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11.
A photochromic nanocomposite based on Keggin structure phosphomolybdic acid (PMoA) well dispersed in polyethyleneglycol (PEG) was fabricated. TEM image showed that PMoA nanoparticles with narrow size distribution were finely dispersed in polymer matrix. FT-IR results showed that the Keggin geometry of polyoxometalates was still preserved inside the composites and strong coulombic interaction was built between PMoA and polymer matrix. Under UV irradiation, the film was reduced photochemically to yield a blue species, which was in accordance with a charge-transfer mechanism. 相似文献
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采用反相悬浮聚合法合成高吸水性树脂.将丙烯酸(单体,水相)用氢氧化钠部分中和,然后与环己烷(溶剂,油相)共混,用水溶性的过硫酸钾做引发剂,N,N-亚甲基双丙烯酰胺做交联剂,在一定的反应温度和时间下,得到聚丙烯酸钠高吸水性树脂. 相似文献
15.
Nanofiber bundles of Ag2S, Ag2Se, and Ag have been successfully synthesized by making use of Ag2C2O4 template nanofiber bundles, utilizing both anion‐exchange and redox reactions. The obtained bundles were polycrystalline nanofibers composed of nanoparticles in which the precursor morphology was well‐preserved, indicating that Ag2C2O4 nanofiber bundles acted as a general sacrificial template for the synthesis of silver‐based semiconductor and metal nanofibers. Dispersing media and transforming reactants were found to be key factors influencing the chemical transformation in the system. In particular, separate single‐crystalline Ag nanofibers were obtained via a nontemplate route when ascorbic acid was used as a relatively weak reductant. An electrical transfer and switching device was built with the obtained Ag2S and Ag nanofiber bundles, utilizing the unique ion‐conductor nature of Ag2S and revealing their potential applications in electronics. 相似文献
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Xin Qi Salapaka M.V. Voulgaris P.G. Khammash M. 《Automatic Control, IEEE Transactions on》2004,49(10):1623-1640
In this paper, the design of controllers that incorporate structural and multiobjective performance requirements is considered. The control structures under study cover nested, chained, hierarchical, delayed interaction and communications, and symmetric systems. Such structures are strongly related to several modern-day and future applications including integrated flight propulsion systems, platoons of vehicles, micro-electro-mechanical systems, networked control, control of networks, production lines and chemical processes. It is shown that the system classes presented have the common feature that all stabilizing controllers can be characterized by convex constraints on the Youla-Kucera parameter. Using this feature, a solution to a general optimal performance problem that incorporates time domain and frequency domain constraints is obtained. A synthesis procedure is provided which at every step yields a feasible controller together with a measure of its performance with respect to the optimal. Convergence to the optimal performance is established. An example of a multinode network congestion control problem is provided that illustrates the effectiveness of the developed methodology. 相似文献
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We have fabricated and tested a high-Tc dc-SQUID magnetometer patterned on a YBCO thin film deposited on a SrTiO3 bicrystal substrate. The measurement of noise spectrum at 77 K showed that the magnetometer has a white noise of 333 fT/Hz1/2 without superconducting shield, corresponding to a flux sensitivity of 14.5 μΦ0/Hz1/2. We constructed a test system for eddy current non-destructive evaluation of conducting aluminum plates by using the magnetometer. Flaws over 10 mm below the surface can be clearly identified. By mapping the magnetic field distribution, we can locate the flaw position. The signals caused by flaw were expanded due to the use of double-D type driving coil with a wider central slit. The experimental results confirmed that this test system could operate in a magnetic unshielded environment. 相似文献
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建立垂直管吸收器管内泡式吸收过程中传热传质的数学物理模型,对其泡式吸收过程进行数值研究,获得泡式吸收方式的一些传热传质特性,为吸收器的优化设计提供一定理论指导。 相似文献
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引导大学生自主学习,培养大学生的自主学习能力,已逐步成为高等教育工作者的共识.如何促进大学生的自主学习,关键取决于两个方面:就学生而言,要树立自主学习的观念,强调学习的自主性、主动性、自觉性、有效性;就教育制度而言,要建立与大学生自主学习相匹配的高考招生制度、学籍管理制度、学生管理制 相似文献