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71.
72.
P. Koštial I. Špička Z. Jančíková V. Rusnák 《Materialwissenschaft und Werkstofftechnik》2015,46(11):1110-1118
The paper deals with theoretical and experimental aspects of lumped capacitance model (LCM) application for the study of heat transport in different materials. Patented construction of the measuring chamber together with special software the fundamental features of which are presented here allows evaluating thermal conductivity k, specific heat capacity cp and thermal diffusivity α. Obtained results are in relatively very good agreement with those obtained from independent measurement or table values. 相似文献
73.
F. Cajner S. Kovačić H. Rafael A. Vugrinčić V. Šimunović B. Gržeta 《Materialwissenschaft und Werkstofftechnik》2015,46(1):69-77
Nitriding increases surface hardness and improves wear resistance of stainless steels. However, nitriding can sometimes reduce their corrosion resistance. In this paper, the influence of nitriding on the corrosion resistance of martensitic stainless steel was investigated. Plasma nitriding at 440 °C and 525 °C and salt bath nitrocarburizing were carried out on X17CrNi16‐2 stainless steel. Microhardness profiles of the obtained nitrided layers were examined. Phase composition analysis and quantitative depth profile analysis of the nitrided layers were preformed by X‐ray diffraction (XRD) and glow‐discharge optical emission spectrometry (GD‐OES), respectively. Corrosion behaviour was evaluated by immersion test in 1% HCl, salt spray test in 5% NaCl and electrochemical corrosion tests in 3.5% NaCl aqueous solution. Results show that salt bath nitrocarburizing, as well as plasma nitriding at low temperature, increased microhardness without significantly reducing corrosion resistance. Plasma nitriding at a higher temperature increased the corrosion tendency of the X17CrNi16‐2 steel. 相似文献
74.
75.
A largely increased number of GGGGCC repeats located in the non-coding region of C9orf72 gene have been identified as the leading cause of two related neurological disorders, familial amyotrophic lateral sclerosis (ALS) and frontotemporal dementia (FTD). We examined G-quadruplex forming ability of GGGGCCrepeat containing oligonucleotides with four guanine tracts chosen as the smallest possible model to form a unimolecular G-quadruplex. These oligonucleotides are readily to folded into G-quadruplexes in the presence of K+ ions. However, the formation of multiple structures makes structural analysis challenging and time consuming. We observed that flanking sequences on 5'- and 3'-ends as well as mutations of loop residues have a profound effect on folding. Sequence d[(G4C2)3G4] was chosen for further scrutiny and optimization of nuclear magnetic resonance (NMR) spectroscopic properties with dG to 8Br-dG substitutions at specific positions in the sequence under different folding conditions. Expectedly, folding into desired predominant topology is facilitated when substituted residue adopted a syn conformation in the naturally-occurring structure. Single dG to 8Br-dG substitution at position 21 and fine tuning of folding conditions facilitate folding of d[(G4C2)3GGBrGG] into (mostly) a single G-quadruplex, and thus enable determination of its high-resolution structure by high-field NMR. 相似文献
76.
The transformation of fertility and family behaviour in post-socialist countries was quick and the changes were striking. An account of the changes is the subject of dispute and the mechanisms have still not been explained in a fully satisfying manner. Relatively little attention has been paid to the changes in spatial aspects concerning the broadening of changes in family behaviour. The aim of this paper is to answer the question as to whether changes spread stochastically in post-socialist countries or if there are obvious spatial patterns. The study tries to answer the questions whether there are any cores of changes which may be understood as innovations, if there is any spatial clustering and if the extent is hierarchically arranged. 相似文献
77.
78.
Vilko Mandić Emilija Tkalčec Stanislav Kurajica 《Journal of the American Ceramic Society》2014,97(7):2264-2271
Monophasic gel with stoichiometric 3Al2O3·2SiO2 composition and gels with 0.99, 1.96, and 2.91 mol% La2O3 added were sol–gel derived. The crystallization path, structure evolution, microstructure, and morphology of calcined premullite powders and sintered ceramic bodies have been investigated as a function of La2O3 content and sintering temperature. In addition to mullite, spinel phase at about 980°C, and α‐alumina at above 1000°C were determined; however, neither La2O3 nor La‐related compounds had crystallized. The La2O3 predominately incorporated into the glassy phase, enhanced with La2O3 level, which affected both mullite structure and composition, as confirmed by electron microscopy, Rietveld structure refinement, determination of unit cell parameters, electron microscopy, and achieved density of the sintered bodies. Increased thermal treatment changes the alumina/silica ratio in mullite (towards 3:2 below 1200°C, and toward 2:1 above), and decreases the mullite/amorphous ratio. Sintered dense ceramic bodies revealed a positive densification effect and increased sinterability as a result of the lanthanum‐induced increase in glassy phase. 相似文献
79.
Hot embossing is an emerging technology, which enables cost‐effective and high‐productivity nanofabrication. It is important to optimize the processing parameters to achieve high replication accuracy nanostructure fabrication. In this article, to reveal the interrelationship between the hot embossing conditions and replication accuracy of two‐dimensional (2D) polyethylene terephthalate (PET) nanochannels, the numerical simulations were conducted by using the generalized Maxwell model. The constants of the generalized Maxwell model were calculated by a newly established fitting formula based on experimental compressive creep curves rather than tensile stress relaxation curves. Replication accuracy of 2D PET nanochannels was evaluated by a method based on weighted averages. Orthogonal method was employed during numerical simulations to optimize the hot embossing process. Under optimized hot embossing parameters, 2D PET nanochannels, ~80 nm wide, 250 nm deep and 4 mm long, were precision‐imprinted into a PET sheet. POLYM. ENG. SCI., 54:2398–2406, 2014. © 2013 Society of Plastics Engineers 相似文献
80.
Roland Vogel Regine Boldt Marijan Vučak Liane Häußler 《Polymer Engineering and Science》2014,54(9):2057-2063
It has been reported in the technical literature that whiskers of rodlike single crystals can be used in order to generate shish‐kebab structures or other different lamellae morphologies during isothermal or dynamic crystallization of sheared or presheared polymer melts. The expected advantage of the changed crystalline structure is a reinforcing effect of the composite. A lot of papers reported about the application of inorganic and organic whiskers such as cellulose and chitin whiskers. This study reports on an attempt to use acicular PCC as appropriate whisker for improving mechanical properties of polypropylene. In this article special attention is given to demonstrate the effect of flow induced crystallization under varying shear conditions in order to improve the mechanical properties. The effects were demonstrated using rheology, thermal analysis, tensile testing, and transmission electron microscopy. POLYM. ENG. SCI., 54:2057–2063, 2014. © 2013 Society of Plastics Engineers 相似文献