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排序方式: 共有1317条查询结果,搜索用时 62 毫秒
261.
Yoshinobu Nakamura Kazuhiro Yamamura Nozomi Karyu Kohei Shitajima Syuji Fujii Yoshiaki Urahama 《Journal of Adhesion Science and Technology》2013,27(9):821-838
The influences of debonding rate and temperature on the peel behavior of polyacrylic block copolymer/tackifier system were investigated. Poly(methyl methacrylate)-block-poly(n-butyl acrylate)-block-poly(methyl methacrylate) triblock copolymer (MAM) with hard block contents of 23 (MAM-23) and 16 wt.% (MAM-16) and a 1/1 blend with a diblock copolymer (MA) consisting of the same components (MAM-23/MA, total hard block content of 15 wt.%) were used as the base polymer. A special rosin ester was used as a tackifier at various contents in the block copolymer/tackifier system. The peeling process at the probe/adhesive interface during probe tack testing was observed using a high-speed microscope at 23 °C with debonding rate of 10 mm/s. Three different peeling mechanisms were observed. Type A, where peeling progressed linearly from the edge to the center of the probe without cavitation (MAM-23). Type B, where peeling progressed linearly from the edge to the center of the probe with cavitation (MAM-16). Type C, where cavitation occurred over the entire adhesive layer, and peeling initiation was delayed (MAM-23/MA). The peel behavior of MAM-23 changed from Type A to Type B with a decrease of the debonding rate (1 mm/s) or increase of the temperature (40 °C). In contrast, there was no change for MAM-16 and MAM-23/MA. Cavity formation in an adhesive layer restrains peeling; therefore, it is desirable for improvement of the adhesion strength. The tack properties increased with the tackifier content, and the formation of cavitation was less than that for the systems without the tackifier. 相似文献
262.
Naohisa Tamura Kazuhiro Ban Shinya Takahashi Shoji Obuchi 《The Journal of Adhesion》2013,89(4):355-373
Poly(L-lactic acid) (PLLA) was blended with poly(butylenesuccinate) (PBS) using a single-screw extruder to modify the poor characteristics of these polymers. Furthermore, when both polymers were blended, the graft copolymer that was synthesized by partially saponified poly(vinyl alcohol) (PSPVA) and ?-caprolactone (?-CL) was used as a novel compatibilizer. The structure of the synthesized compatibilizer was determined by 1H or 13C NMR. From this result, the ring-opening polymerization of the ?-CL occurred at the hydroxyl group of PSPVA. The structures of the PLLA/PBS solvent-cast blended films could be observed via an optical microscope. From the optical microscopic observation, the structures of the solvent-cast blended films with the synthesized compatibilizer were more homogeneous than those of the solvent-cast blended films without the compatibilizer. The mechanical properties of the PLLA/PBS extruded blended films were determined by a tensile test. The result showed the tensile strength of the blended films with the synthesized compatibilizer was greater than that of the blended films without the compatibilizer. 相似文献
263.
Kazuhiro Yamamura Syuji Fujii Yoshinobu Nakamura Kazuko Fujiwara Shigeki Hikasa Yoshiaki Urahama 《应用聚合物科学杂志》2013,129(3):1008-1018
The influence of diblock copolymer addition on the tack properties of a polyacrylic triblock copolymer/tackifier system was investigated. For this purpose, poly(methyl methacrylate)‐block‐poly(n‐butyl acrylate)‐block‐poly(methyl methacrylate) triblock copolymer (MAM) and a 1/1 blend with a diblock copolymer consisting of the same components (MA) were used as base polymers, and a tackifier was added in amounts ranging from 10 to 30 wt %. The temperature dependence of tack was measured by a probe tack test. The tack of MAM/MA at room temperature was significantly higher than that of MAM, and the improvement of MAM/MA upon the addition of the tackifier was higher than that of MAM. The peeling process at the probe/adhesive interface during the probe tack test was observed using a high‐speed microscope. It was found that for MAM/MA, cavitation was caused in the entire adhesive layer, and peeling initiation was delayed by the absorption of strain energy due to deformation of the adhesive layer. In contrast, for MAM, peeling progressed linearly from the edge to the center of the probe. The greater flexibility of the soft block chain in the diblock copolymer resulted in improved interfacial adhesion. 1H pulse nuclear magnetic resonance analysis showed that the addition of the tackifier improved the cohesive strength of the adhesive. Adhesion strength is affected by two factors: the development of interfacial adhesion and cohesive strength. In the MAM/MA/tackifier system, the presence of MA and the tackifier improved the interfacial adhesion and cohesive strength, respectively. © 2012 Wiley Periodicals, Inc. J. Appl. Polym. Sci., 2013 相似文献
264.
