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61.
The Change of X‐ray Diffraction Peak Width During in situ Conventional Sintering of Nanoscale Powders
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Jean‐Marie Lebrun Shikhar K. Jha Kiran S. Naik Kevin C. Seymour Waltraud M. Kriven Rishi Raj 《Journal of the American Ceramic Society》2016,99(3):765-768
Diffraction peaks of nanoscale particles of 3 mol% yttria‐stabilized zirconia become sharper as the powder sinters. The reduction in the peak width is correlated with the increase in density. The sharpening of the peak agrees reasonably well with the remaining free surface area as the sample sinters. Therefore, high curvature of the free surface of the pores is assumed to lead to peak broadening (the grain boundaries that grow at the expense of the free surfaces of the pores do not have this curvature). The change in the grain size during sintering does not make a significant contribution to peak width. 相似文献
62.
Susana M. Olhero Ajay Kaushal José M. F. Ferreira 《Journal of the American Ceramic Society》2014,97(3):725-732
This study reports on the fabrication of BST (Ba0.6Sr0.4TiO3)‐based 3D microcomponents through an aqueous colloidal approach. The BST powder was synthesized by solid‐state reaction assisted by thermal analysis and XRD diffraction. Well crystalline cubic BST single phase was obtained upon heat‐treating the precursor powder mixture at 1200°C–1250°C. The reactivity of the BST powder toward water was evaluated by the changes in pH and concentration of leached ionic species along aging time. Hydrolysis reactions were suppressed by chemisorbing a suitable phosphate‐based protective agent and enabled an excellent dispersion ability to be achieved. Aqueous suspensions with solids loadings as high as 50 vol% that are stable against hydrolysis for several days could easily be prepared from the surface‐treated BST powder in aqueous solutions of an epoxy resin. After adding a suitable hardener, the colloidal suspensions could easily be cast into soft silicon rubber molds to obtain homogeneous and high dense green BST bodies. 相似文献
63.
Jaykumar Patel Deepesh Khandwal Babita Choudhary Dolly Ardeshana Rajesh Kumar Jha Bhakti Tanna Sonam Yadav Avinash Mishra Rajeev K. Varshney Kadambot H. M. Siddique 《International journal of molecular sciences》2022,23(2)
The frequency and severity of extreme climatic conditions such as drought, salinity, cold, and heat are increasing due to climate change. Moreover, in the field, plants are affected by multiple abiotic stresses simultaneously or sequentially. Thus, it is imperative to compare the effects of stress combinations on crop plants relative to individual stresses. This study investigated the differential regulation of physio-biochemical and metabolomics parameters in peanut (Arachis hypogaea L.) under individual (salt, drought, cold, and heat) and combined stress treatments using multivariate correlation analysis. The results showed that combined heat, salt, and drought stress compounds the stress effect of individual stresses. Combined stresses that included heat had the highest electrolyte leakage and lowest relative water content. Lipid peroxidation and chlorophyll contents did not significantly change under combined stresses. Biochemical parameters, such as free amino acids, polyphenol, starch, and sugars, significantly changed under combined stresses compared to individual stresses. Free amino acids increased under combined stresses that included heat; starch, sugars, and polyphenols increased under combined stresses that included drought; proline concentration increased under combined stresses that included salt. Metabolomics data that were obtained under different individual and combined stresses can be used to identify molecular phenotypes that are involved in the acclimation response of plants under changing abiotic stress conditions. Peanut metabolomics identified 160 metabolites, including amino acids, sugars, sugar alcohols, organic acids, fatty acids, sugar acids, and other organic compounds. Pathway enrichment analysis revealed that abiotic stresses significantly affected amino acid, amino sugar, and sugar metabolism. The stress treatments affected the metabolites that were associated with the tricarboxylic acid (TCA) and urea cycles and associated amino acid biosynthesis pathway intermediates. Principal component analysis (PCA), partial least squares-discriminant analysis (PLS-DA), and heatmap analysis identified potential marker metabolites (pinitol, malic acid, and xylopyranose) that were associated with abiotic stress combinations, which could be used in breeding efforts to develop peanut cultivars that are resilient to climate change. The study will also facilitate researchers to explore different stress indicators to identify resistant cultivars for future crop improvement programs. 相似文献
64.
In the present communication, fifteen different glazing systems ranging from 3 mm single glazed clear glass to double glazed with low-e and solar control coating, have been analysed in terms of their human thermal comfort impact. Thermal comfort is measured in term of PMV (predicted mean vote) and PPD (predicted percentage of dissatisfied). Study encompasses all the six climatic zones of India. By using OPTICS 5.0 and WINDOW 5.0, U-values, solar heat gain coefficient, inside glazing surface temperatures and inside solar radiation have been computed. Depending upon different climatic zones, six sets of different design conditions, in terms of ambient temperatures, solar radiation and wind velocity, have been chosen. Typical values of metabolic rate and clothing insulation taken are 1.2 met and 0.5 clo for summer and 1.0 met and 1.0 clo for winter, respectively. Inside room air velocity is taken as 0.15 m s−1 round the year. Room temperature is taken as 20 °C in winter and 25 °C in summer. It is found that for cold station (e.g. Leh) all glazings except solar control glazings, ensure thermal comfort and total PPD is less than 10% (|PMV|?0.5). For warm and hot climates, solar control glazings are thermally suitable. Results for winter night of Delhi shows that all the 15 glazings are inadequate for thermal comfort and PPD, due to cold feeling, varies between 27% and 33% approximately. 相似文献
65.
