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A simple method was developed for the determination of cadmium (Cd) and lead (Pb) in milk serum prepared by spontaneous souring, using graphite furnace atomic absorption spectrophotometry. Samples of raw milk were collected from the bulk holding tanks of thirty-six dairy farms in twelve localities in Izmit. The samples were kept at room temperature (25 °C) for 48 h in order to allow the pH to decrease below 4.6, and the casein and fat to precipitate. Milk serum was filtered and directly injected into a graphite tube. The standard addition method was employed, and 0.1% phosphoric acid was used as the matrix modifier. The mean recoveries from three added concentrations were 91.4% for Cd and 95.8% for Pb. Cadmium and Pb concentrations found in the reference standard milk powder using this method were close to the certified values. The mean Cd contents obtained from thirty-six samples were 0.257 μg L−1, ranging from 0.180 to 0.398 μg L−1. The mean Pb contents found were 6.83 μg L−1, ranging from 5.32 to 9.94 μg L−1.  相似文献   
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In this article we introduce the work of the National and State Libraries Australasia Digital Preservation Technical Registry project.

Any technical registry model must allow digital preservation analysts to understand the technical form of the content they are tasked with preserving, understand the capabilities they have in relation to that content, and reflect on the community position in relation to those capabilities. We believe the solution outlined here is well placed to deliver the information required to answer these questions, and in a manner that makes it easy to understand, reference and augment.

The primary focus of this article is to describe the format model, which is the most radical part of the Digital Preservation Technical Registry. The flexibility the model provides delivers on all of the requirements outlined by the NSLA partners and project team members; this includes the ability to reference many layers constituting a format, including relationships between specifications and implementations of real-world formats. We seek input from members of the community on the model and suggestions for use cases and requirements that we have not envisaged.  相似文献   
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An efficient catalytic system to oxidize quantitatively aliphatic diols using Trametes versicolor laccase and TEMPO has been developed in aqueous medium. Oxidations have occurred in a non‐stereoselective fashion but with complete regio‐ and/or monoselectivity, obtaining lactones with excellent purity after simple extraction. This catalytic system has been demonstrated to be scalable, compatible with the presence of a variety of functionalities, and also allowed the successful enzyme recycling using a laccase‐cross‐linked enzyme aggregates (CLEA) preparation.  相似文献   
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Foams of an engineering plastic, poly(ether imide), were extruded using a single screw extruder employing pressurized CO2 as the blowing agent. The porosity, pore size distributions, and the density of the foams were especially affected by the pressure drop, the pressure loss rate, and temperature at the die. Significant increases in porosity and pore size and corresponding decreases in density were observed when the pressure imposed on CO2 became greater than the critical pressure values of CO2 (i.e., the temperature was always greater than the critical temperature of the CO2 in the extruder and the die). The viscoelastic material functions of the extruded foams depended especially on the density of the foam, with the elastic modulus increasing with density. The incorporation of nanosilica particles in the 0.08–0.6% by weight range increased only the density of the foam and did not provide any benefits in controlling of the nucleation rate and the pore size distribution, presumably due to their poor dispersibility and agglomerated state in the single screw extruder. POLYM. ENG. SCI., 54:2064–2074, 2014. © 2013 Society of Plastics Engineers  相似文献   
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