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101.
H. S. Tripathi B. Mukherjee S. Das M. K. Haldar S. K. Das A. Ghosh 《Ceramics International》2003,29(8):915-918
Stoichiometric magnesium aluminate spinel was synthesized by reaction sintering of alumina with caustic and sintered magnesia. The volume expansion of 5–7% during MgAl2O4 formation was utilized to identify the starting temperature of spinel formation and densification by high temperature dilatometry. The magnesia reactivity was determined by measurement of crystallite size and specific surface area. Caustic magnesia and sintered magnesia behave differently vis-à-vis phase formation and densification of spinel. Densification of stoichiometric Mag-Al spinel was carried out between 1650 and 1750 °C. Attempts were made to correlate the MgO reactivity with microstructure and densification of spinel. 相似文献
102.
Low temperature steam reforming of ethanol in the temperature range of 200–360°C was studied to maximize the production of H2. The optimum reaction conditions in presence of a suitable catalyst can produce mainly the desired products H2 and CO2. Cu/Al2O3 catalysts with six different concentrations ranging from 0 to 10 wt.% Mn, were prepared, characterized and studied for the ethanol-steam reforming reaction. Maximum ethanol conversion of 60.7% and hydrogen yield of 3.74 (mol H2 / mol ethanol converted) were observed at 360°C for catalyst with 2.5 wt.% Mn loading. 相似文献
103.
The use of tetravalent ceric ions to initiate graft-copolymerization of methyl methacrylate onto natural rubber (NR) has been investigated. The rate of grafting has been determined by varying the concentration of monomer and cerium(IV), the temperature and the solvents. The graft yield increases with increasing monomer concentration up to 1.877 M, with further increase of the monomer, the graft yield decreases. The percentage of grafting increases with increasing cerium(IV) concentration up to 0.035 M, thereafter it decreases. With increasing temperature the graft yield increases. The effect of CuSO4 on the rate of grafting has also been investigated. A plausible mechanism has been suggested and the kinetic rate expressions have been derived. 相似文献
104.
The viscosity and apparent molar volume of solutions of KBrO3, NaBrO3 KIO3, NaIO3, K2SO4 and Na2SO4 in dioxane (mass fraction: 10, 20 and 30%)-water mixtures at 30, 35, 40 and 45°C have been measured. The ions appear to interact appreciably and the ion-solvent interaction is of the order BrO?3 > IO?3 > SO2?4 and K+ > Na+. 相似文献
105.
Full and semi-IPNs were prepared from epoxy and poly methyl methacrylate (PMMA), by the sequential mode of synthesis and were characterized by measurements of ultimate tensile strength (UTS), elongation at break, modulus, and toughness. Aromatic polyamine adducts and ethylene glycol dimethacrylate were used as the crosslinkers for epoxy and comonomer/crosslinker for methyl methacrylate monomer, respectively. Higher UTS and modulus of the semi-IPNs over full IPNs were attributed to the higher probability of interpenetration. The weight retention in the thermal decomposition of the IPNs and semi-IPNs were higher than the epoxy homopolymer. This enhancement was presumably related to the presence of the unzipped methyl methacrylate monomer which acted as radical scavangers in the epoxy degradation. © 1994 John Wiley & Sons, Inc. 相似文献
106.
Chinmoy Saha Siva Ponnupandian Francis R. Costa Gert Heinrich Nikhil K. Singha 《Polymer Engineering and Science》2021,61(12):3163-3169
This investigation reports the synthesis of a new class of polyurethane (PU) based on bis(hydroxyalkyl) polydimethylsiloxane (PDMS) as diol and isophorone diisocyanate as diisocyanate followed by the preparation of PU/layered double hydroxide (PU/LDH) nanocomposite via ex-situ technique. Nuclear magnetic resonance and Fourier-transform infrared spectroscopy studies confirm the formation of PU and incorporation of PDMS into the PU backbone. Thermogravimetry analysis revealed that thermal stability of the composite improves significantly with incorporation of LDH into the PU matrix. This may be accredited to the barrier effect rendered by the LDH layers. Differential scanning calorimetry study reveals that with the incorporation of LDH, glass transition temperature (Tg) of the composite increases for an optimum level of loading beyond which it remains constant. 相似文献
107.
