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941.
Summary The ring-opening polymerization of 2-phenyl-1,3,-6,2-trioxaphosphocane (4), an eight-membered cyclic phosphonite, has been investigated. Cationic initiators of PhCH2-Cl and MeOTf gave polymers, whereas anionic and radical initiators did not yield polymer. The structure of polymer was examined by IR, 1H, 31P, and 31C NMR spectroscopy of polymers and elemental analysis as well as the alkaline hydrolysis products. The polymer consisted of two different units, i.e., the major part is the normal phosphinate structure 5 and the minor part is the isomerized unit 6 in 7% with PhCH2Cl initiation and in 34% with MeOTf initiator. The difference in nature of propagating species from these two initiators are discussed in connection with their reactivities.On leave from the Institute of Chemistry, Academia Sinica, Beijing, China 相似文献
942.
901快速强力胶的研制 总被引:3,自引:0,他引:3
详细论述了一种新型改性SBS溶剂型胶粘剂的配方设计、制备工艺、基本性能等有关问题。 相似文献
943.
熔体塔式造粒法生产尿基复混肥 总被引:2,自引:0,他引:2
化肥企业生产尿基复混肥对于农业科学施肥、提高肥料利用率、避免环境污染及促进企业产品结构调整都具有十分重要的意义。熔体塔式造粒法生产尿基复混肥较之其它方法优越性更为显著,笔者简要介绍该法的生产机理、工艺流程、技术特点、国内现状及产品市场前景等方面的一些情况。 相似文献
944.
抗蚜威原药和制剂的气相色谱分析 总被引:2,自引:0,他引:2
本文报道了抗蚜威的气相色谱分析方法,其标准偏差为0.019,变异系数为0.244%,回收率为99 ̄101%,适于抗蚜威原药和制剂的分析。 相似文献
945.
Sodium-ion battery (SIB) is an ideal device that could replace lithium-ion battery (LIB) in grid-scale energy storage system for power because of the low cost and rich reserve of raw material. The key challenge lies in developing electrode materials enabling reversible Na+ insertion/desertion and fast reaction kinetics. Herein, a core-shell structure, FeS2 nanoparticles encapsulated in biphase TiO2 shell (FeS2@TiO2), is developed towards the improvement of sodium storage. The diphase TiO2 coating supplies abundant anatase/rutile interface and oxygen vacancies which will enhance the charge transfer, and avoid severe volume variation of FeS2 caused by the Na+ insertion. The FeS2 core will deliver high theoretical capacity through its conversion reaction mechanism. Consequently, the FeS2@TiO2 nanorods display notable performance as anode for SIBs including long-term cycling performance (637.8 mA·h·g-1 at 0.2 A·g-1 after 300 cycles, 374.9 mA·h·g-1 at 5.0 A·g-1 after 600 cycles) and outstanding rate capability (222.2 mA·h·g-1 at 10 A·g-1). Furthermore, the synthesized FeS2@TiO2 demonstrates significant pseudocapacitive behavior which accounts for 90.7% of the Na+ storage, and efficiently boosts the rate capability. This work provides a new pathway to fabricate anode material with an optimized structure and crystal phase for SIBs. 相似文献
946.
J. Binner J. Wang B. Vaidhyanathan N. Joomun J. Kilner G. Dimitrakis T. E. Cross 《Journal of the American Ceramic Society》2007,90(9):2693-2697
A microwave/conventional hybrid furnace has been used to anneal virtually fully dense zinc oxide ceramics under pure conventional and a microwave/conventional hybrid heating regime with a view to obtaining evidence for the "microwave effect" during the resulting grain growth. In each case it was ensured that each sample within a series had an identical thermal history in terms of its temperature/time profile. The results showed that grain growth was enhanced during hybrid heating compared with pure conventional heating; the greatest enhancement, a factor of ∼3 increase in average grain size, was observed in the range 1100°–1150°C. The grain growth exponent decreased from 3 during conventional heating to 1.4 during hybrid heating in this temperature range, suggesting an acceleration of the diffusional processes involved. Temperature gradients within the samples were found to be too small to explain the results. This suggests that clear evidence has been found to support the existence of a genuine "microwave effect." 相似文献
947.
用RAP法(reactivo atmosphere process)处理KCl熔体,在不改变生长气氛和RAP继续处理的情况下,提拉生长KCl晶体,以解决高纯、大尺寸、生长速度快、成品率高和有较大经济效益的问题。 相似文献
948.
通过对安庆石化总厂化肥厂CO_2压缩机多起强烈振动信号的频谱分析,找出了谱图上的一些规律性特征,并在理论上加以解释,文章还提出了现场应急处理的对策以及根治办法。 相似文献
949.
950.
Providing an easy ingress–egress (I/E) movement remains a challenge for car designers. I/E has been largely studied in kinematics, but not in dynamics. This study proposes: (1) to evaluate and describe the motor torques developed in the lower limbs and lumbar joints during I/E motions and (2) to analyse the influence of the car geometry and subject anthropometry. An experiment was performed to observe 15 subjects of three anthropometrical groups getting in and out of a car mock-up simulating three different vehicle configurations. Motor torques were extracted using an inverse dynamics analysis. Both ingress and egress motions were primarily characterised by large torques. Overall, the taller a subject and the lower the seat of the vehicle were, the larger the peak torques were. Moreover, peak torques were higher for egress than ingress. These results are discussed in regard to the current knowledge on I/E ergonomics. 相似文献