Stoichiometric dye-binding procedure for the determination of the reactive lysine content of soya bean protein

A new analytical method has been developed for the determination of the reactive lysine content of soya bean protein. The method is based on the reaction of the free basic groups of the protein with 1-phenylazo-2 naphthol-6,8 disulphonic acid. With regard to the stoichiometry of the procedure, it has been proved, contrary to earlier reports, that the basic amino acids, histidine, arginine and lysine, each combine with one mole of the dye. After acylation with propionic anhydride lysine alone loses its dye reactivity. The usefulness of the proposed method has been demonstrated by the determination of the reactive lysine content of several untreated, heat-treated and acid-treated soya bean samples. The results show that heat damage of about 5% in reactive lysine content can be measured in 1·5 h with good reproducibility.     

A variational principle for magneto-elastic buckling

A variational principle that can serve as the basis for a magneto-elastic stability (or buckling) problem is constructed. For the two cases of soft ferromagnetic media and superconductors, respectively, it is shown how the variational principle directly yields an explicit expression for the buckling value. The formulation starts from a specific choice for a magneto-elastic Lagrangian L (associated with the so-called Maxwell-Minkowski model for magneto-elastic interactions). For the evaluation of the principle the first and second variations of L are calculated both inside and outside the solid magneto-elastic body. Thus, a general buckling criterion, consisting of an expression for the critical field value, together with a set of constraints for the field variables occurring in the right-hand side of this expression, is constructed. Finally, more detailed formulations are given for, successively, soft ferromagnetic bodies and superconductors. Applications to specific structures, yielding explicit numerical values for the magneto-elastic buckling fields, will be given in a forthcoming paper.     

On Woolfolk and Richardson.

Comments on R. L. Woolfolk and F. C. Richardson's (see record 1985-12614-001) discussion of the ideology of behavior therapy and their argument that behavior therapy cannot develop a conception of what might be appropriate goals of treatment. The present author contends that goals are as much a scientific question as are questions of technique. A scientific approach to the study of goal selection is presented that can be applied to any type of adjustment problem. (8 ref) (PsycINFO Database Record (c) 2010 APA, all rights reserved)     

Interconnection of Subsystem Reduced-Order Models in the Electrothermal Analysis of Large Systems

Heat conduction in an electronic device is commonly modeled as a discretized thermal system (e.g., finite element or finite difference models) that typically uses large matrices for solving complex problems. The large size of electronic-system heat transfer models can be reduced using model reduction methods and the resulting reduced-order models can yield accurate results with far less computational costs. Electronic devices are typically composed of components, like chips, printed circuit boards, and heat sinks that are coupled together. There are two ways of creating reduced-order models for devices that have many coupled components. The first way is to create a single reduced-order model of the entire device. The second way is to interconnect reduced-order models of the components that constitute the device. The second choice (which we call the "reduce then interconnect" approach) allows the heat transfer specialist to perform quick simulations of different architectures of the device by using a library of reduced-order models of the different components that make up the device. However, interconnecting reduced-order models in a straightforward manner can result in unstable behavior. The purpose of this paper is two-fold: creating reduced-order models of the components using a Krylov subspace algorithm and interconnecting the reduced-order models in a stable manner using concepts from control theory. In this paper, we explain the logic behind the "reduce then interconnect" approach, formulate a control-theoretic method for it, and finally exhibit the whole process numerically, by applying it to an example heat conduction problem     

On the hypoelastic-idealplastic constitutive model

Summary Recently, the hypoelastic-idealplastic solid under simple shear has been studied. As an unexpected result, the slope of the stress-strain curve at the beginning of the plastic range turned out to be negative. While all other assumptions remained the same, this effect was recognized for all objective stress rates, which have been used for the hypoelastic constitutive law.The main objective of this paper is an interpretation of this remarkable result, where this interpretation should be given in an acceptable and rational form. To this end, we apply the constitutive assumption of the elastic-idealplastic body for comparison.With 1 Figures     

Development of a simple low-cost solar simulator for indoor collector testing

Indoor test methods for solar collectors are widely accepted and recommended by ASHRAE. The development of a solar simulator for indoor testing and the certification procedure for photo-thermal solar devices is discussed in this paper. The system consists of 14 quartz halogen lamps and provides a testing area of about 1 × 1 m. The irradiance can be varied from 400 to 1500 W/m². This is achieved by varying the input power supplied to individual lamps. The radiation output characteristics of a single lamp have been studied. The distribution of intensity over the covered area of 1·20 × 1·20 m has been recorded using a precision Eppley pyranometer.A variety of collectors—evacuated tubular collectors and flat-plate collectors of both liquid and air heating types—has been tested under sufficiently stable insolation conditions. Results for a conventional solar air heater are presented together with suggestions for further improvements.     

Analysis of the high-frequency spectrum of acoustic emission signals and its relationship to the wear resistance of filled polytetrafluoroethylene

We have performed tribotechnical tests of carbonaceous filled polytetrafluoroethylene in a wide range of loads with the recording of acoustic emission signals. Based on a spectral analysis of the sequence of rms deviations of acoustic emission signals using a discrete Fourier transform, we have constructed a normalized energy spectrum. We show that the mass wear of the material can be determined from the power of the high-frequency component of the spectrum obtained.