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11.
12.
A series of binary blends of poly(ethylene oxide) (PEO), poly(propylene oxide) (PPO), and polytetrahydrofuran (PTHF), characterized by similar average molecular weights, with selected fatty acids (capric acid, lauric acid, myristic acid, palmitic acid, and stearic acid) were prepared by melt mixing. Differential scanning calorimetry was applied to characterize the phase transitions of melting and crystallization, and a synergistic effect was found to occur for PEO/fatty acid blends, as evidenced by the values of the enthalpy of the phase transition. This effect was probably due to hydrogen bonding between PEO and the fatty (carboxylic) acids, which facilitated the formation of crystalline structures; an analysis of IR spectroscopy data showed a shift in the absorption bands of OH groups. The morphology development of the PEO/carboxylic acid blends, as observed with polarizing light microscopy, could be described as spherulitic growth with spontaneous selection of the lamellar thickness. The textures of the individual fibrils, consisting of stacks of several tens of lamellae corresponding to PPO and PTHF, were less regular than the texture of PEO and showed large macroscopic heterogeneity. © 2003 Wiley Periodicals, Inc. J Appl Polym Sci 90: 861–870, 2003 相似文献
13.
Krzysztof Kaczmarski Dongmei Zhou Georges Guiochon 《Chemical engineering science》2003,58(11):2325-2338
The adsorption isotherm data of R- and S-1-indanol and of their racemic mixture on cellulose tribenzoate were measured by frontal analysis. These experimental data were fitted to the single-component and the modified competitive Bilangmuir isotherms. The overloaded elution profiles of bands of the pure enantiomers and of the racemic mixture were calculated for different sample sizes, using the best competitive isotherm model and the General Rate Model of chromatography coupled with the generalized Maxwell-Stefan equation that describes the surface diffusion flux. The calculated and the experimental profiles were found to be in excellent agreement in all cases. The parameters of the model of the mass transfer kinetics were derived from the band profiles obtained for the pure enantiomers. The same values of these parameters give an excellent prediction of the profiles of multicomponent bands. The new model described here allows a satisfactory interpretation of the competitive mass transfer kinetics. 相似文献
14.
Rajmund S. Dybczyński Marta Pyszynska Krzysztof Kulisa Anna Bojanowska-Czajka 《分离科学与技术》2020,55(7):1364-1379
ABSTRACTNew ion interaction chromatographic (IIC) method employing Kromasil 100 C18 column and tetra-n-butylammonium hydroxide (TBAOH) as an ion interaction reagent (IIR) is able to separate yttrium from Rare Earth Elements (REE) as anionic complexes with nitrilotriacetic acid (NTA). New method for the chromatographic determination of Y in REE mixture was devised and validated by the analysis of the certified reference material (CRM). Potential possibilities of the new chromatographic system for larger scale applications including macro-micro events were demonstrated. 相似文献
15.
In this paper, basic relationships and algorithms for numerical simulation of non-linear, self-excited vibrations in single degree-of-freedom cutting systems are presented. Non-linearities due to the tool leaving the cut, as well as interference between the cutting tool clearance face and cutting surface waviness, were taken into consideration. Examples of vibration simulation results are shown. 相似文献
16.
Krzysztof Michalak 《Optimization methods & software》2016,31(2):392-404
Evolutionary algorithms (EAs) are often employed to multiobjective optimization, because they process an entire population of solutions which can be used as an approximation of the Pareto front of the tackled problem. It is a common practice to couple local search with evolutionary algorithms, especially in the context of combinatorial optimization. In this paper a new local search method is proposed that utilizes the knowledge concerning promising search directions. The proposed method can be used as a general framework and combined with many methods of iterating over a neighbourhood of an initial solution as well as various decomposition approaches. In the experiments the proposed local search method was used with an EA and tested on 2-, 3- and 4-objective versions of two well-known combinatorial optimization problems: the travelling salesman problem (TSP) and the quadratic assignment problem (QAP). For comparison two well-known local search methods, one based on Pareto dominance and the other based on decomposition, were used with the same EA. The results show that the EA coupled with the directional local search yields better results than the same EA coupled with any of the two reference methods on both the TSP and QAP problems. 相似文献
17.
