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21.
Transparent conducting SnO2 powders doped with 10% Fe content were prepared by a polymerized complex method under acidic solutions, and annealed finally at 550 °C, and at 600 °C. These samples were characterized by X-ray diffraction, magnetization, and Mössbauer spectrometry at room temperature. Rutile SnO2 phase was obtained for both samples, and the crystallite sizes were in the range of 13-14 nm. Both samples exhibit magnetization and the saturation magnetization was smaller for the sample annealed at 600 °C than for sample annealed at 550 °C. Room temperature Mössbauer spectra for both samples showed the presence of two different paramagnetic iron sites but no magnetic sextets. These results suggest that ferromagnetism originates from magnetic defects and not directly from iron ions. 相似文献
22.
Saburo Matsuoka Hiroyuki Masuda Masuo Shimodaira 《Metallurgical and Materials Transactions A》1990,21(8):2189-2199
The fatigue threshold and low-rate crack propagation properties for a carbon steel, two high-strength steels, and two stainless
steels were investigated in a 3 pct sodium chloride aqueous solution at frequencies between 0.03 and 30 Hz. Tests were conducted
in a manner designed to avoid crack closure. Under freely corroding conditions, the effective values of the threshold stress
intensity factor range, ΔKth,eff, were lower than in air for all of the steels. In particular, the ΔKth,eff values for the carbon and high-strength steels were almost equal to the theoretical ΔKth value of about 1 MPa m1/2 calculated on the basis of the dislocation emission from the crack tip. At a given ΔK level higher than the threshold, the
fatigue crack propagation rates accelerated with decreasing frequency for all of the steels. Under cathodic protection, the
threshold and fatigue crack propagation properties were coincident with those in air regardless of material and frequency.
The observed fatigue crack propagation behavior in a 3 pct NaCl solution was closely related to the corrosion reaction of
the bare surface formed at the crack tip during each loading cycle. 相似文献
23.
Tadao Aizawa 《Electrical Engineering in Japan》2009,166(2):32-38
Most general‐purpose analyzers for harmonic analysis on distribution lines are designed to sample the data of one or two power supply periods. In other words, these analyzers process waveforms and display the results based on the assumption that the analyzed waveforms contain no noninteger components, such as subharmonics and interharmonics. When waveforms containing noninteger components are analyzed with these general‐purpose analyzers, the results often indicate components that are not actually present. This paper proposes a technique of waveform judgment and explains its method of application. The technique allows noninteger components to be recognized in analyzed waveforms from the properties of Lissajous figures, and clarifies the types of components and the time windows necessary for appropriate analysis. © 2008 Wiley Periodicals, Inc. Electr Eng Jpn, 166(2): 32– 38, 2009; Published online in Wiley InterScience ( www.interscience.wiley.com ). DOI 10.1002/eej.20536 相似文献
24.
Masaaki Suzuki Yoshihisa Hasegawa Masayuki Aizawa Yoshinori Nakata Takeshi Okutani Kohei Uosaki 《Journal of the American Ceramic Society》1995,78(1):83-89
The structure of silicon carbide–silicon nitride (SiC–Si3 N4 ) composite particles synthesized using a CO2 laser was studied by magic angle spinning nuclear magnetic resonance (MAS-NMR) and electron spin resonance (ESR). The structure around Si atoms changed by introducing N. C atoms around Si were substituted by N atoms, and N-rich configurations around Si atoms increased stepwise as the N content increased. The low N content composite particles consisted of mainly SiC phase containing dissolved N. N atoms were partly present in β-SiC microcrystal and partly in the grain boundary layer in the particle. N atoms were tetrahedrally surrounded by four Si atoms in β-SiC microcrystal and were trivalent state bonded to three Si atoms in the grain boundary layer. The high N content particles consisted of SiC, Si3 N4 , and amorphous phases, whose amount depended on N content. 相似文献
25.
Kotohiko Sekoguchi Koji Mori Masuo Kaji Megumi Miwa Masao Nakazatomi Hideo Shimizu 《亚洲传热研究》1996,25(8):568-579
Gas-liquid interfacial profiles in plug flow for both upward and downward flows were obtained using semi-supermultiple point-electrode probes, comprising 67 sensing tips arranged on a tube diameter. Typical interfacial profiles are demonstrated for both flows. Close inspection of the profiles reveals that four zones exist in a pair of gas and liquid slugs for upward plug flow and a high slip velocity region in downward plug flow. The lengths of the swelling liquid front zone and the wake zone were determined. The length of the wake zone strongly depends on the relative velocity between the liquid film around the gas slug and the liquid phase in the liquid slug. Characteristic distributions of bubbles within liquid slugs were found, i.e., three types of radial distributions of void fraction, namely saddle-shaped, trapezoidal and bullet-shaped distributions, exist for upward flow. The two types for downward flow exclude the saddle-shaped distribution. © 1997 Scripta Technica, Inc. Heat Trans Jpn Res, 25 (8): 568–579, 1996 相似文献
26.
