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21.
Indranil Roy Manish Chauhan Farghalli A. Mohamed Enrique J. Lavernia 《Metallurgical and Materials Transactions A》2006,37(3):721-730
Thermal stability in bulk ultrafine-grained (UFG) 5083 Al that was processed by gas atomization followed by cryomilling, consolidation,
and extrusion, and that exhibited an average grain size of 305 nm, was investigated in the temperature range of 473 to 673
K (0.55 to 0.79 T
m
, where T
m
is the melting temperature of the material) for different annealing times. Appreciable grain growth was observed at temperatures
> 573 K, whereas there was limited grain growth at temperatures < 573 K even after long annealing times. The values of the
grain growth exponent, n, deduced from the grain growth data were higher than the value of 2 predicted from elementary grain growth theories. The
discrepancy was attributed to the operation of strong pinning forces on boundaries during the annealing treatment. An examination
of the microstructure of the alloy suggests that the origin of the pinning forces is most likely related to the presence of
dispersion particles, which are mostly introduced during cryomilling. Two-grain growth regimes were identified: the low-temperature
region (<573 K) and the high-temperature region (>573 K). For temperatures lower than 573 K, the activation energy of 25 ±
5 kJ/mol was determined. It is suggested that this low activation energy represents the energy for the reordering of grain
boundaries in the UFG material. For temperatures higher than 573 K, an activation energy of 124 ± 5 kJ/mol was measured. This
value of activation energy, 124 ± 5 kJ/mol, lies between that for grain boundary diffusion and lattice diffusion in analogous
aluminum polycrystalline systems. The results show that the strength and ductility of bulk UFG 5083 Al, as obtained from tensile
tests, correlate well with substructural changes introduced in the alloy by the annealing treatment. 相似文献
22.
Uma Maheswar Rao S. S. M. S. Abdul Majeed C. Venkataseshaiah R. Sarathi 《Bulletin of Materials Science》2002,25(6):473-475
In the present work, tracking phenomena has been studied with silicone rubber material under the a.c. and d.c. voltages following
IEC-587 standards. The surface condition of the tracked zone was analysed using wide angle X-ray diffraction (WAXD) and thermogravimetric
differential thermal analysis (TG-DTA) studies. The tracking time was different for a.c. and d.c. voltages. 相似文献
23.
Mohamed Salah Foda 《Journal of the science of food and agriculture》1981,32(11):1109-1114
A fermentation procedure using wheys from buffalo milk, sweet rennet and salted wheys containing up to 15% NaC1, and based on the selection of salt-tolerant fungal cultures for production of microbial proteins and some economically important enzymes, is described. Certain strains of Aspergillus flavus, A. niger, A. ochraceus and A. terreus gave yields of mycelium ranging between 1.5 and 30 g on a dry weight basis. Strong proteolytic activities were exhibited by A. ochraceus, A. flavus and, to a lesser extent, by A. niger in the presence of salt up to 10% as final concentration. Powerful milk-clotting activities were also detected in culture supernatants of A. flavus and A. ochraceus. Extracellular β-galactosidases were released in to the culture fluids of these fungal strains with variable activities, depending upon the salt content of the growth medium. The application of the procedure is discussed. 相似文献
24.
25.
Mohamed A. Mekewi 《Materials Research Innovations》2002,6(4):214-217
Polyisobutylene succinic anhydride-urea/polyamines (PIBSA) copolymers were synthesized as potential antioxidants and detergent
dispersant agents for lubricating oils samples (SAE-30). Homogeneity, thermal stability and dispersancy of the solutions were
determined. Fully soluble oil compounds that are thermally stable up to 250 °C were achieved.
The oxidation stability of lube oil samples in the presence of four designed PIBSA additives (varying in the number of amine
groups) was determined for a time period of up to 72 hours. The dependence of the additive efficiency on its concentration
was studied to achieve maximum stability. Some PIBSA additives at concentration 3.0 · 104 ppm exhibit the best results.
Dispersivity values were measured at predetermined oxidation times. The results proved reliable dispersion capability as the
nitrogen content of the additive is increased, i.e. the increase in the basic character of the additive leads to the increase
in the neutralization capability. Moreover, the designed PIBSA additives retain their efficiency after long oxidation times,
confirming their role as multifunctional nitrogen containing polymeric additive.
