Epifluorescence microscopy study of a quadruple node of triple junctions of grain boundaries in a Eu2+‐doped Kcl:Kbr solid solution by using the doping ion as a fluorochrome

A typical quadruple node (QN) of triple junctions (TJs) of grain boundaries (GBs) in a Eu²⁺‐doped KCl_0.52Br_0.48 solid solution is investigated from the geometrical point of view by epifluorescence microscopy using the doping ion as a fluorochrome. The excitation and fluorescence optical properties of the fluorochrome were previously characterised by spectrophotometry whereas the structural nature of the studied material as well as its Bravais lattice type, unit cell size and long‐range translational order degree was determined by X‐ray diffraction. A three‐dimensional reconstruction was built from the microscopy images of different optical cross‐sections of the studied arrangement of crystal defects. In the close vicinity of the QN, the studied arrangement of crystal defects adopts the geometry of a collapsed tristetrahedron which, centred at the QN, has its legs along the TJs and, hence, has its faces as collapsed in pairs into the GBs. The angles defined by different TJ couples as well as the dihedral angles defined by the different GB couples meeting in every TJ were measured at the QN site. All, the image recording and stacking as well as the measuring procedures are carefully described. The measured TJ angles (97°, 117°, 95°, 117°, 99° and 130° ± 2°) depart from the characteristic angle (109.47°) of a tetrahedron whereas the measured GB angles (101°, 119°, 140°; 125°, 127°, 108°; 133°, 109°, 119°; 129°, 99° and 132° ± 2°) depart from the angular argument (120°) of a 3‐fold symmetry rotation indicating that, in the close neighbourhood of the QN, the studied arrangement of crystal defects is structurally unstable. Such an instability is associated with an observed mismatch in orientation (by angles of 20°, 15°, 33° and 30° ± 2°) between the TJs and some <111> zone axis matrix lattice crystallographic directions ([], [11], [11] and [11]), respectively). Local variations in anionic composition, existing within the solid solution matrix, are discussed to be responsible for this mismatching and, therefore, for the observed structural instability.     

专用面粉配比控制系统

介绍了一种为专用面粉加工工厂设计的配粉控制系统，由微型机实现管理，由PLC实现过程控制，并从软件，硬件及控制待方面阐述控制方案。     

公用车辆运行数据无线采集传输系统

针对公用车辆运行数据人工采集和录入效率低且不可靠等问题,提出了无线射频数据通信的设计。给出了采用SM5964单片机和NRF905单片射频收发器来实现车辆运行数据的无线采集传输的设计方案,包括车载机模块、无线发射和接收模块以及单片机和PC机之间的串行通信模块。该设计方案可推广应用于其他需要无线通信的数据采集系统。     

定位误差计算的一种简便方法——工序基准极位简图法

给出一种计算定位误差的简便方法,笔者称之为工序基准极位简图法。这种方法使工序基准极端位置的判定变得简捷,适用于较复杂的定位误差分析计算及多种定位方案的比较问题。     

高效液相色谱法测定五种茶叶中咖啡因含量

目的：采用高效液相色谱法测定了5种茶叶中咖啡因的含量。方法：采用Phenonm enxC18（4.6 mm×250 mm,5μm）反相色谱柱,流动相CH3OH H2O=5.5 4.5,流速1.0（mL·m in^-1）,检测波长为272 nm,柱温为35℃,在所选条件下,样品中待测组分与其它组分分离良好（R〉1.5）,通过重复性实验和加标回收实验,验证了方法的稳定性和可靠性。在本实验范围内各组分的峰面积和浓度之间具有良好的线性关系,r^2=0.999 9,5种茶叶的咖啡因回收率97.48%～107.73%,RSD=2.6%～3.0%。     

500kV海底电缆油泵站远程监控系统研究

海底电缆油泵站作为海南联网工程的重要组成部分,满足3根海底电缆用油及压力需求.油泵站系统投运9年,出现多起故障,当海底电缆油泵站控制系统故障后,无法监控油泵站的运行状况,无法手动对油泵站系统进行就地操作及了解海底电缆的供油情况.研究海底电缆油泵站的工作原理,打破原有代码屏蔽,开发一套海底电缆油泵站远程监控系统,实现对油泵站的远程监控.     

A self‐calibrated delay‐locked loop with low static phase error

In conventional delay‐locked loop circuits, the charge and discharge of the charge pump result in mismatched current reflecting the size of the static phase error. The static phase error between feedback clock and reference clock is likely to be within tens or hundreds of picoseconds (ps). We thus propose an approach using digital calibration methods to reduce the charge pump current mismatch by means of the setup time of the D‐type flip flop. The setup time of D‐type flip flop is determined and duplicated to detect the phase error between the reference clock and feedback clock. It results in a very small static phase error between the reference clock and feedback clock. This paper used a 0.18 µm CMOS process design, with a reference frequency of 700 ~ 900 MHz. The active area is 0.031 mm², and the phase error after correction is less than 5 ps. Copyright © 2015 John Wiley & Sons, Ltd.     

内燃机车电脑计量加油系统的研制

重点介绍内燃机车电脑计量加油机的工作原理、主要试验、总体设计、电脑计量设计和技术特点,从技术创新和现场应用相结合的角度,总结了该机研制过程中的主要技术工作。     

一种新型的IGBT驱动保护电路

介绍一种新型的性能较完善的IGBT驱动保护电路。实验结果表明,该电路能快速、安全、可靠地实现保护功能。     

核与辐射安全法规标准制修订管理原型数据库系统

介绍了核与辐射安全法规标准制修订管理系统的基本需求,原型数据库系统的数据结构、终端软件的功能以及原型数据库系统的应用情况。