S. K. Albert C. R. Das V. Ramasubbu A. K. Bhaduri S. K. Ray Baldev Raj 《Journal of Materials Engineering and Performance》2002,11(3):243-249
A root-cracked blade in a high-pressure steam turbine of a nuclear power plant had to be replaced with a new blade by cutting
the shroud to remove the cracked blade. This necessitated in situ welding of a new shroud piece with the existing shroud after
the blade replacement. The in situ welding of the shroud, a 12% Cr martensitic stainless steel with tempered martensite microstructure,
was carried out using gastungsten arc welding and 316L austenitic stainless steel filler metal followed by localized postweld
heat treatment at 873 K for 1 h using a specially designed electrical resistance-heating furnace. Mock-up trials were carried
out to ensure that sound welds could be made under the constraints present during the in situ repair welding operation. In
situ metallography of the repair weld after postweld heat treatment confirmed the adequate tempering of the martensitic structure
in the heat-affected zone. Metallurgical investigations carried out in the laboratory on a shroud test-piece that had been
welded using the same procedure as employed in the field confirmed the success of the in situ repair operation. The alternate
option available was replacing the cracked blade and the shroud piece to which it is riveted with a new one, reducing the
height of all the blades attached to the shroud by machining, riveting the blades with reduced height to the new shroud, and,
finally, dynamic balancing of the entire turbine after completion of the repair. This option is both time-consuming and expensive.
Hence, the successful completion of this repair welding resulted in enormous savings both in terms of reducing the downtime
of the plant and the cost of the repair. The turbine has been put back into service and has been operating satisfactorily
since December 2000. 相似文献
108.
Galvannealed coating of high strength interstitial free (IF-HS) steel was characterised by Glow Discharge Optical Emission Spectroscopy (GDOES) and colour-etching techniques. Overalloyed galvannealed coatings with considerably high amount of Γ and Γ1 phases were detected in the first set of experiments. Necessary process modifications in galvannealing furnace were made to maximise the ä phase in the galvannealed coating, which was confirmed through GDOES and colour-etching techniques. As a result, an improvement in galvannealed product quality with a better powdering resistance property during forming has been achieved. 相似文献
109.
Dual polarized triple band hybrid MIMO cylindrical dielectric resonator antenna for LTE2500/WLAN/WiMAX applications 下载免费PDF全文
In this communication, triple band hybrid multi‐input–multi‐output (MIMO) cylindrical dielectric resonator antenna (CDRA) with high isolation is examined. The proposed MIMO antenna includes two symmetric folded microstrip line feeding structures along with CDRA at two different ends of substrate. Two inverted L‐shaped strips on the ground plane are used to enhance the isolation (S12 < ?15 dB) as well as to generates 2.7 GHz frequency band. Metallic strip on the ground plane act as an electromagnetic reflector and also enhance the isolation between two antennas (S12 < ?20 dB). Archetype of proposed MIMO antenna design has been fabricated and tested to validate the simulated results. The proposed antenna operates at three different frequency bands 2.24–2.38 GHz, 2.5–3.26 GHz, and 4.88–7.0 GHz (S11 < ?6 dB) with the fractional bandwidth 6.06%, 26.4%, and 35.7%, respectively. Folded microstrip lines generate path delay between the electric field lines and originate circular polarization characteristics in the frequency range 5.55–5.75 GHz with the fractional bandwidth of 3.55%. In order to satisfy the different performance requirement of MIMO antenna such as envelop correlation coefficient, mean effective gain, effective diversity gain, peak gain are also examined. The proposed antenna is found suitable for LTE2500, WLAN, and WiMAX applications. © 2016 Wiley Periodicals, Inc. Int J RF and Microwave CAE, 2016. 相似文献
110.
Badal Soni Saswati Debnath Pradip K. Das 《International Journal of Speech Technology》2016,19(3):525-536
An important task of speaker verification is to generate speaker specific models and match an input speaker’s utterance with these models. This paper focuses on comparing the performance of text dependent speaker verification system using Mel Frequency Cepstral Coefficients feature and different Vector Quantization (VQ) based speaker modelling techniques to generate the speaker specific models. Speaker-specific information is mainly represented by spectral features and using these features we have developed the model which serves as an important entity for determining the claimed identity of the speaker. In the modelling part, we used Linde, Buzo, Gray (LBG) VQ, proposed adaptive LBG VQ and Fuzzy C Means (FCM) VQ for generating speaker specific model. The experimental results that are performed on microphonic database shows that accuracy significantly depends on the size of the codebook in all VQ techniques, and on FCM VQ accuracy also depend on the value of learning parameter of the objective function. Experiment results shows that how the accuracy of speaker verification system is depend on different representations of the codebook, different size of codebook in VQ modelling techniques and learning parameter in FCM VQ. 相似文献