饮用水中挥发性三卤甲烷(THM)_s测定方法的改进

本文使用吹扫捕集法来前处理水样,用带有电子捕获检测(ECD)的气相色谱仪来测定水中三卤甲烷(THM)_s。水样加标回收率在85%～115%之间,相对标准偏差在5%左右。实验结果表明,该法具有简单、快速、灵敏的特点。     

A multi-criterion interaction-oriented model with proportional rule for designing supply chain networks

Supply chain management has offered a way to improve the industrial environment becomes more competitive. While, the commonly seen methodologies may be effective in solving the production–distribution problem only from supplier- or customer-oriented consideration, those cannot present the interactive relationship between upstream and downstream enterprises. In the competitive semiconductor industry environment, considering the viewpoints of the supplier and consumer simultaneously is particularly required, because multiple manufacturing and demanding steps are performed at separate situations, concurrently. In this paper, we propose an interaction-oriented approach, which bases on the analytic hierarchy process (AHP) methodology and proportional rule, to solve the semiconductor distribution problem with multiple quantitative and qualitative criteria. The developed approach gives an expected satisfaction for the all participators of the whole chain while the cooperative information is shared perfectly and effectively. Analysis results demonstrate the proposed methodology is efficient and effective through a real world case study.     

胨冻样芽孢杆菌(Bacillus mucilaginosus)对烟草灰霉病菌(Botrytis cinerea)的抑制作用

本文首次报道胨冻样芽孢杆菌XDB1和D4B1对烟草灰霉病菌(Botrytis cinerea)的抑制作用。实验表明,XDB1和D4B1的发酵原液和无细胞提取物具有相同的抑菌效果,而经121℃处理30分钟后,抑菌活性丧失。D481菌株的抑菌活性高于XDB1,钾长石作为基质时的活性高于土壤矿物。但是,XDB1和D481对立枯丝核病菌(R..solani)、西瓜尖孢镰刀菌(F.oxysporum)、腐霉(Pythium sp)、小麦全蚀病菌(G.graminis)、烟炭疽病菌(C.gloeosporides)、烟草赤星病菌(A.alternata)、烟草黑胫病菌(P.nicotianae、串珠镰刀病菌(F.moniliforme)和水稻稻瘟病菌(P.grisea)无抑制作用。     

以硅氧烷醇锂为催化剂的氟硅生胶的合成

介绍了单体三氟丙基甲基环三硅氧烷通过硅氧烷醇锂催化剂聚合成氟硅生胶,讨论了不同催化剂及其用量,原料中水分含量、不同乙烯基含量对氟硅生胶分子量的影响.     

盐湖沉积储层孔隙结构特征及演化模式--以马王庙油田为例

盐湖沉积条件下的沉积环境及储集层特征等具有与淡水沉积不同的特征,通过对江汉盐湖盆地马王庙地区储层孔隙结构特征的研究,揭示了孔隙结构的宏观及微观特征.该区新沟咀组下段砂岩储层孔隙类型以粒间溶孔为主,喉道主要为片状、弯片状及点状喉道.Ⅱ、Ⅲ油组的物性比Ⅰ油组好,平面上孔隙分布具分区性.孔喉配置主要为大孔中喉,次为大孔粗喉及中孔中喉.孔隙结构受沉积环境及成岩作用的影响.以马36井Ⅱ油组砂岩为例,建立了孔隙演化定量模式.     

Optically tuned superconductive-dielectric resonators with whispering-gallery modes

An analytical method is presented for calculating the resonant frequency andQ-factor of a superconducting dielectric disk resonator operating in millimeter-wave regime with whispering-gallery mode. Resonant frequency shift due to the optical generation of quasi-particles in superconducting film is investigated as a function of photon flux. An optically tunable resonant frequency of about 500 MHz is estimated, and good agreement is found between numerical results and experimental ones.     

溶质原子在再结晶运动晶界上偏聚的研究

Ｂ~（１０）（ｎ，α）Ｌｉ~７裂变反应的径迹显微照相技术被用来研究含硼Ｆｅ－３０％Ｎｉ合金高温热变形再结晶过程中硼在晶界上的偏聚行为，实验表明，含硼Ｆｅ－３０％Ｎｉ合金１０００℃热变形２０％再结晶过程中，运动晶界前方发生硼偏聚而后方发生贫硼现象，而在静止晶界上看不到硼偏聚，随着再结晶新晶粒的长大，运动晶界上的硼偏聚变弱。本文提出，可以用晶界对溶质原子热运动散射的量子理论来解释溶质原子在运动晶界上的偏聚现象。     

SAPO-34/SiO_2催化甲醇制烯烃

采用水热法合成了SAPO-34分子筛,并用X射线粉末衍射仪和扫描电子显微镜对SAPO-34分子筛的结构进行了表征,同时探讨了黏合剂种类、甲醇分压、催化剂粒径和硅源等对SAPO-34分子筛催化甲醇制烯烃(MTO)反应性能的影响。实验结果表明,在MTO反应中,三烯(乙烯、丙烯和丁烯)选择性在反应初期存在明显的诱导期;以S iO2为黏合剂合成的SAPO-34/S iO2催化剂不但可缩短MTO反应的诱导期,三烯选择性也较未添加黏合剂或以A l2O3为黏合剂时高1~2个百分点;且当催化剂活性明显下降时,三烯选择性下降的幅度较小。催化剂粒径、甲醇分压及硅源对催化剂的诱导期也有明显的作用。在甲醇分压低于19kPa、催化剂粒径0.25~0.38mm、S iO2为黏合剂、硅酸四乙酯为硅源时,SAPO-34/S iO2催化剂的MTO性能明显提高。     

Modeling lossy anisotropic dielectric waveguides with the method oflines

This paper presents a new formulation useful for modeling waveguides constructed from lossy inhomogeneous anisotropic media. Our approach is based on a pair of Sturm-Liouville type wave equations that have been derived to handle inhomogeneous, diagonalized complex permittivity and permeability tensors. The method of lines is then applied to these wave equations, and related field equations, creating an indirect eigenvalue problem that correctly models this class of structure. Some refinements to the method of lines are also proposed, particularly, regarding the construction of the modal matrices found in the eigenvalue problem. Using our approach, modal dispersion curves have been computed for millimeter-wave and optical structures. Comparisons made with results available from the literature validate our approach