Experimental dynamic characterizations and modelling of disk vibrations for HDDs

Currently, the rotational speed of spindle motors in HDDs (Hard-Disk Drives) are increasing to improve high data throughput and decrease rotational latency for ultra-high data transfer rates. However, the disk platters are excited to vibrate at their natural frequencies due to higher air-flow excitation as well as eccentricities and imbalances in the disk-spindle assembly. These factors contribute directly to TMR (Track Mis-Registration) which limits achievable high recording density essential for future mobile HDDs. In this paper, the natural mode shapes of an annular disk mounted on a spindle motor used in current HDDs are characterized using FEM (Finite Element Methods) analysis and verified with SLDV (Scanning Laser Doppler Vibrometer) measurements. The identified vibration frequencies and amplitudes of the disk ODS (Operating Deflection Shapes) at corresponding disk mode shapes are modelled as repeatable disturbance components for servo compensation in HDDs. Our experimental results show that the SLDV measurements are accurate in capturing static disk mode shapes without the need for intricate air-flow aero-elastic models, and the proposed disk ODS vibration model correlates well with experimental measurements from a LDV.     

A Method for Received Waveform Reconstruction Based on Bender Element Test Using Frequency-swept Signal

An experimental technique for reconstructing the received wave of bender element tests based on linear system theory is shown in this paper. In order to identify the frequency response of testing apparatus, bender element tests using frequency-swept signals are performed. Received waves for one-period sine pulse transmitting with various frequencies are calculated and compared with observed waves in several kinds of soil samples and testing apparatuses. The linearity of the testing system is also confirmed by coherence function. It is shown that calculated data are less affected by random noise and show good agreement with observed data in regards to not only waveform itself but also resulting shear wave velocity. It is mentioned that this technique can provide simulations for arbitrary transmitted waveform with high signal/noise ratio after laboratory tests are performed. It is also mentioned that this technique is advantageous when sufficient amplitude of received wave cannot be ensured or shear wave velocity must be verified, for example, due to uncertainty of arrival time by near-field effect.     

Geometry dependence of microstructure and microhardness for selective electron beam-melted Ti–6Al–4V parts

In an additive-manufactured metallic part, distinct and different microstructure and mechanical properties may exist in different areas due to differences in shape and location. Two parts, one with straight-finned structure and the other with curve-finned structure, were fabricated by the selective electron beam melting method using pre-alloyed Ti–6Al–4V ELI powder. Microstructural characterisation of these two parts that have varying fin thickness and shape was carried out to investigate the synthetical influence of 2D planar build geometry and in-fill hatching strategy on selective electron beam melting. It was found that the β interspacing is larger in the curve-finned structure, leading to a lower microhardness as compared to the straight-finned structure. It suggests a slower cooling rate in the curve-finned structure due to the differences in build geometry and in-fill hatching strategy.     

Synthesis,Characterisation, and Evaluation of a Cross-Linked Disulphide Amide-Anhydride-Containing Polymer Based on Cysteine for Colonic Drug Delivery

The use of disulphide polymers, a low redox potential responsive delivery, is one strategy for targeting drugs to the colon so that they are specifically released there. The objective of this study was to synthesise a new cross-linked disulphide-containing polymer based on the amino acid cysteine as a colon drug delivery system and to evaluate the efficiency of the polymers for colon targeted drug delivery under the condition of a low redox potential. The disulphide cross-linked polymers were synthesised via air oxidation of 1,2-ethanedithiol and 3-mercapto-N-2-(3-mercaptopropionamide)-3-mercapto propionic anhydride (trithiol monomers) using different ratio combinations. Four types of polymers were synthesised: P10, P11, P151, and P15. All compounds synthesised were characterised by NMR, IR, LC-MS, CHNS analysis, Raman spectrometry, SEM-EDX, and elemental mapping. The synthesised polymers were evaluated in chemical reduction studies that were performed in zinc/acetic acid solution. The suitability of each polymer for use in colon-targeted drug delivery was investigated in vitro using simulated conditions. Chemical reduction studies showed that all polymers were reduced after 0.5–1.0 h, but different polymers had different thiol concentrations. The bacterial degradation studies showed that the polymers were biodegraded in the anaerobic colonic bacterial medium. Degradation was most pronounced for polymer P15. This result complements the general consensus that biodegradability depends on the swellability of polymers in an aqueous environment. Overall, these results suggest that the cross-linked disulphide-containing polymers described herein could be used as coatings for drugs delivered to the colon.     

