高沸点溶剂法合成原乙酸三甲酯

对低沸点溶剂法制备原乙酸三甲酯工艺进行了改进，比较了煤油、2-乙基己醇、氯苯、异佛尔酮、邻苯二甲酸二丁酯、乙二醇二丁醚等高沸点溶剂对反应的影响，筛选出最优高沸点溶剂煤油：研究了新反应体系的醇解pH值、溶剂的循环使用次数对反应的影响及溶剂循环损耗率，结果表明，醇解的最佳pH值为5．6；随着溶剂循环次数增加，原乙酸三甲酯收率从83．6％(1次)逐渐下降到76．7％(16次)；溶剂次平均损耗率4．6％。实现了直接蒸馏产品，溶剂循环使用的新工艺。避免了旧工艺先蒸溶剂，后蒸产品，产品大量分解，收率低等缺点。     

An ergonomics study of thumb movements on smartphone touch screen

This study investigated the relationships between thumb muscle activity and thumb operating tasks on a smartphone touch screen with one-hand posture. Six muscles in the right thumb and forearm were targeted in this study, namely adductor pollicis, flexor pollicis brevis, abductor pollicis brevis (APB), abductor pollicis longus, first dorsal interosseous (FDI) and extensor digitorum. The performance measures showed that the thumb developed fatigue rapidly when tapping on smaller buttons (diameter: 9 mm compared with 3 mm), and moved more slowly in flexion–extension than in adduction–abduction orientation. Meanwhile, the electromyography and perceived exertion values of FDI significantly increased in small button and flexion–extension tasks, while those of APB were greater in the adduction–abduction task. This study reveals that muscle effort among thumb muscles on a touch screen smartphone varies according to the task, and suggests that the use of small touch buttons should be minimised for better thumb performance.     

基于环状电极的电容式润滑油磨粒检测系统设计

摩擦副非正常磨损时将产生直径为几十微米的大金属磨粒。采用阻抗类方法检测磨粒时,要求传感器具有较高的灵敏度。为此,设计了差分结构的环状极板电容式传感器。应用电容/数字转换芯片AD7746将传感器的输出直接转换为数字信号,省去了前端复杂的信号调理电路,简化了设计,并且有效地降低了寄生电容和杂散电容的影响。实验表明:系统分辨率可以达到0.125 fF,极大提高了系统灵敏度。     

Communicating Is Crowdsourcing: Wi-Fi Indoor Localization with CSI-Based Speed Estimation

Numerous indoor localization techniques have been proposed recently to meet the intensive demand for location-based service (LBS). Among them, the most popular solutions are the Wi-Fi fingerprint-based approaches. The core challenge is to lower the cost of fingerprint site-survey. One of the trends is to collect the piecewise data from clients and establish the radio map in crowdsourcing manner. However the low participation rate blocks the practical use. In this work, we propose a passive crowdsourcing channel state information (CSI) based indoor localization scheme, C²IL. Despite a crowdsourcing based approach, our scheme is totally transparent to the client and the only requirement is to connect to our 802.11n access points (APs). C²IL is built upon an innovative method to accurately estimate the moving speed solely based on 802.11n CSI. Knowing the walking speed of a client and its surrounding APs, a graph matching algorithm is employed to extract the received signal strength (RSS) fingerprints and establish the fingerprint map. For localization phase, we design a trajectory clustering based localization algorithm to provide precise real-time indoor localization and tracking. We develop and deploy a practical working system of C²IL in a large office environment. Extensive evaluations indicate that the error of speed estimation is within 3%, and the localization error is within 2 m at 80% time in a very complex indoor environment.     

异构数据库数据迁移的研究与实现

数据是业务运转的基础．是企业的宝贵资产。企业在系统升级过程中往往会遇到数据迁移问题,由于新系统与旧系统经常存在数据结构异构的情况．使数据迁移工作难以实现。开发一款异构数据库数据迁移工具,该工具通过框架程序在ODBC（Open Database Connectivity）开发平台以及XML技术的支持下实现数据结构异构的数据库数据迁移。     

3D Shape Segmentation and Labeling via Extreme Learning Machine

We propose a fast method for 3D shape segmentation and labeling via Extreme Learning Machine (ELM). Given a set of example shapes with labeled segmentation, we train an ELM classifier and use it to produce initial segmentation for test shapes. Based on the initial segmentation, we compute the final smooth segmentation through a graph‐cut optimization constrained by the super‐face boundaries obtained by over‐segmentation and the active contours computed from ELM segmentation. Experimental results show that our method achieves comparable results against the state‐of‐the‐arts, but reduces the training time by approximately two orders of magnitude, both for face‐level and super‐face‐level, making it scale well for large datasets. Based on such notable improvement, we demonstrate the application of our method for fast online sequential learning for 3D shape segmentation at face level, as well as realtime sequential learning at super‐face level.     

Automatic 3D Indoor Scene Updating with RGBD Cameras

Since indoor scenes are frequently changed in daily life, such as re‐layout of furniture, the 3D reconstructions for them should be flexible and easy to update. We present an automatic 3D scene update algorithm to indoor scenes by capturing scene variation with RGBD cameras. We assume an initial scene has been reconstructed in advance in manual or other semi‐automatic way before the change, and automatically update the reconstruction according to the newly captured RGBD images of the real scene update. It starts with an automatic segmentation process without manual interaction, which benefits from accurate labeling training from the initial 3D scene. After the segmentation, objects captured by RGBD camera are extracted to form a local updated scene. We formulate an optimization problem to compare to the initial scene to locate moved objects. The moved objects are then integrated with static objects in the initial scene to generate a new 3D scene. We demonstrate the efficiency and robustness of our approach by updating the 3D scene of several real‐world scenes.     

A generalized method for correcting instrument spreading in gel permeation chromatography

A general method of chromatogram correction for skewed instrument spreading in gel permeation chromatography is presented. The correction method is so general that there is no restriction on the shape of the spreading function. It admits nonsymmetric, non-Gaussian as well as nonconvolution type. Aspects of solution techniques are discussed and an illustrative example is given to elucidate the method.     

射流流化床内流体力学行为的模拟研究

以流化床应用为代表的气固流动系统是许多化工过程中的重要组成部分 ,CFD( computational fluid dynamics)方法能够为其优化设计和放大提供所需要的信息 .本文采用双欧拉模型 ,与 Gidaspow等的实验结果进行了对比 ,模拟了二维射流流化床内气泡的形成规律 ,得到了带锥型分布器的流化床内瞬时空隙率和气固相速度分布等流体力学参数 .对锥型分布器流化床的实验结果表明 ,模拟得到的气泡的形状与实验现象相接近 .