玻纤增强复合材料及其复合绝缘横担覆冰特性研究

为了指导复合材料横担在重冰区的应用,本文开展了玻纤增强复合材料及复合材料绝缘横担的覆冰特性研究.结果表明:空白样品在垂直悬挂方式下的覆冰量和冰闪络电压均优于水平悬挂样品,且覆冰量均少于对应的亲水性的纯铝棒和Q345钢棒;涂覆PRTV涂料的复合材料样品覆冰量比空白样品少,对应的闪络电压大幅提升,且对应样品的冰面粘附力值最小,为纯铝棒冰面粘附力值的19％,而空白样品的冰面粘附力值为纯铝棒的78％.硅橡胶复合绝缘横担的覆冰特性正好和复合材料试样相反,水平悬挂方式下复合绝缘横担覆冰量相比垂直悬挂的同规格复合绝缘子减少了30％,闪络电压提高了51％.     

模具敏捷制造系统研究

针对模具设计制造过程复杂、条件苛刻和单件或小批量生产的特点 ,论述了模具产业发展敏捷制造技术的必要性。提出了模具敏捷制造系统框架和基于STEP与特征技术实现信息集成与过程集成的运行机制。阐述了基于Internet/Intranet的开放式可视化协同工作平台的模具敏捷制造实施方案。     

Effect of supports on the redox performance of pyrite cinder in chemical looping combustion

Chemical looping combustion (CLC) is a clean and efficient flame-free combustion technology,which combust the fuels by lattice oxygen from a solid oxygen carrier with inherent CO2 capture.The develop-ment of oxygen carriers with low cost and high redox performance is crucial to the whole efficiency of CLC process.As the solid by-product from the sulfuric acid production,pyrite cinder presented excellent redox performance as an oxygen carrier in CLC process.The main components in pyrite cinder are Fe2O3,CaSO4,Al2O3 and SiO2 in which Fe2O3 is the active component to provide lattice oxygen.In order to sys-tematic investigate the functions of supports (CaSO4,Al2O3 and SiO2) in pyrite cinder,three oxygen car-riers (Fe2O3-CaSO4,Fe2O3-Al2O3 and Fe2O3-SiO2) were prepared and evaluated in this study.The results showed that Fe2O3-CaSO4 displayed high redox activity and cycling stability in the multiple redox cycles.However,both Fe2O3-Al2O3 and Fe2O3-SiO2 experienced serious deactivation during redox reactions.It indicated that the inert Fe-Si solid solution (Fe2SiO4) was formed in the spent Fe2O3-SiO2 sample,which decreased the oxygen carrying capacity of this sample.The XPS results showed that the oxygen species on the surface of Fe2O3-CaSO4 could be fully recovered after the 20 redox cycles.It can be concluded that CaSO4 is the key to the high redox activity and cycling stability of pyrite cinder.     

综合能源互联网配电网故障定位与隔离的研究

基于"互联网+"的智慧能源互联网综合服务是互联网在电力行业的体现,充分利用了计算机技术、信息技术及人工智能技术等,具有信息的高效处理与状态的全面感知等优点,是实现万物互联互通的重要手段.现阶段配电网故障定位与隔离存在过程较繁琐、计算量及存储量大等缺陷,因此结合互联网中边缘计算的思想,提出一种基于综合能源互联网的配电网故障定位与隔离方法,设计了适用于综合能源互联网中配电网故障定位与隔离的模式与算法,实现了高效、快速定位的目标,同时减少了计算量与存储量,最后通过算例验证了方法的有效性.     

PAN/FPU Composite Nanofiber Membrane with Superhydrophobic and Superoleophobic Surface as a Filter Element for High-Efficiency Protective Masks

