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排序方式: 共有484条查询结果,搜索用时 15 毫秒
11.
Takashi Kanno Changmin Kim Daisuke Yamanaka Ken-ichi Ishibashi Hiroshi Tanaka Naohito Ohno Yoshiyuki Adachi 《International journal of molecular sciences》2021,22(4)
Because Japanese cedar pollen (JCP) contains beta-1,3-d-glucan (BG), there is concern that its lingering presence in the atmosphere, especially during its scattering period, may cause false positives in the factor-G-based Limulus amebocyte lysate (LAL) assay used to test for deep mycosis (i.e., G-test). Hence, we examined whether the LAL assay would react positively with substances contained in JCP by using the G-test to measure JCP particles and extracts. BG was purified from the JCP extract on a BG-specific affinity column, and the percentage extractability was measured using three different BG-specific quantitative methods. The G-test detected 0.4 pg BG in a single JCP particle and 10 fg from a single particle in the extract. The percentage extractability of JCP-derived BG was not significantly different among the three quantitative methods. As the JCP particles should technically have been removed during serum separation, they should be less likely to be a direct false-positive factor. However, given that the LAL-assay-positive substances in the JCP extract were not distinguishable by the three BG-specific quantitative methods, we conclude that they may cause the background to rise. Therefore, in Japan false positives arising from JCP contamination should be considered when testing patients for deep mycosis. 相似文献
12.
Masuda Takahiro Fujimitsu Kazushige Sumikawa Kosei Kajita Takahiro Tang Yongpeng Hirosawa Shoichi Takizawa Yoichi Yumoto Manabu Otagiri Yoshiharu Horita Zenji 《Metallurgical and Materials Transactions A》2021,52(9):3860-3870
Metallurgical and Materials Transactions A - This study examines strain distribution occurring in the high-pressure sliding (HPS) processing for rods of pure Al and an AZ61 alloy. The strain... 相似文献
13.
The solvothermal synthesis of highly luminescent and homogeneous Gd2O3:Eu3+ nanophosphor using diethylene glycol as medium, followed by controlled combustion with citric acid as fuel is reported. The influence of concentrations of carboxylic acid and metal cations on the structure, morphology and luminescence properties are investigated in detail. The microscopic investigations indicate the nanocrystalline nature and the strong influence of cation concentration on the size, shape and agglomeration of the particles. It is found that increase in concentration of metal cations lead to the reduction in agglomeration of nanophosphors. The large value of intensity parameter Ω2, suggested that Eu3+ ions reside in a more asymmetric environment, resulted in intense emission due to 5D0–7F2 electric dipole transition. Emission decay analysis of the samples exhibited one exponential nature. The samples prepared under optimum conditions showed a quantum efficiency of 78.63% and a moderately high life time of 1.217 ms. 相似文献
14.
This paper demonstrates two simple ways to increase 5-hydroxymethylfurfural (HMF) yield (selectivity) in fructose dehydration with various solid acid catalysts. One is a water removal from the reaction mixture by a mild evacuation at 0.97 × 105 Pa; it increases HMF yield for various catalysts (heteropoly acid, zeolite, and acidic resin). The removal of water suppresses two undesired reactions: the hydrolysis of HMF to levulinic acid and the reaction of partially dehydrated intermediates to condensation products. The other method is a decrease in the particle (bead) size of the resin (Amberlyst-15). The crushed and sieved Amberlyst-15 powder in a size of 0.15–0.053 mm shows 100% HMF yield at high fructose concentration (50 wt.% in DMSO), which is to our knowledge the highest yield to date. Near-infrared spectroscopic characterization of adsorbed water suggests that the enhanced yield can be caused by an improved removal of adsorbed water in a small-size resin particle. 相似文献
15.
Kentaro Yanagihara Jumpei Taketsugu Kiyoshi Fukui Shigeru Fukunaga Shinsuke Hara Ken-ichi Kitayama 《Wireless Personal Communications》2007,40(3):401-415
In this paper, we propose a new energy efficient clustering scheme with transmission power control named “EACLE” (Energy-Aware
CLustering scheme with transmission power control for sEnsor networks) for wireless sensor networks, which are composed of
the following three components; “EACLE clustering” is a distributed clustering method by means of transmission power control,
“EACLE routing” builds a tree rooted at a sink node and sets the paths from sensor nodes taking energy saving into consideration,
and “EACLE transmission timing control” changes the transmission timing with different levels of transmission power to avoid
packet collisions and facilitates packet binding.
