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31.
Andreea Groza Simona Liliana Iconaru Gabriel Jiga Patrick Chapon Sofia Gaiaschi Nicolae Verga Mircea Beuran Alina Mihaela Prodan Mihai Matei Serban Andrei Marinescu Roxana Trusca Daniela Predoi 《Polymer Engineering and Science》2019,59(12):2406-2412
The bio hydroxyapatite (HAp) was used from a long time in different medical and environmental applications. The HAp layers with a uniform surface were used for various medical applications such as orthopedic and dental metal implants. In this work, we reported on the influence of X‐ray radiation on the structural and morphological properties of composite layers based on HAp and polydimethylsiloxane (PDMS) deposited on titanium substrates. The HAp:PDMS layers were investigated by different complementary methods such as scanning electron microscopy (SEM), Fourier transform infrared spectroscopy (FTIR), and glow discharge optical emission spectrometry (GDOES). FTIR spectral analysis showed that the molecular structure of the coatings was not changed after their irradiation even though, the depth profile analysis performed by GDOES indicated a depletion of Ca and P elements from the HAp:PDMS irradiated samples. By SEM, we showed that the morphological features of the coatings were also changed, as the irradiated layers are delaminated. The biological assays confirmed that the antibacterial activity of HAp:PDMS composite layers increased after irradiation. The results obtained in this study highlighted that the biological properties of HAp:PDMS layers could be influenced by irradiation. POLYM. ENG. SCI., 59:2406–2412, 2019. © 2019 Society of Plastics Engineers 相似文献
32.
Daniela Cristina Culita Claudia Maria Simonescu Rodica Elena Patescu Silviu Preda Nicolae Stanica Cornel Munteanu Ovidiu Oprea 《Journal of Inorganic and Organometallic Polymers and Materials》2017,27(2):490-502
Three novel magnetic adsorbents were synthesized through the immobilization of di-, tri-, and tetraamine onto the surface of silica coated magnetite nanoparticles. The adsorbents were characterized by XRD patterns, FTIR spectroscopy, elemental and thermogravimetric analysis, magnetic measurements, SEM/TEM, EDX spectroscopy, and N2 adsorption/desorption isotherms. Their capacity to remove copper ions from aqueous solutions was investigated and discussed comparatively. The equilibrium data were analyzed using Langmuir and Freundlich isotherms. The kinetics was evaluated using the pseudo-first-order, pseudo-second-order, and intra-particle diffusion models. The best interpretation for the equilibrium data was given by the Langmuir isotherm for the tri- and tetraamine functionalized adsorbents, while for the diamine functionalized adsorbent the Freundlich model seemed to be better. The kinetic data were well fitted to the pseudo-second-order model. The overall rate of adsorption was significantly influenced by external mass transfer and intraparticle diffusion. It was observed that the adsorption capacity at room temperature decreased as the length of polyamine chain immobilized on the adsorbent surface increased, the maximum adsorption capacities being 52.3 mg g?1 for 1,3-diaminopropan functionalized adsorbent, 44.2 mg g?1 for diethylenetriamine functionalized adsorbent, and 39.2 mg g?1 for triethylenetetramine functionalized adsorbent. The sorption process proved to be highly dependent of pH. The results of the present work recommend these materials as potential candidates for copper removal from aqueous solutions. 相似文献
33.
Rodinel Ardeleanu Anton Airinei Gabriela Sacarescu Liviu Sacarescu Nicolae Voiculescu 《大分子材料与工程》2002,287(9):597-603
The complexation ability of some linear crown ether‐siloxane copolymers of ester or amide type with cations as K+ and NH4+ was investigated spectrophotometrically in order to select the polysiloxane receptors that achieve good ion transport ability by bulk liquid membrane systems. The transport properties of the potassium picrate through a liquid membrane using siloxane‐crown ether polyamide as carrier were discussed. 相似文献
34.