Recently, because of the outbreak of COVID-19, the demand for various types of filter elements in protective materials has increased globally. Furthermore, new requirements for the filtration performance of PM2.5 liquid (oil) particles have been put forward. In this work, Superhydrophobic and superoleophobic composite nanofibers with excellent filtration capacity for oil and salt particles are developed through the modification of polyacrylonitrile (PAN) by fluoro-polyurethane (FPU) doping. The results show that the PAN/FPU composite nanofibers doped with 9 wt% FPU has a uniform fiber morphology with a diameter of 240 ± 30 nm. Compared to the pure PAN nanofibers, the water-based contact angle of PAN/FPU increases from 90 ± 5° to 151 ± 5°, and the oil-based contact angle increases from 58 ± 2° to 152 ± 3°. Importantly, at a high flow rate of 95 L min⁻¹, the filtration efficiency of the PAN/FPU nanofiber membrane for 0.3 µm oil particles increases from 92 ± 1% to 99.2 ± 0.1%. After cyclic loading, the filtration efficiency of 0.3 µm oil particles remains above 98%. Meanwhile, the filtration efficiency for 0.3 µm salt particles remains at 98.23 ± 0.1%. The PAN/FPU nanofiber membrane developed in this work is effective in applications and has good market prospects as a protective filtration material.     

A “Three-in-One” Multifunctional Probe for Bcl-2/Mcl-1 Profiling and Visualizing in Situ

Bcl-2 and Mcl-1, the two arms of the anti-apoptotic Bcl-2 family proteins, have been identified as key regulators of apoptosis and effective therapeutic targets of cancer. However, no small-molecular probe is capable of profiling and visualizing both Bcl-2 and Mcl-1 simultaneously in situ. Herein, we report a multifunctional molecular probe (BnN₃-OPD-Alk) by a “three-in-one” molecular designing strategy, which integrated the Bcl-2/Mcl-1 binding ligand, fluorescent reporter group and photoreactive group azido into the same scaffold. BnN₃-OPD-Alk exhibited sub-micromolar affinities to Bcl-2/Mcl-1 and bright green self-fluorescence. It was then successfully applied for Bcl-2/Mcl-1 labeling, capturing, enriching, and bioimaging both in vitro and in cells. This strategy could facilitate the precise early diagnosis and effective therapy of dual Bcl-2/Mcl-1-related diseases.     

CHARAC TERIZATION OF TiAl POWDER PRODUCED BY MECHANICAL ALLOYING

The microstructure,alloying reaction and sintering behavior of the powder produced by Mechanical Al-loying(MA)for 8 h from 64 wt.-% Ti powder and 36 wt.-% Al powder were studied by scanning electronmicroscopy,optical microscopy,X-ray diffractometry,differential scanning calorimetry(DSC)and dilatometry.The mechanically alloyed powder partictes are Ti-Al composite particles.Thus,titanium aluminides can formeasily in the powder through diffusion during heat treatment.It is shown that the sintering behavior of this pow-der,different from the behaviors of TiAl alloy powder and mixed powder of 64 wt.-% Ti powder and 36 wt.-%Al powder,changes from expansion at temperatures below 1000℃ to shrinkage at temperatures above 1000℃.Homogeneously alloyed TiAl material with a density over 96% of the theoretical density can be produced fromthe mechanically alloyed powder by compaction-sintering.     

Effect of Heat Treatment on Microstructure and Mechanical Properties of Extruded PM Ti–6Al–4V Alloy With Deformation Flowlines

Metallurgical and Materials Transactions A - Two heat treatments, namely 955°C/2h/AC (AC = air cooling) and 955°C/4h/FC (FC = furnace cooling), were carried out on...     

基于地质勘查技术的矿山环境地质灾害预防探析

中国矿产资源总量庞大,很多矿产资源开采难度较高,勘查和解决好矿山环境地质灾害,是从业人员面临的难题之一。简述了利用地质勘查技术勘查矿山环境地质灾害的重要性,分析了典型矿山环境地质灾害类型,介绍了先进地质勘查技术,并给出了相关技术支撑下的矿山环境地质灾害预防对策,以提升矿山资源开采安全性。     

近2年我国锆铪及锆化学制品雕生产、贸易及研发概况

介绍了我国近2年来海绵锆、锆铪制品和锆化学品的生产、进出口概况,以及重要研发进展。我国工业级海绵锆产量从2003年的100t增加到2005年的174t,2005年的销售量达到150t;锆粉与锆-铝消气剂等年产量在10t左右;锆材和锆设备年产量在100t以上;锆化学制品品种有10余种,年产量已达到20×104t。锆砂的沸腾氯化工艺、锆铪的MIBK法分离工艺、以电熔ZrO2为原料制取粗ZrCl2工艺和Al-Y复合ZrO2粉的生产工艺等的研发工作,都取得了突破性进展。