Factors influencing magnetic polymer microspheres prepared by dispersion polymerization

Magnetic iron oxide (Fe₃O₄) was prepared by a coprecipitation method. Core–shell composite magnetic polymer microspheres with carboxyl groups were synthesized by the dispersion polymerization of styrene and acrylic acid in the presence of magnetic oxide, and dibenzoyl peroxide was used as an initiator. The synthesized magnetic polymer microspheres were characterized with X‐ray diffraction, transmission electron microscopy, scanning electron microscopy, Fourier transform infrared spectroscopy, and so forth. The results indicated that the product was single‐phase Fe₃O₄, and its average size was about 10 nm. The configuration of the microspheres, which contained carboxyl groups, was spherical, and the average size was about 2 μm. The results of vibrating sample magnetometry tests showed that the magnetic powders produced by different surfactants had different saturation magnetizations. When poly(ethylene glycol) with a weight‐average molecular weight of 4000 was used as a surfactant, the saturation magnetization of the samples reached 69.2 emu/g. The factors that affected the shape, magnetism, size, and distribution of the microspheres were also studied. © 2007 Wiley Periodicals, Inc. J Appl Polym Sci 2007     

An SVD-based adaptive robust speech steganography using MDCT coefficient

Multimedia Tools and Applications - Speech is one of the essential ways of communication. The study of speech steganography provides great value in information security. To improve imperceptibility...     

音频大地电磁测深在某隧道工程中的应用

音频大地电磁(AMT)在隧道的工程地质勘察是一种非常有效的方法,它具有不受高阻屏蔽、轻便、探测深度相对较大等优点,在宏观上可以查明隧道地层岩性分界、地质构造及其赋水性。以某隧道音频大地电磁勘察为例,分别对AMT的采集手段、工频干扰去噪、静态校正、反演方法等关键技术问题进行分析,并结合实际资料对该工作区的地层分布、断层及其破碎带的赋水情况等进行分析和解释,在其应用中取得了理想的效果。     

SiO_2/Al_2O_3 RATIO OF HYDRATED SODIUM ALUMINOSILICATE IN ALUMINA PRODUCTION

ＳｉＯ２／Ａｌ２Ｏ３ＲＡＴＩＯＯＦＨＹＤＲＡＴＥＤＳＯＤＩＵＭＡＬＵＭＩＮＯＳＩＬＩＣＡＴＥＩＮＡＬＵＭＩＮＡＰＲＯＤＵＣＴＩＯＮ①ＤｅｎｇＨｏｎｇｍｅｉ，ＺｅｎｇＷｅｎｍｉｎｇ，ＣｈｅｎＮｉａｎｙｉＳｈａｎｇｈａｉＩｎｓｔｉｔｕｔｅｏｆＭｅｔａｌｕ...     

Effects of laser beam energy and incident angle on the pulse laser welding of stainless steel thin sheet

This paper reports an experimental study of laser spot welding on stainless steel sheets. A pulsed Nd:YAG laser was used to weld the stainless steel specimen in the range of laser energy 0.6–1.2 J and incident angle 30–75° (the angle of the laser beam incident direction to the sheet surface). Metallography was applied to measure the cross-sectional size and shape of the welded spot. From the experimental results, it is found that as the laser energy increases, the penetration depth, bead length, and bead width of the welded spot increase. As the laser incident angle increases, the penetration depth and the bead width increase while the bead length decreases. The results illustrate that the shape and size of the welded spot depend not only on the laser energy, but also on the incident angle of laser beam.     

用于腺苷检测的基于级联扩增核酸适体电化学传感界面的构建研究

该文报道了一种基于酶级联扩增的电化学核酸适体检测腺苷的新方法。当腺苷存在时,滚环扩增的引物通过E.coli DNA连接酶的作用与通过巯基组装在金电极上的固定探针连接。在pHi29 DNA聚合酶的作用下,滚环扩增反应进行并产生一条与环形探针完全互补的长的单链,然后将大量金纳米粒子标记的核酸探针与滚环扩增的产物杂交。该传感界面电化学行为的结果表明,通过酶级联扩增的方法提高了检测腺苷的阻抗响应灵敏度,且选择性和重现性良好。用于腺苷的检测时,其线性范围为2.0μmol/L~100μmol/L,最低检测浓度为2.0μmol/L,表明该传感界面的设计可作为一种通用方法而有望用于其它目标物的检测。     

Parallel computation of determinants of matrices with multivariate polynomial entries

In this paper we present an extension to the work of Björck et al. for computing the determinants of matrices with univariate or bivariate polynomials as entries to multivariate case. The algorithm supports parallel computation and has been implemented on a multi-core cluster computer system. We show how to use our approach to calculate two unsolved problems, which arise from computational geometry optimization and electric power engineering, and analyze the time complexity as well as bits complexity.     

探析办公自动化的网络安全

随着社会科学以及社会经济的高速发展,计算机已经普及到了日常的工作、生活,而利用计算机的办公自动化,更是办公的阶段性提高.但是,办公的自动化也伴随着一些网络的安全问题,而提高网络的安全监管,防止信息的失真、修改、盗取,就显得非常重要了.本文就这个问题进行简单的探讨.     

CAD/CAE公共服务平台中资源共享智能型系统研究

在产业技术公共服务平台的影响和带动下,随着其用户规模不断扩大和信息技术的发展,越来越要求平台服务向智能化发展,有必要对其中之一的资源共享智能型系统建设进行探讨。