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991.
992.
Huaying Ren Huan Wang Li Lin Miao Tang Shuli Zhao Bing Deng Manish Kumar Priydarshi Jincan Zhang Hailin Peng Zhongfan Liu 《Nano Research》2017,10(4):1189-1199
In the chemical vapor deposition growth of large-area graphene polycrystalline thin films,the coalescence of randomly oriented graphene domains results in a high density of uncertain grain boundaries (GBs).The structures and properties of various GBs are highly dependent on the misorientation angles between the graphene domains,which can significantly affect the performance of the graphene films and impede their industrial applications.Graphene bicrystals with a specific type of GB can be synthesized via the controllable growth of graphene domains with a predefined lattice orientation.Although the bicrystal has been widely investigated for traditional bulk materials,no successful synthesis strategy has been presented for growing two-dimensional graphene bicrystals.In this study, we demonstrate a simple approach for growing well-aligned large-domain graphene bicrystals with a confined tilt angle of 30° on a facilely recrystallized single-crystal Cu (100) substrate.Control of the density of the GBs with a misorientation angle of 30° was realized via the controllable rapid growth of subcentimeter graphene domains with the assistance of a cooperative catalytic surface-passivation treatment.The large-area production of graphene bicrystals consisting of the sole specific GBs with a tunable density provides a new material platform for fundamental studies and practical applications. 相似文献
993.
A series of nanocomposite LiFe(1-2x)ZrxPO4/C (x = 0.01,0.02, 0.03, 0.04, 0.06) were prepared by carbon thermal reduction method. With this strategy, the Li3PO4 impurity phase can be obviously reduced in the Zr-doped samples and the electrochemical performance is obviously improved by Zr doping compared with the undoped one. The best electrochemical performances were observed in LiFe(0.92)Zr(0.04)PO4/C as well as good cycle stability. 相似文献
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Shi‐Yang Tang Ruirui Qiao Sheng Yan Dan Yuan Qianbin Zhao Guolin Yun Thomas P. Davis Weihua Li 《Small (Weinheim an der Bergstrasse, Germany)》2018,14(21)
Functional nanoparticles comprised of liquid metals, such as eutectic gallium indium (EGaIn) and Galinstan, present exciting opportunities in the fields of flexible electronics, sensors, catalysts, and drug delivery systems. Methods used currently for producing liquid metal nanoparticles have significant disadvantages as they rely on both bulky and expensive high‐power sonication probe systems, and also generally require the use of small molecules bearing thiol groups to stabilize the nanoparticles. Herein, an innovative microfluidics‐enabled platform is described as an inexpensive, easily accessible method for the on‐chip mass production of EGaIn nanoparticles with tunable size distributions in an aqueous medium. A novel nanoparticle‐stabilization approach is reported using brushed polyethylene glycol chains with trithiocarbonate end‐groups negating the requirements for thiol additives while imparting a “stealth” surface layer. Furthermore, a surface modification of the nanoparticles is demonstrated using galvanic replacement and conjugation with antibodies. It is envisioned that the demonstrated microfluidic technique can be used as an economic and versatile platform for the rapid production of liquid metal‐based nanoparticles for a range of biomedical applications. 相似文献
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采用适射电子显微镜对五种Fc—C—N合金的板条马氏体的束内和束界区进行详细的观察和分析。研究发现板条马氏体组织中存在填塞马氏体。板条马氏体组织是由一簇簇平行排列的大小板条,以及填充在马氏体板条间,束界和界隅内的不定外形的填塞马氏体和条间残余奥氏体薄膜或膜片所构成。 相似文献
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本文采用气体蒸发法制备出粒度不到5nm的Sn及其氧化物的超微粉。利用热重,差热分析和X射线衍射谱等测试方法研究了热处理制度对其粒度,成份和气敏特性的影响,发现了SnO_2正交相的存在。 相似文献