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991.
Gerrit Wienhfer Kristin Schrder Konstanze Mller Kathrin Junge Matthias Beller 《Advanced Synthesis \u0026amp; Catalysis》2010,352(10):1615-1620
Arenes are selectively oxidized to the corresponding quinones employing ruthenium(2,2′,6′:2′′‐terpyridine)(2,6‐pyridinedicarboxylate) [Ru(tpy)(pydic] as catalyst and hydrogen peroxide as the terminal oxidant. Applying alkylated naphthalenes and phenols, benzo‐ and naphthoquinones are obtained in up to 93% yield. The industrially interesting oxidation of 2‐methylnaphthalene gave 74% of the corresponding quinones and 60% of menadione (vitamin K3). 2,3,5‐Trimethylbenzoquinone which constitutes the key intermediate for vitamin E is obtained in 83% yield. 相似文献
992.
A high-pressure cell for kinetic studies on gas hydrates by powder x-ray diffraction 总被引:1,自引:0,他引:1
Luzi M Girod M Naumann R Schicks JM Erzinger J 《The Review of scientific instruments》2010,81(12):125105
A new high-pressure-low-temperature cell was developed for in situ observations of gas hydrates by powder x-ray diffraction. The experimental setup allows investigating hydrate formation and dissociation as well as transformation processes between different hydrate crystal structures as a function of pressure, temperature, and feed gas composition. Due to a continuous gas flow, the composition of the gas phase is kept constant during the whole experiment. This is crucial for the formation of mixed hydrates formed from feed gas mixtures that contain one or more components in low concentrations. The pressure cell can be used in a pressure range between 0.1 and 4.0 MPa and a temperature range between 248 and 298 K. First results of time-resolved measurements of a mixed structure II CH(4) + iso-C(4)H(10) hydrate and a structure I CO(2) hydrate are presented. 相似文献
993.
论述了纳米技术产品的生命周期以及各方面的风险评估。对溶胶凝胶过程,包括其使用、应用以及由该技术生产的产品进行了详细的阐述。进一步证明了在当今已经可能以负责任的态度处理纳米材料。 相似文献
994.
Haixia Zhang Dongfeng Yuan Matthias Ptzold Yi Wu Van Duc Nguyen 《Wireless Communications and Mobile Computing》2010,10(6):758-771
In this paper, we extend the geometrical one‐ring multiple‐input multiple‐output (MIMO) channel model with respect to frequency selectivity. Our approach enables the design of efficient and accurate simulation models for wideband space‐time MIMO channels under isotropic scattering conditions. Two methods will be provided to compute the parameters of the simulation model. Especially, the temporal, frequency and spatial correlation properties of the proposed wideband space‐time MIMO channel simulator are studied analytically. It is shown that any given specified or measured discrete power delay profile (PDP) can be incorporated into the simulation model. The high accuracy of the simulation model is demonstrated by comparing its statistical properties with those of the underlying reference model with specified correlation properties in the time, frequency and spatial domain. As an application example of the new MIMO frequency‐selective fading channel model, we study the influence of various channel model parameters on the system performance of a space‐time coded orthogonal frequency division multiplexing (OFDM) system. For example, we investigate the influence of the antenna element spacings of the base station (BS) antenna as well as the mobile station (MS) antenna. It turns out that an increasing of the antenna element spacing at the BS side results in a higher diversity gain than an increasing of the antenna element spacing at the MS side. Furthermore, the diversity gain brought in by space‐time block coding schemes is investigated by simulation. Our results show that transmitter diversity can significantly reduce the symbol error rate (SER) of multiple antenna systems. Finally, the influence of the Doppler effect and the impact of imperfect channel state information (CSI) on the system performance is also investigated. Copyright © 2009 John Wiley & Sons, Ltd. 相似文献
995.
What we believe to be a new optical approach for the identification of mines and explosives by analyzing the surface materials and not only bulk is developed. A conventional manually operated mine prodder is upgraded by laser-induced breakdown spectroscopy (LIBS). In situ and real-time information of materials that are in front of the prodder are obtained during the demining process in order to optimize the security aspects and the speed of demining. A Cr4+:Nd3+:YAG microchip laser is used as a seed laser for an ytterbium-fiber amplifier to generate high-power laser pulses at 1064 nm with pulse powers up to E(p) = 1 mJ, a repetition rate of f(rep.) = 2-20 kHz and a pulse duration of t(p) = 620 ps. The recorded LIBS signals are analyzed by applying neural networks for the data analysis. 相似文献
996.
Link M Schreiter M Weber J Primig R Pitzer D Gabl R 《IEEE transactions on ultrasonics, ferroelectrics, and frequency control》2006,53(2):492-496
Solidly mounted film bulk acoustic resonators (FBAR) operating at 850 MHz in the shear vibration mode have been fabricated. C-axis inclined zinc oxide (ZnO) thin films realized by modified reactive magnetron sputtering were used: Coupling factors k2 of 1.7% and Q-factors of 312 were determined in air. Q-factors of 192 were measured in water, making these devices attractive for sensing applications in liquids, e.g., biosensing. 相似文献
997.
