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排序方式： 共有651条查询结果，搜索用时 15 毫秒
61.
B. W. Wojciechowski 《加拿大化工杂志》1992,70(4):721-726
This work introduces the Temperature-Scanning Adiabatic Plug-Flow Reactor (TSAR-PF), a fast and efficient method for studying kinetics. The proposed method of operation and data reduction offers an attractive alternative to the isothermal methods presently used in kinetic studies and catalyst evaluation and reduces the labour required to collect such data by some orders of magnitude, making studies over a broad range of conditions possible at reasonable cost. The proposed experimental method involves ramping (scanning) of the input temperature to an adiabatic plug-flow reactor while recording both conversion and output temperature. The interpretation of this data to yield rate parameters is described. 相似文献
62.
Hürmüs Gürsu Yamur Güner Kamil Burak Dermenci Metin Genten Ahmet Furkan Bulu Umut Savac&#x; Servet Turan Yücel ahin 《国际能源研究杂志》2019,43(10):5346-5354
Nowadays, doped graphenes are attracting much interest in the field of Li‐ion batteries since it shows higher specific capacity than widely used graphite. However, synthesis methods of doped graphenes have secondary processes that requires much energy. In this study, in situ synthesis of N‐doped graphene powders by using of cyclic voltammetric method from starting a graphite rod in nitric acid solution has been discussed for the first time in the literature. The N‐including functional groups such as nitro groups, pyrrolic N, and pyridinic N have been selectively prepared as changing scanned potential ranges in cyclic voltammetry. The electrochemical performance as anode material in Li‐ion batteries has also been covered within this study. N‐doped graphene powders have been characterized by electrochemical, spectroscopic, and microscopic methods. According to the X‐ray photoelectron spectroscopy and Raman results, N‐doped graphene powders have approximately 16 to 18 graphene rings in their main structure. The electrochemical analysis of graphene powders synthesized at different potential ranges showed that the highest capacity was obtained 438 mAh/g after 10 cycles by using current density of 50 mA/g at N‐GP4. Furthermore, the sample having higher defect size shows better specific capacity. However, the more stable structure due to oxygen content and less defect size improves the rate capabilities, and thus, the results obtained at high current density indicated that the remaining capacity of N‐GP1 was higher than the others. 相似文献
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64.
Lucyna Dymińska Maciej Calik Abduladhim Moamer M. Albegar Adam Zając Kamil Kostyń Jadwiga Lorenc 《International Journal of Food Properties》2017,20(9):2003-2015
Thirteen edible oils: sunflower, avocado, hemp, high-linolenic flax, low-linolenic flax, safflower, walnut, roasted sesame, rice, corn, rapeseed, pumpkin seed, and hazel were studied in this work. Their fatty acid composition, iodine, acidic, peroxide, and saponification values were determined. Infrared and Raman spectra of the oils were recorded in the range 400–3200 cm?1. The integral intensities of the bands at about 1655 and 2852 cm?1 corresponding to ν(C=C) and ν(CH2) vibrations were evaluated and used to construct a relationship between the spectroscopic data and the iodine value. The following linear dependencies were obtained: Iν(C=C)/Iν(CH2) = 7.449 × 10?4 × iodine value – 0.0339 and Iν(C=C)/Iν(CH2) = 9.299 × 10?4 × iodine value – 0.023 for the infrared and Raman spectra with a correlation coefficient 0.988 and 0.976, respectively. These calibration lines can be used to determine the iodine value for oils with unknown unsaturation level, and may be applied for margarines and other fatty materials. 相似文献
65.
