysis in resource-limited settings.     

面向个性化云服务的动态信任模型

为更好地实践云计算为用户提供廉价按需服务的宗旨,满足服务请求者的个性化需求,提出一种面向个性化云服务的动态信任模型。基于细粒度服务思想定义个性化云服务,通过引入时间衰减因子和建立高效激励机制修正直接信任值,以灰色系统理论为基础计算实体间的评价相似度,并将评价相似度和推荐者的推荐可信度作为合成推荐信任值的重要因素,同时提出一种基于评价相似度的自信因子赋值方法,以提高合成综合信任值的准确性。实验结果表明,与GM-Trust模型及CCIDTM模型相比,该模型的交互成功率分别平均提高了4%和11%。     

(α-MS)S-B-(α-MS)S三嵌段共聚物的合成及其结构与性能

以α-甲基苯乙烯(α-MS),苯乙烯(S)和丁二烯(B)为单体,采用两步聚合偶合法,先将α-MS,S,THF及n-BuLi于30℃下聚合1h,再加入环己烷和B,于50℃下聚合4h,最后加入偶合剂苯甲酸苯酯,反应2～3h,即得到(α-MS)S-B-(α-MS)S三嵌段热塑性弹性体。该共聚物经GPC,IR,UV,NMR,DSC等表征,(?)_n=(10～13)×10~4,(?)_w/(?)_n=1.1～1.3;当硬段/软段为30/70(质量比)时,软段中1,4-结构含量为70％～85％,形态具有相分离特征,随α-MS/S值的增加,硬段T_g可在90～160℃调节,其力学性能有一定的改善,并接近或超过SBS热塑性弹性体。     

自适应收扩系数的双中心协作QPSO算法

针对量子粒子群优化(QPSO)算法迭代后期种群多样性下降、收敛速度慢、易陷入局部最优的缺点,提出一种自适应收缩-扩张系数的双中心协作最子粒子群优化算法。该算法从2个方面进行改进:(1)自适应调节收缩-扩张系数,其目的是帮助粒子跳出局部最优点,提高粒子的全局搜索能力;(2)双重更新全局最优位置,即在每次迭代中,先后分别采用2种不同的方式更新全局最优位置。第1种方式与QPSO算法一致,第2种方式则引入双中心粒子,使其和当前全局最优位置在相应维度上合作,从而达到更新全局最优位置的目的。从固定迭代次数和固定精度角度分析算法性能,仿真结果表明,相比于QPSO算法,该算法在保证复杂度较低的情况下,可提高收敛速度,增强全局和局部搜索能力。