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61.
Hirano K. Okamura J. Taira T. Sano K. Toyoda A. Ikeda M. 《Semiconductor Manufacturing, IEEE Transactions on》2001,14(3):202-206
Developers used in photolithography contain toxic tetramethylammoniumhydroxide (TMAH) and this creates a problem of how to properly treat developer wastewater. We have developed a TMAH wastewater treatment technique that consists of a combination of two novel decomposition processes: pyrolyzing TMAH to TMA and decomposing TMA to N 2, H2O, and CO2 by means of a selective oxidation catalyst for nitrogenous compounds. We have tested a system using this technique in long-term treatment of the actual wastewater and have found it to be sufficiently practical. The running cost of a treatment system using our technique would be about one-ninth that of disposing of the wastewater as industrial waste but about 2.3 times that of biological treatment. Compared with biological treatment, however, our system is tolerant to many treatment conditions and operation management is much easier. Furthermore, it occupies only about one-sixth the area of a biological treatment system 相似文献
62.
The effects of heat-treating atmosphere on the thermal stability of low-oxygen silicon carbide fiber were investigated. Heat-treatment of EB-cured PCS fiber were conducted at 1573 K in argon, nitrogen or vacuum of 10–6 atm. Subsequently the fibers were exposed to 1873 K in argon. The strength of fibers were strongly influenced by the heat-treating atmosphere. When heat-treated in nitrogen, the fibers absorbed nitrogen. High-temperature exposure caused severe degradation of strength owing to the decomposition of silicon oxycarbonitride phase. When heat-treated in vacuum, the fiber surface was smooth and pore-free, minimizing the degradation of strength at high temperature. 相似文献
63.
Effects of the fabrication processing on the microstructure and properties of composites were investigated. High-density Ni-Co dispersed-Al2O3 (Al2O3/Ni-Co) composites were obtained by hydrogen reduction and consolidated using hot pressing and pulse electric current sintering (PECS) of Al2O3, Ni(NO3)2·6H2O and Co(NO3)2·6H2O powder mixtures. Microstructural investigations of the hot-pressed composite fabricated using again wet/dry ball-milled powder mixture after calcination revealed that fine Ni-Co particles, about 145 nm in diameter, dispersed homogeneously at the matrix grain boundaries. In particular, fine microstructure of dispersion with the average size of 90 nm was realized for the specimen consolidated by PECS method. High strength of over 1 GPa and hardness of 19 GPa were measured for the nanocomposites prepared from the again ball-milled powder mixture. The ferromagnetism of nano-sized Ni-Co contributes to the magnetic properties of the composites. A change in the coercive force with dispersion size was observed. Also, the extent of magnetic response by an applied stress was strongly influenced by the size of Ni-Co particles. The relations between microstructure and mechanical as well as magnetic properties are discussed. 相似文献
64.
65.
A newly developed magnetic regenerator material Er(Ni0.075Co0.925)2, having high specific heat at temperatures from 10 to 20 K, has been tested inside the second regenerator of a two-stage GM cryocooler. Different working conditions have been examined: four Er(Ni0.075Co0.925)2/Pb material ratios, three displacer reciprocating speeds, and two cryocooler stroke lengths. In the best working conditions, the experimental results show a cooling power improvement up to 15% over the whole temperature range from 10 to 20 K compared to that of the same GM cryocooler employing only lead. 相似文献
66.
67.
Naoya Kanbayashi Arisa Yamazawa Koichiro Takii Taka‐aki Okamura Kiyotaka Onitsuka 《Advanced Synthesis \u0026amp; Catalysis》2016,358(4):555-560
We report the asymmetric allylic alkylation of allylic chlorides with silyl enolates as a carbon nucleophile using a planar‐chiral cyclopentadienyl‐ruthenium (Cp′Ru) catalyst. The reaction proceeds under unusually mild conditions to give the desired branched products with complete regioselectivity and high enantioselectivity, and reactive functional groups, such as aldehyde, can be tolerated. In this reaction system, Cp′Ru plays an important role in activating both silyl enolate and allylic chloride.
68.
Chinatsu Okamura Takashi Ueda Kazuhiro Hasezaki 《Journal of Electronic Materials》2010,39(9):2172-2175
Single-phase β-Zn4Sb3 materials were prepared by mechanical grinding (MG). Source materials for the Zn4Sb3 ingots were prepared using three different processes after the direct melting of constituent elements. In process 1, the
ingot was obtained by quenching the melt in water within an evacuated quartz ampoule. In process 2, the ingot was heat-treated
for 100 h at 723 K after process 1. In process 3, the ingot was heat-treated for a total of 200 h in two stages at 723 K and
673 K after process 1. The resultant ingots were mechanically ground and sintered at 623 K by hot pressing. The sintered materials
were characterized by x-ray diffraction, differential thermal analysis (DTA), and thermoelectric property measurements. The
thermal conductivity of the sintered materials was 0.88 W m−1 K−1 at room temperature, being slightly lower than that reported for the materials prepared by a conventional method. Results
indicate that the dimensionless figure of merit of the single-phase β-Zn4Sb3 ranged from 1.06 to 1.31 at 573 K. 相似文献
69.
70.
Masashi Hosokawa Koretaro Takahashi Yuji Kikuchi Mutsuo Hatano 《Journal of the American Oil Chemists' Society》1995,72(11):1287-1291
Highly unsaturated fatty acid-containing phospholipids (HUFA-PL), which serve to increase the deformability of human red blood
cells, were prepared through porcine phospholipase A2-mediated esterification of the lysophosphatidylcholine, which was derived from soy phosphatidylcholine (PC), and by Lipozyme-mediated
acidolysis. Through these processes, phospholipase A2, with formamide as a water mimic, enhanced the incorporation of HUFA into positionsn-2 of PC and suppressed hydrolysis of the synthesized PL. On the other hand, Lipozyme-mediated acidolysis between positionsn-1 of soy PC and HUFA was enhanced by a combination of water and propylene glycol. Simultaneously, the recovered PL products
showed decreased hydrolysis of newly synthesized health-beneficial HUFA-PL. 相似文献