Bethge M 《Journal of the Optical Society of America. A, Optics, image science, and vision》2006,23(6):1253-1268
The performance of unsupervised learning models for natural images is evaluated quantitatively by means of information theory. We estimate the gain in statistical independence (the multi-information reduction) achieved with independent component analysis (ICA), principal component analysis (PCA), zero-phase whitening, and predictive coding. Predictive coding is translated into the transform coding framework, where it can be characterized by the constraint of a triangular filter matrix. A randomly sampled whitening basis and the Haar wavelet are included in the comparison as well. The comparison of all these methods is carried out for different patch sizes, ranging from 2x2 to 16x16 pixels. In spite of large differences in the shape of the basis functions, we find only small differences in the multi-information between all decorrelation transforms (5% or less) for all patch sizes. Among the second-order methods, PCA is optimal for small patch sizes and predictive coding performs best for large patch sizes. The extra gain achieved with ICA is always less than 2%. In conclusion, the edge filters found with ICA lead to only a surprisingly small improvement in terms of its actual objective. 相似文献
998.
Seleverstov O Zabirnyk O Zscharnack M Bulavina L Nowicki M Heinrich JM Yezhelyev M Emmrich F O'Regan R Bader A 《Nano letters》2006,6(12):2826-2832
Lately certain cytotoxicity of quantum dots (QDs) and some deleterious effects of labeling procedure on stem cells differentiation abilities were shown. In the present study we compared cytotoxicity and intracellular processing of two different-sized protein-conjugated QDs after labeling of the human mesenchymal stem cells (hMSC). An asymmetrical intracellular uptake of red (605 nm) and green (525 nm) quantum dots was observed. We describe for the first time a size-dependent activation of autophagy, caused by nanoparticles. 相似文献
999.
Georg Lochas Andreas Forner Donald Mathes Matthias Stengler Nico Beuche 《Bautechnik》2009,86(11):704-709
Derzeit entsteht der 4. Erweiterungsbau der Deutschen Nationalbibliothek in Leipzig. Der neue Baukörper grenzt bereichsweise an die Bestandsgebäude und wurde 6 bis 8 m unterhalb der bestehenden Fundamente gegründet. Der setzungsempfindliche Baugrund infolge eines 4 m mächtigen Kohleflözes musste in der Planung besonders berücksichtigt werden. Um die Bestandsgebäude gegen Setzungen, Rissbildungen und Schiefstellungen zu schützen, wurden außergewöhnliche Sicherungsmaßnahmen realisiert: –·Zusammenspannen der Gebäude mittels Anordnung von Zugstäben –·Auskreuzung gefährdeter Bereiche durch Holz‐Fachwerkverbände –·Anwendung einer besonderen Technologie der HDI‐Unterfangung. Mit diesen Maßnahmen konnten ungleichmäßige Setzungen und Rissbildungen weitestgehend vermieden werden. The German National Library in Leipzig – 4th extension – Special features of the underpinning and safety measures of inventory. At present the 4th extension of the German National Library in Leipzig is under construction. The new building is near the existing buildings and was founded in 6 to 8 m below the existing foundations. The ground is liable to subsidence due to a 4 m thick coal seam. This had to be specially considered in the planning. To protect the existing buildings against settlements, cracking and misalignment extraordinary safety measures were implemented: –·tensioning arrangement of buildings by means of tension bars –·strengthening of vulnerable areas by timber trussed bond –·using a special technology of grouted underpinning With these measures, non‐uniform settlements and cracks could be largely avoided. 相似文献
1000.
Im Beitrag wird auf Besonderheiten bei der Umsetzung des Generalplans Küstenschutz Niedersachsen/Bremen im Land Bremen eingegangen. Im ersten Teil werden die Grundlagen und Ergebnisse des Generalplans sowie die administrative Aufstellung des Landes Bremen zur Anpassung des Hochwasserschutzes beschrieben. Das Instrument der Kostenvergleichsrechnung wird vorgestellt, welches in Bremen bereits im frühen Projektstadium zur Bewertung der Vorzugslösungen eingesetzt wird. Ein wichtiger Aspekt bei der Umsetzung des Generalplans sind die technischen Anforderungen, die sich aus den bestehenden Hochwasserschutzanlagen ergeben. Weiterhin müssen im Land Bremen die Maßnahmen zum Hochwasserschutz im Wesentlichen unter Berücksichtigung der bestehenden konstruktiv geprägten Ufer (Spundwände und Kaianlagen) umgesetzt werden. Dabei sind spezielle Anforderungen hinsichtlich der aktuellen und zukünftigen Nutzung insbesondere in den Hafenrevieren zu berücksichtigen. Beispielhaft werden begleitende Projekte der INROS LACKNER AG vorgestellt. Flood protection in the Federal State and the city of Bremen by adjustment of climate changes. The present article describes how the Federal State and the Free Hanseatic City of Bremen adapts its flood protection with respect to climate changes and global sea level rise. Design basics are compiled in the “Generalplan Küstenschutz Niedersachsen/Bremen” (General Plan for Coastal Protection – Lower Saxony/Bremen). Main results of the general plan will be described and administrative aspects of the adaptation of the flood protection elements in Bremen will be lined out. Special technical requirements as the consideration of existing walls and dikes will be described. Also requirements from harbour operation, recreational use and urban architecture have to be considered as the Bremen port partly undergoes a rapid change in this regard. The instrument of cost analysis will be introduced which is utilised in Bremen at an early stage of planning in order to develop cost effective measures of public founded projects. Mentioned topics will be described based on projects carried out by INROS LACKNER AG. 相似文献