Machining and Ceramic/Ceramic Joining to Form Internal Mesoscale Channels

Ceramics and semiconducting materials with internal channels are crucial in a variety of diverse technologies such as "lab on a chip," fuel cell applications, and cooling of microelectronics. In this paper, techniques for fabricating internal channels in brittle materials first are reviewed. Then, the mechanical machining of surface channels in 99.99% pure alumina partially sintered at 600°C and 700°C is discussed. After machining, the partially sintered alumina is sintered to a density of about 97% of theoretical and then joined to 96% pure alumina to convert the surface channels into internal channels.     

Prospects of non-catalytic supercritical methyl acetate process in biodiesel production

Conventional biodiesel production methods utilize alcohol as acyl acceptor and produces glycerol as side product. Hence, with escalating production of biodiesel throughout the world, it leads to oversupply of glycerol and subsequently causes devaluation in the market. In this study, methyl acetate was employed as acyl acceptor in non-catalytic supercritical methyl acetate (SCMA) process to produce fatty acid methyl esters (FAME) and side product of triacetin, a valuable fuel additive instead of glycerol. Consequently, the properties of biodiesel produced (FAME and triacetin) are superior compared to conventional biodiesel method (FAME only). In this research, the effects of reaction temperature, reaction time and molar ratio of methyl acetate to oil on the yield of biodiesel were investigated. Apart from that, the influence of impurities commonly found in waste oils/fats such as free fatty acids and water were studied as well and compared with methanol-based reactions of supercritical and heterogeneous catalysis. Results show that biodiesel yields in SCMA process could achieve 99 wt.% when the operating conditions were fixed at 400 °C/220 bar for reaction temperature, methyl acetate/oil molar ratio of 30:1 and 60 min of reaction time. Furthermore, SCMA did not suffer from adverse effect with the presence of impurities, proving that SCMA has a high tolerance towards contamination which is crucial to allow the utilization of inexpensive waste oils/fats as biodiesel feedstock.     

Zero-quantised discrete cosine transform prediction technique for video encoding

A new analytical model to eliminate redundant discrete cosine transform (DCT) and quantisation (Q) computations in block-based video encoders is proposed. The dynamic ranges of the quantised DCT coefficients are analysed, then a threshold scheme is derived to determine whether the DCT and Q computations can be skipped without video quality degradation. In addition, fast DCT/inverse DCT (IDCT) algorithms are presented to implement the proposed analytical model. The proposed analytical model is compared with other comparable analytical models reported in the literature. Both the theoretical analysis and experimental results demonstrate that the proposed analytical model can greatly reduce the computational complexity of video encoding without any performance degradation and outperforms other analytical models     

Performance enhancement in organic photovoltaic devices using plasma-polymerized fluorocarbon-modified Ag nanoparticles

In this work, Ag nanoparticles were modified by an ultra-thin plasma-polymerized fluorocarbon film (CF_X) to form a composite CF_X-modified Ag nanoparticles/indium tin oxide (ITO) anode for application in organic photovoltaic (OPV) devices. A CF_X-modified Ag nanoparticles/ITO anode exhibited a superior surface work function of 5.4 eV suited for application in OPV devices. The performance of zinc phthalocyanine:fullerene-based OPV devices showed a significant improvement when the structural identical cells are made with the CF_X-modified Ag nanoparticles/ITO. This work yielded a promising power conversion efficiency of 3.5 ± 0.1%, notably higher than that with a bare ITO anode (2.7 ± 0.1%).