With an indoor wireless channel model which we obtained from channel measurement campaigns in rooms and corridors and an energy
consumption model which we obtained from a measurement of a chipset, we performed computer simulations to investigate the
performance of EACLE in a realistic environment. Our simulation results indicate that EACLE outperforms a conventional scheme
such as EAD (Energy-Aware Data-centric routing) in terms of communication success rate and energy consumption. Furthermore,
we fully discuss the impact of transmission power and timing control on the performance of EACLE. 相似文献
16.
6-(2-Cyanoethylamino)-6-deoxycellulose (Cell-CEA) as a novel cellulose derivative was prepared from 6-bromo-6-deoxycellulose. The influence of the reaction conditions on the degree of substitution was studied in detail. The dielectric characteristics of a Cell-CEA sample having degree of substitution of 0.86, together with those of microcrystalline and regenerated celluloses, have been investigated in the temperature range from −60 to 120°C, and frequency range 30 Hz to 100kHz. One relaxation process, designated as β, was recognised, which was attributed to side-group motions, probably −CH2X (X = OH or NHCH2CH2CN). The higher activation energy of this process and the shift to higher temperature in Cell-CEA, compared with microcrystalline and regenerated celluloses, reflects the enhanced steric constraints involved in the motion of the bulkier, −CH2NHCH2CH2CN, side groups. The results obtained are discussed in terms of the dielectric parameters ϵ″max′ β and Δϵ. 相似文献
17.
18.
The effect of NH4F addition on the high-anodic behaviors of various DSA-type electrodes was investigated in a mixture of sulfuric acid and ammonium sulfate. The pronounced effect of NH4 addition was observed on DSA-type Ti/RuO2, Ti/IrO2?TiO2 electrodes, but not observed on the other electrodes studied. The close relationship was found between the increment of the electrode potential caused by the NH4 addition and the quantity of F? adsorbed on the electrode surface. The effect of NH4F addition was considered to be resulted from the adsorption of F? on the electrode surface, and the presence of adsorbed F? was directly proved. 相似文献
19.
Maki Itoh Toshimitsu Suzuki Yoshihiko Tsujimoto Ken-ichi Yoshii Yoshinobu Takegami Yoshihisa Watanabe 《Fuel》1983,62(1):98-102
Thermal cracking of tar-sand bitumens has been carried out using a two-stage pyrolysis reactor with temperature zones of 440°C and 750–800°C, respectively. Feedstocks were pyrolysed in the first stage into cracked oils, which were carried to the second stage for subsequent pyrolysis. Only 12–14 wt% of ethylene was obtained from tar-sand bitumens at the residence time of 1.2 s in the second stage, although 27 and 16 wt% were obtained from Taching and Iranian heavy vacuum residues, respectively. The tar-sand bitumens contain shorter paraffinic straight-chains and have more branched molecules than the vacuum residues of petroleum. A straight-chain paraffin index is proposed, with which a good correlation was obtained between ethylene yield and the fraction of straight-chain paraffin carbons in the heavy oil. 相似文献
20.
Akio Kishi Seiji Kuroda Tadanobu Inoue Takeshi Fukushima Hisami Yumoto 《Journal of Thermal Spray Technology》2008,17(2):228-233
A new testing procedure to evaluate the interfacial toughness of thermal-sprayed coatings has been developed. The newly designed
test specimen is a modification of the pin test with an artificially introduced weak interface, which is expected to open
up easily under tensile loading and act as a circumferential precrack along the interface between a coating and the substrate.
This configuration makes it possible to calculate the stress intensity factor K
Int at the tip of the precrack, which can be expressed as
, where σ0 is the apparent average stress, a the crack length, R the specimen radius, and F
I the geometrical correction function. Finite-element analysis was carried out to calculate the correction function F
I for various values of a/R. In the experiments, the flat surface of a pin was grit-blasted and a ring-shaped area from the periphery was covered with
carbon using a pencil and set into a mating dice. SUS316L stainless steel was plasma-sprayed onto the flat surface of the
pin and the dice. Then, tensile load was applied to the pin to break the weak interface containing the carbon and finally
the unmodified coating-substrate interface. The load required to pull out the pin was measured for various specimen parameters
such as a and R. The results indicate that the adhesion of the tested coatings can be represented by interface toughness of 1.9 ± 0.1 MPa m1/2. As a consequence, this testing procedure can be considered as a viable method to evaluate adhesion of a thermal-sprayed
coating on a substrate. 相似文献