Kazuyuki Matsumoto Yasuhiro Miyake Yuzo Umeda Hiroshi Matsushita Hiroaki Matsuda Akinobu Takaki Hiroshi Sadamori Kazuhiro Nouso Takahito Yagi Toshiyoshi Fujiwara Kazuhide Yamamoto 《International journal of molecular sciences》2013,14(10):20877-20889
This study aimed to investigate the associations of the serial changes of serum levels of various growth factors with liver regeneration after hepatectomy in healthy liver donors. Sixteen healthy liver donors who underwent conventional liver resection were included. Serum levels of various growth factors before hepatectomy and on postoperative day (POD) 1, 3, 5 and 7 were measured. Liver volume data calculated by multi-detector computed tomography using workstation. The ratio of remnant liver volume on POD 0 to liver volume before the operation was 51% ± 20%. The ratio of liver volume on POD 14 to liver volume on POD 0 were inversely correlated with remnant liver volume on POD 0 (r = −0.91). The ratio of liver volume on POD 14 to liver volume on POD 0 were significantly correlated with serum hepatocyte growth factor (HGF) levels on POD 1 (r = 0.54), serum leptin levels on POD 1 (r = 0.54), and serum macrophage colony-stimulating factor (M-CSF) levels on POD 5 (r = 0.76) and POD 7 (r = 0.80). These results suggest that early-phase elevation of serum levels of HGF, leptin and M-CSF may be associated with the acceleration of liver regeneration after hepatectomy in humans. 相似文献
265.
Shi-Guang Li Ryosuke Matsubara Toshio Matsusue Masatoshi Sakai Kazuhiro Kudo Masakazu Nakamura 《Organic Electronics》2013,14(4):1157-1162
Innovative sensing systems based on THz electromagnetic waves have been attracting a great deal of attention. Although many THz detectors have been developed over the years, it is currently difficult to manufacture low-cost THz sensing/imaging devices. In the present study, we propose to use organic field-effect transistors (OFETs) and small potential fluctuation against the carriers within them (N. Ohashi, H. Tomii, R. Matsubara, M. Sakai, K. Kudo, M. Nakamura, Appl. Phys. Lett. 91 (2007) 162105). We use THz time-domain spectroscopy for OFETs in which the carrier density in the pentacene active layer is modulated by the gate bias. We found evidence that the accumulated free holes in pentacene films can be excited by THz photons to overcome the surrounding barriers in the fluctuating potential. The Drude–Lorentz model could not account for the shape of the absorption spectra, which suggests that the holes are weakly restricted by the potential fluctuation. The integrated absorption intensity was proportional to the transfer characteristics of the OFETs. The present findings represent an important step toward developing a new class of THz-wave sensors. 相似文献
266.
Yuki Hori Kazuhiro Fujimori Kenji Tsuruta Shigeji Nogi 《Electrical Engineering in Japan》2013,184(3):27-35
In this paper, a transducer that is suitable for the ultrasonic wireless power transmission system is discussed. The transducer is designed based on Mason's equivalent circuit theory, basically. The transducer was developed using design parameters optimized by multiphysics analysis. As a result, it is con?rmed that the transmission e?ciency is drastically improved to more than 50%. This result suggests that wireless power transmission by acoustic wave is feasible. © 2013 Wiley Periodicals, Inc. Electr Eng Jpn, 184(3): 27–35, 2013; Published online in Wiley Online Library (wileyonlinelibrary.com). DOI 10.1002/eej.22406 相似文献
267.
268.
Katsuyuki Kunii Kazuhiro Narahara Shoji Yamanaka 《Microporous and mesoporous materials》2001,50(2-3):181-185
A microporous aluminophosphate molecular sieve, AlPO4-H3, was prepared without using organic templates. It was crystallized at temperatures as low as 90 °C from aluminophosphate gels with a molar ratio of Al2O3/P2O51; the addition of seed crystals was essential. AlPO4-H3 was topotactically and irreversibly converted into AlPO4-D at 300 °C, which adsorbed water up to 0.2 ml/g at 25 °C, although nitrogen gas was hardly adsorbed at liquid nitrogen temperature. 相似文献
269.
The effect of thermal cycling and aging in martensitic state in Ti-Pd-Ni alloys were investigated by DSC and TEM observations. It is shown that the thermal cycling causes the decreases in M, and Af temperatures in Ti50Pd50-xNix (x=10, 20, 30) alloys, but no obvious thermal cycling effect was observed in Ti50Pd50Pd40Ni10 alloys and the aging effect shows a curious feature, i.e., the Af temperature does not saturate even after relatively long time aging, which is considered to be due to the occurrence of recovery recrystallization during aging. 相似文献
270.
Giuseppe Pezzotti Hans-Joachim Kleebe Kazuhiro Okamoto Ken'ichi Ota 《Journal of the American Ceramic Society》2000,83(10):2549-2555
Three high-purity SiAlON materials (Si6− z Al z O z N8− z , z = 1, 2, 3) were characterized with respect to both structure and viscous behavior of internal grain boundaries. Internal friction experiments provided a direct measure of the intrinsic viscosity of grain boundaries and concurrently revealed the occurrence of a grain-boundary interlocking mechanism that suppressed sliding. A residual glass phase (consisting of aluminum-rich SiO2 ) and nanometer-sized mullite residues were found at glassy triple-grain junctions of the z = 1 SiAlON. A low-melting intergranular phase dominated the high-temperature behavior of this material and caused grain-boundary sliding at temperatures as low as 1100°C. A quantitative analysis of the grain-boundary internal friction peak as a function of oscillation frequency indicated an intergranular film viscosity of log η∼ 7.5 Pa · s at 1100°C. Glass-free grain boundaries were a characteristic of SiAlON materials with z ≥ 2, which yielded a significant improvement in refractoriness as compared to the z = 1 SiAlON material. In these materials, relaxation resulting from grain-boundary sliding was suppressed, and the internal friction curve simply experienced an exponential-like increase. 相似文献