两步法合成双氰胺工艺

采用两步法由氰氨化钙合成双氰胺,通过正交试验,考察了水解温度、聚合温度、聚合时间对产品收率的影响,确定了最佳的工艺条件:水解温度42℃、聚合温度70℃、聚合时问150 min,此条件下,双氰胺收率可达85.73％。     

双时基频率校准电路

提供精确的时间基准是精密仪器和高精度设备计时和工作的关键技术之一。文中采用两套晶振电路，通过分频产生高频和低频两个频率信号，采用编码的方法对两个频率信号在每一个时钟周期内进行动态校核，只有两个晶振的频率在允许的精度范围内，或同时增大（缩小）相同的倍数，校核后频率信号才是正确的，且能给系统提供精确的时间基准。该方法能有效防止系统的时钟周期因意外的原因伸长或缩短。整个电路可以作为精密仪器或高精度设备的一个模块电路。     

地源热泵——辐射地板联供试验

通过地源热泵－辐射地板系统冬夏联供试验，讨论了该系统作为新型环保节能空调方式的可行性及优越性，并对运行中出现的问题进行分析。     

I/OIMAGESYSTEM微波中继应用

微波中继的应用非常广泛 ,目前在二维、三维施工中跨越障碍物时 ,一般都使用微波中继站来传输命令和数据。文章就微波中继及I/OIMAGESYSTEM“蛇形排列”先进功能的实际应用进行了详细的阐述 ,同时提出了使用微波中继站应注意的问题。     

一种在Kalman滤波中引入径向速度测量的新方法

研究在距离和径向速度测量噪声统计相关的情形下把径向速度测量引入Kalman滤波的新方法。分析了径向速度测量噪声与位置测量更新后状态滤波误差的统计相关性,根据Gauss-Markov定理导出了对应于径向速度测量的滤波方程由此而得到一种序贯滤波算法。两个不同的蒙特卡罗仿真表明,通过采用这一新算法引人径向速度测量,不仅可以大大提高状态估计的精度,而且其估计性能和计算效率优于传统的EKF。     

钨合金废料的资源再生利用技术

钨是一种稀有金属，钨合金具有高的强度、硬度，较好的耐高温性、耐密性和良好的电性能。广泛应用于航空航天工业、兵器工业、核工业、信息产业、汽车工业和钢铁工业等行业。目前，钨资源短缺，钨合金价格高、用量大，因此各国都把废弃的钨合金作为宝贵的第二钨资源加以再生利用。本文综述了钨合金的再生利用现状，分别总结了硬质合金、高比重合金、钨铜合金和钨材的再生利用技术，并利用生态环境材料的观点。对每种再生利用技术作了简单的评价。     

手机充电器接口标准

推荐理由:保护消费者的利益,减少社会资源的浪费,节能环保. 关键词注释:2006年年底,信息产业部发布行业标准<移动通信手机充电器及其接口的技术要求和测试方法>.     

Cholesterol‐imprinted polymer receptor prepared by a hybrid imprinting method

A novel cholesterol‐imprinted polymer (CMIP‐H) was prepared by a hybrid method of covalent imprinting and non‐covalent imprinting. This approach involves the copolymerization of a template‐containing monomer, cholesteryl 2‐hydroxyethyl methacrylate carbonate, and a cross‐linker, followed by hydrolysis to afford a flexible guest‐binding site accompanied with the easy and efficient removal of a ‘sacrificial spacer’. The effect of solvent on the binding capacity of CMIP‐H towards cholesterol was studied, indicating that a good binding capacity towards cholesterol could be achieved in a less‐polar solvent. The binding experiments of CMIP‐H towards a series of structural analogues of cholesterol, including cholesterol acetate, progesterone and stigmasterol, were carried out in hexane. The results showed that CMIP‐H almost did not bind cholesterol acetate at all because the hydrogen‐bonding site is blocked. It exhibited a similar binding towards both cholesterol and stigmasterol, but much higher binding towards progesterone. Copyright © 2005 Society of Chemical Industry     

Study of a BGO calorimeter using electron and hadron beams from 1 to 50 GeV

A calorimeter of 25 bismuth germanate (BGO) crystals equipped with silicon photodiode readout has been tested at the CERN SPS in the energy range 1–50 GeV. The response for electrons has been shown to be linear in this energy range and the rms resolution obtained ( ) is approximately 1%, for E > 4 GeV. The electron/pion separation was found to be better than 1:500 in the energy range 1–20 GeV. Data on lateral and longitudinal shower development were compared with the results of a Monte Carlo simulation using the SLAC-EGS program and found to be in good agreement.     

Colour Centres and Energy Transfer in BaF2-xClx:Eu2+ Phosphors

The optical absorption spectra of BaF2-xClx:Eu2 after ultraviolet (UV) light excitation were investigated.The differences between the absorption spectra after and before excitation (DAS) were observed.The DAS increase at both the high and the low energy side of F band in BaF2-xClx:Eu2 after 245 nm UV light excitation.The bleach effect of UV light and the absorption of electrons in the valence band may account for the former and the formation of Fa centres (association of F(Cl-) centres), whose absorption band matches the HeNe laser better, may explain the latter.In the write-in process, the transfer of electrons is via tunneling.In the readout process, the transfer of electrons captured in F(F-) and Fa centres is more likely via tunneling, and that of F(Cl-) centres is more likely via conduction band.