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81.
Kunal Kumar Olaf Stefanczyk Koji Nakabayashi Yuuki Mineo Shin-ichi Ohkoshi 《International journal of molecular sciences》2022,23(11)
Molecular vibrations in the solid-state, detectable in the terahertz (THz) region, are the subject of research to further develop THz technologies. To observe such vibrations in terahertz time-domain spectroscopy (THz-TDS) and low-frequency (LF) Raman spectroscopy, two supramolecular assemblies with the formula [NdIII (phen)3 (NCX)3] 0.3EtOH (X = S, 1-S; Se, 1-Se) were designed and prepared. Both compounds show several THz-TDS and LF-Raman peaks in the sub-THz range, with the lowest frequencies of 0.65 and 0.59 THz for 1-S and 1-Se, and 0.75 and 0.61 THz for 1-S and 1-Se, respectively. The peak redshift was observed due to the substitution of SCN− by SeCN−. Additionally, temperature-dependent TDS-THz studies showed a thermal blueshift phenomenon, as the peak position shifted to 0.68 THz for 1-S and 0.62 THz for 1-Se at 10 K. Based on ab initio calculations, sub-THz vibrations were ascribed to the swaying of the three thiocyanate/selenocyanate. Moreover, both samples exhibited near-infrared (NIR) emission from Nd (III), and very good thermometric properties in the 300–150 K range, comparable to neodymium (III) oxide-based thermometers and higher than previously reported complexes. Moreover, the temperature dependence of fluorescence and THz spectroscopy analysis showed that the reduction in anharmonic thermal vibrations leads to a significant increase in the intensity and a reduction in the width of the emission and LF absorption peaks. These studies provide the basis for developing new routes to adjust the LF vibrational absorption. 相似文献
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Yuta Uenoyama Atsushi Matsuda Kazune Ohashi Koji Ueda Misaki Yokoyama Takuya Kyoutou Kouji Kishi Youichi Takahama Masaaki Nagai Takaaki Ohbayashi Osamu Hotta Hideki Matsuzaki 《International journal of molecular sciences》2022,23(9)
Aberrant glycosylation of IgA1 is involved in the development of IgA nephropathy (IgAN). There are many reports of IgAN markers focusing on the glycoform of IgA1. None have been clinically applied as a routine test. In this study, we established an automated sandwich immunoassay system for detecting aberrant glycosylated IgA1, using Wisteria floribunda agglutinin (WFA) and anti-IgA1 monoclonal antibody. The diagnostic performance as an IgAN marker was evaluated. The usefulness of WFA for immunoassays was investigated by lectin microarray. A reliable standard for quantitative immunoassay measurements was designed by modifying a purified IgA1 substrate. A validation study using multiple serum specimens was performed using the established WFA-antibody sandwich automated immunoassay. Lectin microarray results showed that WFA specifically recognized N-glycans of agglutinated IgA1 in IgAN patients. The constructed IgA1 standard exhibited a wide dynamic range and high reactivity. In the validation study, serum WFA-reactive IgA1 (WFA+-IgA1) differed significantly between healthy control subjects and IgAN patients. The findings indicate that WFA is a suitable lectin that specifically targets abnormal agglutinated IgA1 in serum. We also describe an automated immunoassay system for detecting WFA+-IgA1, focusing on N-glycans. 相似文献
84.
Takayoshi Yokoya Rikiya Yoshida Yuki Utsumi Koji Tsubota Hiroyuki Okazaki Takanori Wakita Yoshikazu Mizuguchi Yoshihiko Takano Takayuki Muro Yukako Kato Hiroshi Kumigashira Masaharu Oshima Hisatomo Harima Yoshihiro Aiura Hitoshi Sato Akihiro Ino Hirofumi Namatame Masaki Taniguchi Masaaki Hirai Yuji Muraoka 《Science and Technology of Advanced Materials》2012,13(5)
We have characterized the electronic structure of FeSe1−xTex for various x values using soft x-ray photoemission spectroscopy (SXPES), high-resolution photoemission spectroscopy (HRPES) and inverse photoemission spectroscopy (IPES). The SXPES valence band spectral shape shows that the 2 eV feature in FeSe, which was ascribed to the lower Hubbard band in previous theoretical studies, becomes less prominent with increasing x. HRPES exhibits systematic x dependence of the structure near the Fermi level (EF): its splitting near EF and filling of the pseudogap in FeSe. IPES shows two features, near EF and approximately 6 eV above EF; the former may be related to the Fe 3d states hybridized with chalcogenide p states, while the latter may consist of plane-wave-like and Se d components. In the incident electron energy dependence of IPES, the density of states near EF for FeSe and FeTe has the Fano lineshape characteristic of resonant behavior. These compounds exhibit different resonance profiles, which may reflect the differences in their electronic structures. By combining the PES and IPES data the on-site Coulomb energy was estimated at 3.5 eV for FeSe. 相似文献
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Modeling of Nonlinear Magnetizing Characteristics of Pole Transformer for Analyzing Islanding Prevention of Photovoltaic System
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Yoshiaki Yoshida Hirokazu Suzuki Koji Fujiwara Yoshiyuki Ishihara 《Electrical Engineering in Japan》2014,188(3):46-55
With increasing penetration of distributed generators such as photovoltaic (PV) systems in distribution systems, it is very important to quickly detect islanding caused by power system faults in order to assure electrical safety. We have developed a nonlinear magnetizing characteristics model of pole transformers for use in analyzing islanding prevention in PV systems. Basic experiments on the islanding detection were performed for verification of the proposed model. Analytical results obtained by the proposed model agreed well with experimental results. 相似文献
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