An automatic procedure for the synthesis and optimization of very low-frequency Gm–C integrators

Fully integrated low frequency filters are critical cells that should be carefully designed in order to avoid excessive area occupation. In this work we propose an automatic procedure capable of optimizing the design of G_m?CC integrators, which constitute the basis of a wide class of G_m?CC filters. The optimization target is minimizing the cell area with constraints on input range and low frequency noise. Lower and upper bounds can be fixed to most quantities and design parameters in order to avoid solutions that are not compatible with the physical limitations of the process. The program has been developed within the MATLAB^? platform, exploiting the optimization toolbox. The effect of several important design parameters on the optimization of low frequency integrators has been investigated using the proposed routine. The strong interaction between noise and low frequency constraints has been demonstrated, showing the impressive impact of strict noise specifications on the occupied area. The actual effectiveness of parameters such as the current division factor or approaches such as flicker noise rejection by means of chopper modulation has been investigated. Examples of integrator synthesis, performed using the proposed procedure configured with the parameters of a commercial CMOS process, are presented. The consistence between the characteristics of the cells and the initial specifications has been checked using electrical simulations showing a maximum discrepancy with the initial specifications of nearly 80%. A semi-manual method to refine the synthesized cells and improve the accuracy is proposed.     

A systematic method for predetermined scanning electron microscope analysis in dental science

Scanning electron microscope evaluation could be criticized if the method adopted to correct for bias is not specified in the study design. Observers can draw conclusions from images unconsciously chosen to best support their research hypotheses, impairing the basic research principle of operator's impartiality. In this study, a systematic observation method has been described and verified for repeatability. The number and the observation points on a certain specimen have been predetermined using a scheme along with observation rules previously established in the research protocol. When our instrument is used at an operating magnification between 500× and 1,000× (corresponding to a frame of 250×190 µ and 120×90 µ, respectively), the method allowed 100% repeatable observation frames, with linear frame errors in finding an observation point of 12.5% in length and 16.8% in height. With modifications to accommodate research objective and statistical requirements, the method could be applied to many SEM observation study. SCANNING 32: 97–103, 2010. © 2010 Wiley Periodicals, Inc.     

Personal multimedia services over a common home and access networking environment

This article presents a new end-to-end architecture model that will enable the deployment of a plethora of different multimedia services from diverse suppliers competitively coexisting over a common access and home networking environment. The model is focused on personal multimedia communication services and terminals. The proposed model is a segmentation of the end-to-end multimedia chain into several business segments. The interfaces among segments and functional entities inside each segment are identified and defined in the work. In order to study the impact level of the results achieved, a comparison with the approximation to NGN provided by current standardization bodies in the field (3GPP and TISPAN) is also included in the article. This comparison highlights the advantages of using this model as a solution to offer PMC services.     

Recovery of anthocyanins from eggplant peel

Tartaric and malic acid solutions were tested to extract anthocyanins from eggplant peel by a discontinuous process to obtain a natural red colorant. Extraction optimization was carried out, using different solvents, acid concentration, temperature, time of extraction and solvent-to-solid ratio as independent variables. Tartaric acid was more efficient than malic acid in both extraction yield and rate. Comparative tests were carried out using acidified ethanol as solvent. Delphinidin-3-rutinoside was extracted and identified as the major anthocyanin in eggplant peel. Concentration of different extracts from eggplant peel was carried out using EXA-31, a methacrylic food grade resin, the best performing resin to obtain highly concentrated extracts.     

Mechanical properties and morphology of papers prepared from single-walled carbon nanotubes functionalized with aromatic amides

Carbon nanotube papers (CNT papers, also referred to as “buckypapers”) prepared from chemically functionalized single-walled CNTs are being investigated for their mechanical tensile properties. While the Young’s moduli are unaffected by the functionalization with diazonium salts of aniline or aromatic mono- and bis-amides tensile strengths of CNT papers are found to increase with a growing degree of functionalization, and more pronounced with a growing number of amide groups capable of hydrogen bonding. The importance of hydrogen bonding becomes evident after its inhibition through N-methylation of the amide groups, resulting in a distinct reduction of strength values. Scanning electron micrography indicates that a high degree of functionalization or a high number of amide group results in the formation of domains with aligned CNTs.     

Fully Automatic Visualisation of Overlapping Sets

Visualisation of taxonomies and sets has recently become an active area of research. Many application fields now require more than a strict classification of elements into a hierarchy tree. Euler diagrams, one of the most natural ways of depicting intersecting sets, may provide a solution to these problems.
In this paper, we present an approach for the automatic generation of Euler-like diagrams. This algorithm differs from previous approaches in that it has no undrawable instances of input, allowing it to be used in systems where the output is always required. We also improve the readability of Euler diagrams through the use of Bézier curves and transparent coloured textures. Our approach has been implemented using the Tulip platform. Both the source and executable program used to generate the results are freely available.     

Enhanced field induced martensitic phase transition and magnetocaloric effect in Ni55Mn20Ga25 metallic foams

The high surface/volume ratio and mechanical stability under cyclic strain makes polycrystalline Ni–Mn–Ga metallic foams attractive for magnetic refrigeration. By means of comparison with a polycrystalline bulk material, we have demonstrated that the porous structure of Ni_54.8Mn_20.2Ga_25.0 open-cells metallic foams (porosity varying between 44% and 58%) reduces the temperature span of the phase transition and increases the magnetocaloric effect (MCE). MCE was investigated using calorimetry in a magnetic field. Temperature scan and isothermal experiments have shown a 0.8 K T^?1 shift of the phase transition temperature and a maximum irreversible entropy change of 2.5 Jkg^?1 K^?1. The results indicate that metallic foams can represent a good approach for enhancing field induced phase transitions in magnetic refrigeration applications.