Mobile context-based framework for threat monitoring in urban environment with social threat monitor
Szymon Bobek Grzegorz J. Nalepa Antoni Ligȩza Weronika T. Adrian Krzysztof Kaczor 《Multimedia Tools and Applications》2016,75(17):10595-10616
Engaging users in threat reporting is important in order to improve threat monitoring in urban environments. Today, mobile applications are mostly used to provide basic reporting interfaces. With a rapid evolution of mobile devices, the idea of context awareness has gained a remarkable popularity in recent years. Modern smartphones and tablets are equipped with a variety of sensors including accelerometers, gyroscopes, pressure gauges, light and GPS sensors. Additionally, the devices become computationally powerful which allows for real-time processing of data gathered by their sensors. Universal access to the Internet via WiFi hot-spots and GSM network makes mobile devices perfect platforms for ubiquitous computing. Although there exist numerous frameworks for context-aware systems, they are usually dedicated to static, centralized, client-server architectures. There is still space for research in the field of context modeling and reasoning for mobile devices. In this paper, we propose a lightweight context-aware framework for mobile devices that uses data gathered by mobile device sensors and performs on-line reasoning about possible threats based on the information provided by the Social Threat Monitor system developed in the INDECT project. 相似文献
18.
19.
Krzysztof Kozłowski Przemysław Herman 《Journal of Intelligent and Robotic Systems》2008,53(3):205-221
In this paper we present new control algorithms for robots with dynamics described in terms of quasi-velocities (Kozłowski,
Identification of articulated body inertias and decoupled control of robots in terms of quasi-coordinates. In: Proc. of the
1996 IEEE International Conference on Robotics and Automation, pp. 317–322. IEEE, Piscataway, 1996a; Zeitschrift für Angewandte Mathematik und Mechanik 76(S3):479–480, 1996c; Robot control algorithms in terms of quasi-coordinates. In: Proc. of the 34 Conference on Decision and Control, pp. 3020–3025,
Kobe, 11–13 December 1996, 1996d). The equations of motion are written using spatial quantities such as spatial velocities, accelerations, forces, and articulated
body inertia matrices (Kozłowski, Standard and diagonalized Lagrangian dynamics: a comparison. In: Proc. of the 1995 IEEE
Int. Conf. on Robotics and Automation, pp. 2823–2828. IEEE, Piscataway, 1995b; Rodriguez and Kreutz, Recursive Mass Matrix Factorization and Inversion, An Operator Approach to Open- and Closed-Chain
Multibody Dynamics, pp. 88–11. JPL, Dartmouth, 1998). The forward dynamics algorithms incorporate new control laws in terms of normalized quasi-velocities. Two cases are considered:
end point trajectory tracking and trajectory tracking algorithm, in general. It is shown that by properly choosing the Lyapunov
function candidate a dynamic system with appropriate feedback can be made asymptotically stable and follows the desired trajectory
in the task space. All of the control laws have a new architecture in the sense that they are derived, in the so-called quasi-velocity
and quasi-force space, and at any instant of time generalized positions and forces can be recovered from order recursions, where denotes the number of degrees of freedom of the manipulator. This paper also contains the proposition of a sliding mode control,
originally introduced by Slotine and Li (Int J Rob Res 6(3):49–59, 1987), which has been extended to the sliding mode control in the quasi-velocity and quasi-force space. Experimental results illustrate
behavior of the new control schemes and show the potential of the approach in the quasi-velocity and quasi-force space.
Authors are with Chair of Control and Systems Engineering. 相似文献
20.
In this paper we consider robust stabilization of the class of nonlinear plants of the form $$\dot x = f(x) + \sum\limits_{i = 1}^m {g_i } (x)u_i (t),$$ which are equivalent, under smooth state space coordinate transformations and nonlinear state feedback, to controllable systems. This approach is very sensitive for unknown parameters' values. Parameter adaptation may be used as a technique to robustify minimum-phase systems [3]. We give an example of a locally stable adaptive tracking system in which the last assumption is weakened. The minimum-phase plant considered in the paper is a current-controlled squirrel cage induction motor. 相似文献