The integral diaphragm pressure transducers machined out of precipitation hardened martensite stainless steel (APX4) are widely used for propellant pressure measurements in space applications. These transducers are expected to exhibit dimensional stability and linearity for their entire useful life. These vital factors are very critical for the reliable performance and dependability of the pressure transducers. However, these transducers invariably develop internal stresses during various stages of machining. These stresses have an adverse effect on the performance of the transducers causing deviation from linearity. In order to eliminate these possibilities, it was planned to cryotreat the machined transducers to improve both the long-term linearity and dimensional stability. To study these effects, an experimental cryotreatment unit was designed and developed based on the concept of indirect cooling using the concept of cold nitrogen gas forced closed loop convection currents. The system has the capability of cryotreating large number of samples for varied rates of cooling, soaking and warm-up. After obtaining the initial levels of residual stress and retained austenite using X-ray diffraction techniques, the pressure transducers were cryotreated at 98 K for 36 h. Immediately after cryotreatment, the transducers were tempered at 510 °C for 3 h in vacuum furnace. Results after cryo treatment clearly indicated significant reduction in residual stress levels and conversion of retained austenite to martensite. These changes have brought in improvements in long term zero drift and dimensional stability. The cryotreated pressure transducers have been incorporated for actual space applications. 相似文献
66.
Narayan N. Som Venu Mankad Prafulla K. Jha 《International Journal of Hydrogen Energy》2018,43(47):21634-21641
The state-of-the-art density functional theory (DFT) is employed to study the catalytic activity of arsenene for hydrogen evolution reaction (HER) and oxygen evolution reaction (OER). We have included dispersion correction to get accurate adsorption energy on the individual catalytic surface (top site). Using binding energy calculation, arsenene is shown to be a potential candidate for HER. Here we investigate the stability and electronic properties of the honeycomb structure of the arsenene system using first-principles calculation to find the effect of different dopants on the fundamental band gap, which is one of the primary parameters in the photocatalytic water splitting. Further, we sieved the dopant for better HER catalytic activity by substituting one of the arsenene (As) atoms by B, N, O, Ge, Ga and Se atoms to make arsenene a better candidate for HER. Our studies depict that HER activity is increased by 82% for O-doped arsenene and OER activity by 87% for B-doped arsenene as compared to pristine arsenene. 相似文献
67.
Investigation on germanium oxide-based glasses for infrared optical fibre development 总被引:1,自引:0,他引:1
We demonstrate the suitability of GeO2 for fibre engineering by compositional modifications of core and cladding glasses using the rod-in-tube technique, which have been matched for fibre drawing. The methods adopted for identifying the core–clad combination (56GeO2–31PbO–9Na2O–4Ga2O3 and 55GeO2–30PbO–11Na2O–4Ga2O3) are explained, based on the thermal, viscosity, and optical properties. We specially point out to the relatively high transformation temperature range (Tg > 380 °C) of the glass, which is suitable for chemical sensing and metrological applications in the 150–200 °C. The total intrinsic loss is compared with the measured loss in multi- and single-mode fibres from 0.532 to 2.02 μm, with loss less than 2.5 dB m−1 in the 1000–1600 nm range. The origin of larger loss outside this region is explained. 相似文献
68.
Cadmium-plated 0.35C–3.5Ni–1.5Cr–0.5Mo steel threaded fasteners of 1230 MPa properties class are used for aerospace applications.
These fasteners were torqued to 13 N·m. Few fasteners parted into two pieces while in use under sustained assembly load for
a period of 50 days. The fracture surface of the failed fasteners had two distinct regions when viewed under microscope at
higher magnification. Fractography revealed that the larger region consisted of predominantly intergranular features, whereas
the smaller region had features of microvoid coalescence. From the metallography evidences it was concluded that the fastener
failure was due to hydrogen embrittlement. Electro-deposit of cadmium was identified to be the main source for hydrogen entrapment,
which could not be compelled completely by post-plating baking treatment. 相似文献
69.
The phenomenon of constrained sintering, where large rigid inclusions of alumina have been shown to significantly reduce the rate of sintering of titania [Bordia and Raj (1988) J. Am. Ceram. Soc. 71, 302–310], is shown to subside nearly completely during flash sintering carried out under modest electrical fields. The result is explained by a different mechanism for volumetric and shear deformation under electric fields. It is proposed that vacancy and interstitials generated within the grains migrate to grain boundaries and pores to produce both volumetric and shear strain at equal rates, since, in this way, the diffusion distance for both modes of deformation becomes the same. In conventional sintering, where transport occurs from one interface to another, the diffusion distance for shear is twice as far as for densification, which retards sintering should it become controlled by shear deformation, as seen in constrained sintering. 相似文献
70.
Implementation of monitoring strategy for increasing the efficiency of groundwater pollutant source characterization is often necessary, especially when only inadequate and arbitrary concentration measurement data are initially available. Two main parameters that need to be estimated for efficient and accurate characterization of groundwater pollution sources are: location of the source and the time when the source became active. Complexities involved with the explicit estimation of the time of start and source activity have not been addressed so far in previous studies. The main complexity arises due to the fact that the spatial location and time of activity are inter-related. Therefore, specifying one and solving for the other simplifies the source characterization problem. Hence, in this study, both the source location and time of initiation are treated as unknowns. The developed methodology uses dynamic time warping distance in the linked simulation-optimization model to address some complex issues in designing a monitoring network to efficiently estimate source characteristics including the time of first activity of unknown groundwater source. Performance of the developed methodology is evaluated on illustrative contaminated aquifer. These evaluation results demonstrate the potential use of the developed methodology. 相似文献