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101.
本文报道用于甲基丙烯醛(MAL)选择氧化制甲基丙烯酸(MAA)的PMoV杂多酸盐催化剂的研究结果。IR和XRD考察结果表明,本文所研究的催化剂均具有稳定的Keggin结构,催化剂物相组成为H(4-2y-2)PO4(MoO3)(12-x)(VO3)xCUyCsz。在300℃,原料气组成MAL:H2O:O2:N2=1:10:3:32.体积空速1200h(-1)的条件下,最佳催化剂的MAL转化率为94.1%,MAA选择性达88.7%。 相似文献
102.
The influence of qualitatively different nutrition (physiological and that with lysine, methionine, threonine and vitamins A, B, C deficiencies) on certain toxicokinetic parameters of 3H-aflatoxin B1, after single and multiple (every day, during 5 days) intraperitoneal injections of this agent in a dose of 25 micrograms/animal, was studied in two series of experiments on growing male WAG rats with the initial bw 40-50 g. It has been proved that the main parameters of aflatoxin B1 toxicokinetics depend on the injection multiplicity and the nutrition character. It has been established that the qualitative differences in the nutrition character essentially influence the stages of aflatoxin B1 distribution in the body, the sorption and metabolic transformation in the liver, enterohepatic recirculation, the rate and correlation of the main elimination routes. The nutrition character influences the level of persistence and cumulation of firmly bound aflatoxin B1 adducts in the liver and hepatocytic DNA. Possible mechanisms of such effects of different providing of the body with essential nutrients have been discussed. A conclusion has been made that the modifying effect of nutrition on the key stages of aflatoxin B1 toxicokinetics is realized, ultimately, in varying degree of the animal resistance to mutagenic and carcinogenic action of this agent. 相似文献
103.
We provide an explicit
stability or input-to-state stability (ISS) estimate for a sampled-data nonlinear system in terms of the
estimate for the corresponding discrete-time system and a
function describing inter-sample growth. It is quite obvious that a uniform inter-sample growth condition, plus an ISS property for the exact discrete-time model of a closed-loop system, implies uniform ISS of the sampled-data nonlinear system. Our results serve to quantify these facts by means of comparison functions. Our results can be used as an alternative to prove and extend results in [[Reference to 1]] or extend some results in [[Reference to 4]] to a class of nonlinear systems. Finally, the formulas we establish can be used as a tool for some other problems which we indicate. 相似文献
104.
The possibility of forming special fuel loads for VVER-440 that would make it possible to reduce the amount of transuranium elements in spent nuclear fuel by burning transuranium actinides is examined. Preliminary calculations are performed using the HELIOS spectral code to assess the effectiveness of the transmutation. Transmutation is modeled for two load variants: mixed uranium–plutonium oxide fuel and fuel with inert diluents. The main criterion for effective transmutation is a decrease of the mass of the transuranium elements as compared with an open fuel cycle. 相似文献
105.
1.IntroductionSputtering0fmulticomponentsolidsisaNioripreferentialbecause0fdifferenceinbindingenergy,atthesurfaceaswellasinthebulk,andenergytransferringefficiencybothbetweenaspecificat0micspecieswiththepr0jectileandwiththeenvir0nmentalat0msintargetl',']-C0nsequently,thepreferentialsputteringeffectisi0nenergyandtar-getcomp0sitiondependent.Thetransientc0mp0sitionchangeinthetargetandofthesputteredparticlesduringi0nbombardmentcanbemonit0redwithsurfacesensitiveanal-ysismethods,suchasAES,ISS,etc.… 相似文献
106.