Electronic Publication 相似文献
26.
Abstract. A sufficient condition for the invertibility of univariate periodic moving-average models has been given by Cipra and Ghysels and Hall. We show that this condition is not a necessary one, and provide a necessary and sufficient condition for the general m -variate, d -periodical moving-average MA( q ) case. 相似文献
27.
Maher F. El-Zohry Mohamed A. Abd-Alla 《Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)》1992,55(3):209-215
3-(2′-Chloroethyl)-2-methyl-3,4-dihydroquinazolin-4-one was reacted with acetylacetone, ethyl acetoacetate and diethylmalonate in the presence of sodium ethoxide to afford the alkylation products IV, V and VI , Compounds IV, V and VI were reacted with hydrazine hydrate, phenylhydrazine, hydroxylamine hydrochloride, urea and thiourea to yield 3-(2′-heterocyclicethyl)-2-methyl-3,4-dihydroquinazolin-4-one derivatives VII-XV . The structures of the synthesized compounds were elucidated by elemental analyses and spectroscopic (IR and XH-NMR) analyses. The prepared compounds were tested for their antimicrobial activities in comparison with tetracycline as a reference compound. 相似文献
28.
MM Mustafa 《Canadian Metallurgical Quarterly》1995,70(5):443-447
An active entomologic survey was conducted by a team of trained health workers in a rural area endemic for Chagas' disease in central Brazil. They used pyrethrum as a flushing agent and 4,232 houses were inspected for triatomine bugs both inside and in the immediate environs. Houses with Triatoma infestans or evidence of an established colony were identified and defined as infested houses (cases). The building and environmental characteristics of 161 randomly selected infested houses were compared with 161 matched, noninfested houses (controls) that were the shortest distance from the infested house. Domestic and peridomestic potential risk factors associated with house infestation by Triatoma infestans were assessed by logistic regression analysis. Incomplete house construction (odds ratio [OR] = 2.5, 95% confidence interval [CI] = 1.5-4.1) was confirmed as a risk factor related to the presence or evidence of Triatoma infestans in the dwellings. The study also disclosed a statistically significant association between the presence of rats (OR = 1.6, 95% CI = 1.1-2.6) and indoor crop storage (OR = 2.3, 95% CI = 1.1-5.2) and house infestation. Further experimental field studies using tagged rodents should be conducted to assess their epidemiologic role in the domestic chain of Trypanosoma cruzi transmission. 相似文献
29.
Mohamed Jaziri Tasnim Kossentini Kallel Souad Mbarek Boubaker Elleuch 《Polymer International》2005,54(10):1384-1391
The influence of processing conditions and interfacial modification on the morphology evolution and the composition range within which fully co‐continuous high density polyethylene/polystyrene blend structures can exist during blending in a single screw extruder was studied. Blends ranging from pure A to pure B component, with and without compatibilizer, were prepared under two different shear rates. It was found that high shear rates displaced the breakdown–coalescence balance of the dispersed nodules to the side of coalescence, narrowing the percolation domain and the critical composition for full co‐continuity decreased with increasing shear rates. The addition of a tri‐block compatibilizer induced the percolation threshold of the polystyrene phase to begin at lower percentages of polyethylene but the phase inversion point did not change. The experimental results are discussed in the light of various theoretical models. Copyright © 2005 Society of Chemical Industry 相似文献
30.
The water activities of the mixed aqueous electrolyte NaCl–BaCl2(aq) are measured at total molalities from 0.25 mol kg−1 to about saturation for different ionic strength fractions (y) of NaCl with y=0.33,0.50,0.67. The results allow the deduction of osmotic coefficients. The experimental results are compared with the predictions of the Zdanovskii, Stokes, and Robinson (ZSR), Kusik and Meissner (KM), Robinson and Stokes (RS), Lietzke and Stoughton (LSII), Reilly, Wood, and Robinson (RWR), and Pitzer models. From these measurements, the Pitzer mixing ionic parameters are determined and used to predict the solute activity coefficients in the mixture. The excess Gibbs energy is also determined. 相似文献