Adrian BirtasIulian Voicu Cristian PetcuRadu Chiriac Nicolae Apostolescu 《International Journal of Hydrogen Energy》2011,36(18):12007-12014
Extensive studies have been dedicated in the last decade to the possibility to use hydrogen in the dual-fuel mode to improve combustion characteristics and emissions of a diesel engine. The results of these studies, using pure hydrogen or hydrogen containing gas produced through water electrolysis, are notably different.The present investigation was conducted on a tractor diesel engine running with small amounts of the gas—provided by a water electrolyzer—aspirated in the air stream inducted in the cylinder. The engine was operated at light and medium loads and various speeds.It was found that the addition of HRG gas has a slight negative impact, up to 2%, on the engine brake thermal efficiency. Smoke is significantly reduced, up to 30%, with HRG enrichment, while NOx concentrations vary in both senses, up to 14%, depending on the engine operation mode. A relative small amount of HRG gas can be used with favorable effects on emissions and with a small penalty in thermal efficiency. 相似文献
35.
36.
Tanta‐Verona Nicolescu Andrei Sarbu Stefan Ovidiu Dima Cristian Nicolae Dan Donescu 《应用聚合物科学杂志》2013,127(1):366-374
We report the synthesis of molecularly imprinted sorbents, selective for gallic acid. The particles were prepared by using acrylic acid, acrylonitrile, and hydroxyethyl methacrylate as functional monomers, whereas ethyleneglycol dimethacrylate and 1,4‐buthanediol dimethacrylate were used as crosslinkers. Preparation and manipulation protocols were adjusted considering template's nature. To highlight the influence of monomer/crosslinker nature upon imprinted particles, the adsorption capacity, the imprinting factor, and the distribution and selectivity coefficients were calculated. An imprinting factor of 3.53 and a selectivity coefficient of 6.86 were found for hydroxyethyl methacrylate/ethylene glycol methacrylate system. © 2012 Wiley Periodicals, Inc. J Appl Polym Sci. 2013 相似文献
37.
Dragos Nicolae Vizireanu 《International Journal of Electronics》2013,100(11):1175-1181
The principles for the development of portable instrumentation equipment (multimeters, frequency meters, etc.) using quantised sine signals, with a common unknown fixed frequency, and an estimation algorithm implemented on digital signal processors (DSPs) are described. An unknown internal sine signal is generated. For measurements, analog to digital converters (ADCs) acquire multiple samples of sine signals, which are quantised and transmitted to the DSP. A precise quantised sine signal, with a common unknown fixed frequency, signal estimation algorithm, for DSP-based instrumentation, is presented. An iterative process is performed to obtain amplitudes, phases, dc components, common frequency and to control the ADC number of bits. Final solutions depend on the initial values, obtained using different classical estimation algorithms. The accuracy of the initial values of iterations and the number of used points have a large influence on the speed of convergence. The algorithm stops when quantisation conditions are satisfied. 相似文献
38.
In this article we introduce a new public digital watermarking technique for video copyright protection working in the discrete wavelet transform domain. The scheme uses binary images as watermarks. These are embedded in the detail wavelet coefficients of the middle wavelet sub-bands. The method is a combination of spread spectrum and quantisation-based watermarking. Every bit of the watermark is spread over a number of wavelet coefficients with the use of a secret key. The resilience of the watermarking algorithm was tested against a series of eight different attacks using different videos. To improve the resilience of the algorithm we use error correction codes and embed the watermark with spatial and temporal redundancy. The proposed method achieves a very good perceptual quality with mean peak signal-to-noise ratio values of the watermarked videos of more than 40 dB and high resistance to a large spectrum of attacks. 相似文献
39.
We consider one of the newest analytical methods, the Optimal Homotopy Asymptotic Method (OHAM), to solve nonlinear equations arising in heat transfer. Two specific applications are considered: cooling of a lumped system with variable specific heat and the temperature distribution equation in a thick rectangular fin radiation to free space. Results obtained by OHAM, which does not need small parameters are compared with numerical results and a very good agreement was found. This method provides us with a convenient way to control the convergence of approximation series and adjust convergence regions when necessary. The results reveal that the proposed method is explicit, effective and easy to use. 相似文献
40.
Narad Rampersad Nicolae Santean Jeffrey Shallit Bala Ravikumar 《Theoretical computer science》2009,410(24-25):2431-2441
For each basic language operation we define its “unique” counterpart as being the operation that results in a language whose words can be obtained uniquely through the given operation. These unique operations can arguably be viewed as combined basic operations, placing this work in the popular area of state complexity of combined operations on regular languages. We study the state complexity of unique rational operations and we provide upper bounds and empirical results meant to cast light into this matter. Equally important, we hope to have provided a generic methodology for estimating their state complexity. 相似文献