Hisayasu Mitsui Ryoji Kumazawa Rie Aizawa Tatsuki Okamoto Tetsuo Ito Masaki Kanegami 《Electrical Engineering in Japan》1999,129(4):24-31
Experiments and investigations were carried out on the voltage life of a bar-coil model with a nickel-plated copper conductor covered with mica-alumina composite insulation at a temperature range of 550–850 °C. Diffusion of copper into the insulation layer was observed on the specimens aged for a long period. Insulation with mica paper gave faster diffusion speed and shorter voltage life than insulation with mica flake. The diffusion speed became higher with an increase in temperature. The ac current gradually increased with aging time and increased rapidly just before breakdown. There was the relationship I = aEn (a, n: constants) between ac current I and applied stress E, and n was approximately equal to 1 in the region where thermal unbalance did not occur. Arrhenius's law held in the relationship between ac current and aging time. Therefore, the breakdown mechanism might be that the effective insulation thickness decreased due to copper diffusion into the insulation layer and the ac current increased gradually until thermal breakdown in the last stage. If copper diffuses into the insulation layer, even with no voltage application, the aging time required to decrease the breakdown voltage to a certain level (the voltage life) obeys Arrhenius's law. If the voltage life is dominated by diffusion into the insulation layer, the activation energy for voltage life in the aging test becomes twice that for diffusion, both with and without voltage application. © 1999 Scripta Technica, Electr Eng Jpn, 129(4): 24–31, 1999 相似文献
27.
28.
High‐Performance Dibenzoheteraborin‐Based Thermally Activated Delayed Fluorescence Emitters: Molecular Architectonics for Concurrently Achieving Narrowband Emission and Efficient Triplet–Singlet Spin Conversion 下载免费PDF全文
Thermally activated delayed fluorescence (TADF) materials, which enable the full harvesting of singlet and triplet excited states for light emission, are expected as the third‐generation emitters for organic light‐emitting diodes (OLEDs), superseding the conventional fluorescence and phosphorescence materials. High photoluminescence quantum yield (ΦPL), narrow‐band emission (or high color purity), and short delayed fluorescence lifetime are all strongly desired for practical applications. However, to date, no rational design strategy of TADF emitters is established to fulfill these requirements. Here, an epoch‐making design strategy is proposed for producing high‐performance TADF emitters that concurrently exhibiting high ΦPL values close to 100%, narrow emission bandwidths, and short emission lifetimes of ≈1 µs, with a fast reverse intersystem crossing rate of over 106 s?1. A new family of TADF emitters based on dibenzoheteraborins is introduced, which enable both doped and non‐doped TADF‐OLEDs to achieve markedly high external electroluminescence quantum efficiencies, exceeding 20%, and negligible efficiency roll‐offs at a practical high luminance. Systematic photophysical and theoretical investigations and device evaluations for these dibenzoheteraborin‐based TADF emitters are reported here. 相似文献
29.
Byung-Hak Choe Soo-Keun Shin Sung-Joon Kim Yong-Tai Lee S. B. Kang Masuo Hagiwara 《Metals and Materials International》2005,11(6):429-433
The effects of aging treatment on the microstructures and mechanical properties of a metastable beta titanium alloy Ti-15-3
(Ti−15V−3Al−3Sn-3Cr) have been investigated with hardness measurements, tensile test, and optical and electron microscopy.
Precipitate-free beta structure with average grain size of about 56 μm was obtained after solution treatment at 800°C for
15 min followed by air cooling. Solution treated specimens were aged up to 800 h in the temperature range between 350 and
600°C. The morphology of the precipitates was varied significantly, depending on the aging temperature. The fine aggregates
of α precipitates were dominant above 450°C. Peak hardness values were maintained up to 800 h at 500°C, which showed the superior
thermal stability of α precipitates. Tensile strength increased up to 1600 MPa along with the decrease of elongation after
aging at 350 and 400°C. 相似文献
30.
Toru Katsumata Hiromi Kubo Shuji Komuro Hiroaki Aizawa 《Journal of the American Ceramic Society》2014,97(6):1704-1707
Photoluminescence spectrum, trap depths, and densities of trapped carriers of CaAl2O4:Eu phosphor crystals doped with rare‐earth elements were studied using the thermally stimulated luminescence technique. Trap depths and densities of the specimens vary with rare‐earth elements doped as the auxiliary activators. Tm and Nd are found to be effective for the strong afterglow phosphorescence peaking at λ = 442 nm for several hours after the excitation. CaAl2O4:Eu phosphor crystals doped with Nd and Tm include high density of carriers trapped at E = 0.59 and 0.52 eV, respectively. 相似文献