Necla Ozdemir Yasin Ozgen Mustafa Kiralan Ali Bayrak Neşet Arslan Mohamed Fawzy Ramadan 《Sensing and Instrumentation for Food Quality and Safety》2018,12(2):820-825
Origanum onites and Origanum vulgare are important medicinal plants because of their flavoring, therapeutic, and preservative properties. Drying methods are important for obtaining high quality essential oil from spices. In this study, the effects of different drying processes on the essential oil yield, composition, and antiradical activity were evaluated. Plants were dried under sun light, in a ventilated shady place and in laboratory-type oven, and the oils were extracted with Clevenger type apparatus. Carvacrol and thymol were the major compounds in the essential oils of O. vulgare and O. onites, respectively. The highest oil yield and the highest antioxidant activity values were obtained from shade dried Origanum species followed by oven dried plants. The lowest essential oil yield and the lowest antioxidant activity for O. vulgare were found in fresh plants. The lowest essential oil yield, and the lowest antioxidant activity for O. onites belonged to sun dried plants. It could be concluded that essential oil yield, oil composition and antioxidant activity of both plants were greatly affected by the drying method. 相似文献
107.
Determination of the geographical origin of Slovenian black locust,lime and chestnut honey 总被引:1,自引:0,他引:1
Urška Kropf Mojca Korošec Jasna Bertoncelj Nives Ogrinc Marijan Nečemer Peter Kump Terezija Golob 《Food chemistry》2010
The geographical origin of three Slovenian unifloral honey types (black locust, lime and chestnut) was investigated by analysis of some physico-chemical parameters, the elemental content using total reflection X-ray fluorescence spectrometry (TXRF) and the stable carbon and nitrogen isotope ratios using isotope ratio mass spectrometry (IRMS). The results were interpreted by chemometric methods. A total of 122 samples of Slovenian black locust, lime and chestnut honeys were collected from domestic beekeepers all over Slovenia for three years. Slovenia is a small country by area, but paedologically and climatically diverse, therefore offering interesting possibilities for studying geographical influences. The combination of the investigated parameters offers the possibility of distinguishing among samples of specific honey types from the four different Slovenian natural-geographical macroregions, namely the Alpine, Dinaric, Pannonnian and Mediterranean regions. Lime honey samples were 100% correctly classified, while the success rates for black locust and chestnut honeys were slightly lower at 98.2% and 94.6%, respectively. 相似文献
108.
In this work the program AMPS-1D was used to optimize the performance of the organic solar cells. The cells considered consist of poly(3-HexylThiophène) [P3HT] as electron donors, and (6,6)-phenyl- C61-butyric acid methyl ester [PCBM] as electron acceptor, (P3HT/PCBM) is used as photo-active material, sandwiched between a transparent indium tin oxide (ITO) and layer of poly(3,4 ethylenedioxythiophene)/ poly(styrenesulfonate) (PEDOT/PSS) on top of the ITO electrode and an AL backside contact. The results showed that the optimum thickness of the solar cell is about 400 nm, Voc = 0.61 at T = 300 K. This is in the good agreement with the corresponding computer simulation value of 0.63 V. The maximum limit for the organic solar cell efficiency is about 8%, provided that the band-gap of the cell is about 1.5 eV. 相似文献
109.
110.
Human milk fat analogues containing stearidonic acid (SDA) were produced by enzymatic acidolysis reactions between tripalmitin and free fatty acids (FFA) obtained from hazelnut oil and commercial oil mixture containing Echium oil. Lipozyme® TL IM, immobilized sn-1,3 specific lipase was used in the enzymatic reactions. Response surface methodology (RSM) was applied by using central composite circumscribed design with five levels and three factors. The factors chosen were: Reaction temperature [55–65 °C], reaction time [4–12 h] and substrate molar ratio [3–5 mol/mol (total FFA/tripalmitin)]. Good quadratic models were obtained for the incorporation of SDA and oleic acid. Optimal conditions generated from the models were determined as 60 °C; 8 h, 4 mol/mol for temperature, time and substrate molar ratio, respectively. The models were verified at optimum conditions and furthermore scale-up synthesis of structured lipids (SLs) was performed. Stearidonic and oleic acid contents of the SL from scale-up production were found to be 2.0 and 22.9 mol/100 mol total FA respectively, with 46.2 mol/100 mol total FA of palmitic acid content located at sn-2 position. Besides, oxidative stability and melting profile of final SL were determined for characterization. SL had 6.1 h of induction time, and also had a wider melting range compared with tripalmitin. 相似文献