Khondakar Kamil Reza Jing Wang Ramanathan Vaidyanathan Shuvashis Dey Yuling Wang Matt Trau 《Small (Weinheim an der Bergstrasse, Germany)》2017,13(9)
Cancer diagnosis and patient monitoring require sensitive and simultaneous measurement of multiple cancer biomarkers considering that single biomarker analysis present inadequate information on the underlying biological transformations. Thus, development of sensitive and selective assays for multiple biomarker detection might improve clinical diagnosis and expedite the treatment process. Herein, a microfluidic platform for the rapid, sensitive, and parallel detection of multiple cancer‐specific protein biomarkers from complex biological samples is presented. This approach utilizes alternating current electrohydrodynamic‐induced surface shear forces that provide exquisite control over fluid flow thereby enhancing target–sensor interactions and minimizing non‐specific binding. Further, the use of surface‐enhanced Raman scattering‐based spectral encoding with individual barcodes for different targets enables specific and simultaneous detection of captured protein biomarkers. Using this approach, the specific and sensitive detection of clinically relevant biomarkers including human epidermal growth factor receptor 2 (HER2); Mucin 1, cell surface associated (MUC1); epidermal growth factor receptor; and Mucin 16, cell surface associated (MUC16) at concentrations as low as 10 fg mL?1 in patient serum is demonstrated. Successful target detection from patient samples further demonstrates the potential of this current approach for the clinical diagnosis, which envisages a clinical translation for a rapid and sensitive appraisal of clinical samples in cancer diagnostics. 相似文献
66.
Wan Ahmad Kamil Mahmood Mohammad Hossein Azarian Wan Farahhanim bt Wan Fathilah Eunice Kwok 《应用聚合物科学杂志》2017,134(28)
The present study describes the preparation and characterization of a novel nanocomposite, based on montmorillonite clay (MMT) encapsulation in poly(ethylene glycol) (PEG) by an electrospraying process. PEG/MMT nanocomposites with MMT contents ranging from 1 to 5 wt % were successfully prepared and characterized in relation to their morphological, spectroscopic, structural, and thermal properties. Scanning electron microscopy, transmission electron microscopy, and atomic force microscopy micrographs showed that the PEG nanobeads formed spherical shapes, and with increasing amount of MMT clay, the size of the beads decreased significantly, ranging from 120 to 3.7 nm. The Fourier transform infrared spectroscopy results suggested that there was no significant chemical interaction between PEG and MMT clay. However, the d‐spacing of MMT clay in PEG/MMT increased, a clear indication of the intercalation of PEG in the interlayer spaces of MMT clay. Furthermore, the thermal stability of PEG polymer decreased upon encapsulation of MMT clay in PEG/MMT composites. Nanoindentation results showed that the hardness and Young's modulus of the PEG/MMT composites increased with 3 wt % loading of MMT. © 2017 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2017 , 134, 45048. 相似文献
67.
Transactional memory (TM) is an approach to concurrency control that aims to make writing parallel programs both effective and simple. The approach has been initially proposed for nondistributed multiprocessor systems, but it is gaining popularity in distributed systems to synchronize tasks at large scales. Efficiency and scalability are often the key issues in TM research; thus, performance benchmarks are an important part of it. However, while standard TM benchmarks like the Stanford Transactional Applications for Multi‐Processing suite and STMBench7 are available and widely accepted, they do not translate well into distributed systems. Hence, the set of benchmarks usable with distributed TM systems is very limited, and must be padded with microbenchmarks, whose simplicity and artificial nature often makes them uninformative or misleading. Therefore, this paper introduces Helenos, a realistic, complex, and comprehensive distributed TM benchmark based on the problem of the Facebook inbox, an application of the Cassandra distributed store. 相似文献
68.
Firouz FADAEIFARD Khamirul Amin MATORI Meysam TOOZANDEHJANI Abdul Razak DAUD Mohd Khairol Anuar Mohd ARIFFIN Norinsan Kamil OTHMAN Farhad GHARAVI Abdul Hadi RAMZANI Farhad OSTOVAN 《中国有色金属学会会刊》2014,24(4):1004-1011
采用场发射扫描电子显微镜(FE-SEM),研究转速对厚度为5 mm的6061-T6铝合金搅拌摩擦搭接焊接头的宏观和微观组织、硬度、搭接头剪切性能和失效模式的影响。结果表明:在最低的转速度下,上模板和下模板具有十分相似的硬度分布。采用EDX分析发现,焊核区的断裂面中含有Fe的化合物。 相似文献
69.
70.