Novel application of nanocrystalline nickel electrodeposit: Making good diamond tools easily, efficiently and economically

Electrodeposition has been identified as a feasible and economical technique for nanomaterials application. This article details an improved approach to producing better diamond tools at lower cost and with higher productivity. Pulse-electroformed nanocrystalline nickel was used as the new matrix. The pulse parameters were determined after examination of the microstructure, grain size, hardness and tensile strength of the deposits obtained at different average current densities (J_m) with constant pulse-on time and pulse-off time. It is shown that, with J_m ranging from 1 Adm^− 2 to 14 Adm^− 2, the grain size decreases sharply from 180 nm to about 10 nm while the hardness and tensile strength significantly increase at first and then reach their peaks respectively, although the strength fails to stay long. Current density J_m that produced the highest hardness and strength of deposit (with grain size of 20 nm) was chosen for new diamond tools that exhibited 20.2% longer service life than their usual Ni-Co counterparts. Therefore, nanocrystalline electrodeposits are expected to be an upgrading substitute for conventional polycrystalline matrix.     

用微量元素涂料改善球铁件热节组织的试验研究

对RE、Tc、Bi、Sb等微量元素以涂料形式对球铁件厚大热节部位进行微合金化,以改善其组织的可能性进行了试验研究,结果表明:多元微量元素涂料可有效地消除碎块状石墨,提高球化率,改善球铁组织,涂料层厚度影响微合金化程度而应严格控制,该工艺具有简便。无炉料污染、可代替冷铁以确保复杂铸件组织均一等优点。     

工艺因素对82B钢280 mm x325 mm铸坯凝固过程的影响

为模拟不同工艺条件下的连铸坯的凝固过程,采用有限元法模拟了82B钢连铸的凝固过程,获得280 mm×325 mm连铸坯的温度场。结果表明,随拉速从0.60 m/min增加到0.76 m/min,凝固时f_s=1处与f_s=0处皆后移,但中心凝固时间反而增加了9.8%。随过热度由15℃增加到50℃时,凝固末端f_s=1处同样后移,约后移1.1 m。根据模拟结果改进连铸工艺,当拉速从0.60 m/min增加到0.76m/min,增加轻压下工艺可改善低倍质量。     

顶头形状对穿孔毛管壁厚均匀性及能耗影响的研究

针对目前穿孔顶头形状研究所存在的问题,在实验室内就提高一次穿孔毛管的壁厚均匀性及降低能耗进行了系统的试验研究,初步研制成功一种新型的平头对心顶头。     

聚丙烯纤维水相异相接枝马来酸酐

本文研究了用水相异相法在聚丙烯纤维上接枝马来酸酐，用称重法测定接枝率，结果认为，随着反应中使用的马来酸酐和过硫酸铵浓度的提高，所得产物的接枝率显著提高，而反应温度和反应时间的影响则是开始随温度升高和时间延长接枝率上升，达到最大值后下降，在本实验中，各种反应条件下，都可以得到超过1．8％的接枝率。     

GPU accelerated online multi-particle beam dynamics simulator for ion linear particle accelerators

An online beam dynamics simulator is being developed for use in the operation of an ion linear particle accelerator. By employing Graphics Processing Unit (GPU) technology, the performance of the simulator has been significantly increased over that of a single CPU and is therefore viable in the demanding accelerator operations environment. Once connected to the accelerator control system, it can rapidly respond to any control set point changes and predict beam properties along an ion linear accelerator in pseudo-real time. This simulator will be a virtual beam diagnostic tool which is especially useful when direct beam measurements are not available. Details about the code structure design, physics algorithms, GPU implementations, and performance are presented.     

Electrosyntheses and characterization of poly(5‐bromoindole) in boron trifluoride diethyl etherate

Poly(5‐bromoindole) (PBrI) films were synthesized electrochemically by direct oxidation of 5‐bromoindole in pure boron trifluoride diethyl etherate. The oxidation potential of 5‐bromoindole in this medium was measured to be only 0.97 V vs. saturated calomel electrode, which was lower than that determined in acetonitrile + 0.1 mol L^?1 Bu₄NBF₄ (1.08 V). PBrI films obtained from this medium showed good electrochemical behavior and good thermal stability. Structural studies showed that the polymerization of 5‐bromoindole ring occurred at 2,3 position. As‐formed PBrI films were thoroughly soluble in strong polar solvent dimethylsulfoxide and partly soluble in tetrahydrofuran. Fluorescent spectral studies indicated that PBrI was a good blue‐light emitter. The excitation and emission spectra of PBrI showed a significant shift to longer wavelength compared with that of the monomer, consistent with the greater extent of electron delocalization. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 101: 539–547, 2006     

Efective Error-Tolerant Keyword Search for Secure Cloud Computing简

The existing solutions to keyword search in the cloud can be divided into two categories： searching on exact keywords and searching on error-tolerant keywords. An error-tolerant keyword search scheme permits to make searches on encrypted data with only an approximation of some keyword. The scheme is suitable to the case where users＇ searching input might not exactly match those pre-set keywords. In this paper, we first present a general framework for searching on error-tolerant keywords. Then we propose a concrete scheme, based on a fuzzy extractor, which is proved secure against an adaptive adversary under well-defined security definition. The scheme is suitable for all similarity metrics including Hamming distance, edit distance, and set difference. It does not require the user to construct or store anything in advance, other than the key used to calculate the trapdoor of keywords and the key to encrypt data documents. Thus, our scheme tremendously eases the users＇ burden. What is more, our scheme is able to transform the servers＇ searching for error-tolerant keywords on ciphertexts to the searching for exact keywords on plaintexts. The server can use any existing approaches of exact keywords search to search plaintexts on an index table.     

风机及泵用差动调速装置的节能效果分析

差动调速装置是一种适用于大中型风机及泵类的高效节能传动装置,它能有效调节风机及泵的流量或使其运行于高效工作区。该装置具有调速方便、效率高、节能效果显著、造价低、可靠性高等一系列优点。     

杂多化合物催化剂在精细化工合成中的应用

本文综术了杂多化合物作为酸催化剂，催化烷基化和去烷基化反应、缩聚反应、水合和失水、酯化和醚化反应；以及作为氧化催化剂，在烯烃、芳烃、酚的氧化和环氧化反应中的应用。表面杂多化合物作为催化剂在合成精细化学中有广泛的应用价值。