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11.
Coating of 0.65Pb(Mg1/3Nb2/3)O3–0.35PbTiO3 (PMN–PT) relaxor ferroelectrics by a sol–gel method is followed by growth of epitaxial SrRuO3 (SRO) metallic oxide electrodes on SrTiO3 (STO) single-crystal substrate by pulsed laser deposition. High-quality PMN–PT films on SRO with preferred growth orientation were successfully fabricated by controlling the operation parameters. Structural properties of relaxor ferroelectric PMN–PT thin films on SRO/STO substrates have been studied by X-ray diffraction (XRD), transmission electron microscopy (TEM) and atomic force microscopy (AFM). In-plane and out-of-plane alignments of the heterostructure are confirmed and the structural twinning of the materials are also revealed. 相似文献
12.
A thin film of poly(l-serine) was prepared via electropolymerization for the determination of trace levels of estradiol. In pH 5.0 phosphate buffer,
l-serine was oxidized during the cyclic potential sweeps between −0.60 and 2.0 V, forming a thin film at the electrode surface.
The electrochemical behavior of estradiol was investigated. The oxidation peak potential of estradiol shifts negatively at
the poly(l-serine) film-coated glassy carbon electrode (GCE) compared with that at the bare GCE. Otherwise, the oxidation peak current
greatly increases at the poly(l-serine) film-modified GCE. These phenomena suggest that the poly(l-serine) film exhibits catalytic activity towards the electrochemical oxidation of estradiol. Based on this, a sensitive,
rapid and simple electrochemical method was proposed for the determination of estradiol. The limit of detection is evaluated
to be 2.0 × 10−8 mol L−1. Finally, this method was successfully used to determine estradiol in blood serum. 相似文献
13.
High molecular weight, high functionality diamino telechelic polybutadienes (TPBs) were synthesized by ring-opening metathesis polymerization (ROMP) of 1,5-cyclooctadiene (COD) in the presence of a chain transfer agent, 1,8-dicyano-4-octene, followed by lithium aluminum hydride reduction. Melt coupling of diamino TPB with anhydride-terminated polystyrene (PS-anh) resulted in the formation of styrene-butadiene-styrene (SBS) triblock copolymers; ca. 80% maximum conversion of PS-anh was achieved within 30 s. The results from SAXS, TEM, and rheological measurements of the coupling products confirmed the formation of SBS triblock copolymers having lamellar morphology. A fluorescent-labeled PS-anh was used to study the coupling kinetics by diluting the reactants by the addition of non-functional PS. 相似文献
14.
A multiple steam generator tube rupture (MSGTR) event in APR1400 has been investigated using the best estimate thermal hydraulic system code, MARS1.4. The effects of the parameters such as the number of ruptured tubes, rupture location, affected steam generator on the analysis of the MSGTR event in APR1400 are examined. In particular, tube rupture modeling methods, single tube modeling (STM) and double tube modeling (DTM), are compared. The APR1400 is found to have the capability of allowing more than 30 min to operators for the MSGTR event of five tubes. The effects of rupture location on the MSSV lift time is not significant in the case of STM, but the MSSV lift time for tube-top rupture is found to be 25.3% larger than that for rupture at the hot-leg side tube sheet in the case of DTM. The MSSV lift time for the cases that both steam generators are affected (4C5x, 4C23x) are found to be larger than that of the single steam generator cases (4A5x, 4B5x) due to a bifurcation of the primary leak flow. The discharge coefficient of Cd is found to affect the MSSV lift time only for a smaller value of 0.5. It is found that the most dominant parameter governing the MSSV lift time is the leak flow rate. Whether any modeling method is used, it gives the similar MSSV lift time if the leak flow rate is close, except in the case where both steam generators are affected. Therefore, the system performance and the MSSV lift time of the APR1400 are strongly dependent on the break flow model used in the best estimate system code. 相似文献
15.
Jiří Polívka 《Journal of Infrared, Millimeter and Terahertz Waves》1996,17(10):1779-1788
In his earlier paper on Active Microwave Radiometry, the author indicated that microwave noise can be used to map field density distribution inside radiators and in antenna systems, without the need for anechoic chambers. The presented paper gives details and results of such experiment. The method is described, details of equipment are given and results are presented with a concluding commentary. 相似文献
16.
Kyeong-Sik Shin Kyeong-Kap Paek Jung-Ho Park Tae-Song Kim Byeong-Kwon Ju Ji Yoon Kang 《Electron Device Letters, IEEE》2007,28(7):581-583
In this letter, we examined whether the parasitic bipolar junction transistors (BJTs) in the MOSFET fabricated by the standard CMOS process can play a role as a fluorescence detector. To suppress the action of two vertical parasitic BJTs, the gate and n-well were tied in the parasitic BJTs, and the body node was connected to the drain. The proposed device was compared with the inherent and the parasitic diodes in the MOSFET. It had 100 times higher photocurrents than the diodes in the MOSFET. In addition, it was applied for the detection of the fluorescent signal, and could detect near 10 nM of Alexa 546. Therefore, CMOS-process-compatible parasitic BJTs can be used as a photodetector in an integrated fluorescence detector. 相似文献
17.
纤维表面处理对植物纤维增强水泥的物理力学性能影响 总被引:2,自引:0,他引:2
植物纤维增强水泥的力学性能具有湿敏感性,随湿度增加弯曲强度下降幅度较大。本文工作采用的几种浸渍处理纤维表面的方法,有效地改善了这种状况,其中一种经处理的纤维增强水泥较没有处理的对比试样在饱水状态下的弯曲强度提高了67%,气干状态提高了18%,缩小了二者间的差距。 相似文献
18.
19.
The compacts consisted of , -Si3N4 and free silicon are heat treated in the range 1650° C to 1750° C in an argon atmosphere in order to observe the following behaviours; the to phase transformation and variations of the microstructure during heat treatment in silicon nitride. For the microstructural observation of the heat treated specimens, the same grains in the polished surface were investigated before and after eliminating the retained silicon by etching. The to phase transformation, in this case, occurs via silicon melts irrespective of added -Si3N4. Both and phases are soluted and precipitated into molten silicon and their morphology are changed from an equiaxed shape to prismatic one. Although elongated grains are precipitated at low temperature or in the early stage of heat treatment, fine precipitated grains are mainly observed with increasing heat treating temperature. 相似文献
20.