Methods for determining pesticides and polychlorinated biphenyls in food samples--problems and challenges

Determination of residual amounts of pesticides and polychlorinated biphenyls (PCBs) in food samples requires the use of specific techniques regarding sample preparation as well as instrumental analysis which should be characterized by a very low detection limit. A problem associated with the use of pesticides and PCBs is the need for controlling their residues in the environment, particularly in food, as these chemicals show a propensity to accumulate. The analysis of food samples for the presence of pesticides and PCBs brings on many difficulties because of the specificity of sample preparation consisting of multistep purification procedures of samples that contain trace amounts of an analyte. Concentration determinations of pollutants that easily dissolve in complex matrices, particularly in the presence of a large apportionment of interfering substances, pose a big challenge. Therefore, the basic step in food analysis for the presence of pesticides and PCBs is sample preparation which mainly consists of analyte enrichment and the removal of interfering substances. But all steps of the analytical procedure that include sample collection and preparation, extraction of analytes from matrix, extract purification, and final determination, are very significant; their precision and correct application have a decisive effect on the final result.     

Rope loading in frictional systems

The subject of this paper is the analysis of the maximum loading of ties in multiband frictional systems. Systems like these occur in different branches of mechanical engineering; they are commonly used for passengers elevators. Although the rope system of the elevator contains rockers, in order to equalize the loading of the separate bands, remarkable differences in loading do occur.

Conditions of static equilibrium of the rope system, having the form of inequalities, have been found. Programming methods have been applied, to find the maximum loading of ropes which can occur in different multiband systems. Results of the analysis have been compared with the results of experiments.     

Wireless link prediction and triggering using modified Ornstein–Uhlenbeck jump diffusion process

Through time domain observation, typical wireless signal strength values seems to exhibit some forms of mean-reverting and discontinuous “jumps” behaviour. Motivated by this fact, we propose a wireless link prediction and triggering (LPT) technique using a modified mean-reverting Ornstein–Uhlenbeck (OU) jump diffusion process. The proposed technique which we refer as OU-LPT is an integral component of wireless mesh network monitoring system developed by ICT FP7 CARrier grade wireless MEsh Network project. In particular, we demonstrate how this technique can be applied in the context of wireless mesh networks to support link switching or handover in the event of predicted link degradation or failure. The proposed technique has also been implemented and evaluated in a real-time experimental testbed. The results show that OU-LPT technique can significantly enhance the reliability of wireless links by reducing the rate of false triggers compared to a conventional linear prediction technique and therefore offers a new direction on how wireless link prediction, triggering and switching process can be conducted in the future.     

Existence of optimal solutions of two-directionally continuous linear repetitive processes

In the paper, an existence theorem for a Lagrange optimal control problem connected with a two-directionally continuous variant of a linear autonomous repetitive process is derived. As a corollary, existence of an optimal solution in the case of cost functional depending on a fixed ??end-function?? is obtained.     

New friction welding technology for joining tubes with lids

The article presents the results of research on the use of the new technology of friction welding with a non-wearing tool for welding pipe ends with lids. The pipes and lids were made of aluminium alloy EN AW 2017A, non-weldable by conventional methods. The aim of the study was to verify the possibility of welding the lid to the pipe using the FSW method as well as a new method with a tool with specially profiled friction surface. The article presents the results of structural tests and strength tests of the weld joints obtained using the new technique.     

Quasilinearized Regression

Estimation in nonlinear regression usually requires a considerable amount of computational work. If it is possible to linearize the original formulas, the linear regression is sometimes applied to transformed linear relations. The method of quasilinearized regression (first order approximation of nonlinear regression), comparable to linear regression, with respect to computational effort, is described in this paper. This method gives substantially better results than linear regression of linearized formula.