富钛BaO-TiO2(Ti/Ba=4～4.5)系微波介质陶瓷

采用固相反应法制备了富钛BaTi4+xO9+2x(x=0.0-0.50)微波介质陶瓷,探讨了TiO2含量以及烧结温度对物相组成和介电性能的影响.在1300～1350 ℃烧结BaTi4+xO9+2x陶瓷即可达到约98%的相对密度.当x≤0.28时,BaTi4+xO9+2x陶瓷为BaTi4O9单相.随TiO2含量的增加,BaTi4+xO9+2x陶瓷从BaTi4O9单相逐渐转变成以BaTi4O9为主相,同时出现TiO2和Ba2Ti9O20相,并且随烧结温度提高,TiO2含量较多的试样中出现更多的Ba2Ti9O20相.随TiO2含量的增加介电常数逐渐增大,而Qf值呈下降趋势.Qf值从x=0.0时的约40 000 GHz逐渐降低至x=0.50时的15 000 GHz.     

Resistance of Mo-bearing stainless steels and Mo-bearing stainless-steel coating to naphthenic acid corrosion and erosion-corrosion

Naphthenic acid corrosion (NAC) and erosion-corrosion (NAEC) behavior of Mo-bearing (0-7.0 wt.%) stainless steels have been investigated in laboratory to evaluate the essential role of Mo on their NAC and NAEC resistance. The NAC and NAEC resistance of a high-velocity-oxygen-fuel (HVOF) thermal sprayed Mo-bearing stainless-steel coating was also investigated in both laboratory and an oil refinery. It was found that increasing the Mo content remarkably enhanced the NAC and NAEC resistance of stainless steels. The Mo-rich areas or phases in the steels played an importance role in resisting the NAEC. The HVOF coating showed excellent NAC and NAEC resistance in laboratory tests. The 700-day field test in an oil refinery revealed that the coating can effectively prevent the carbon-steel substrate from erosion-corrosion during long-term exposure in oil-refining environment. The corresponding NAC and NAEC mechanisms of the stainless steels and the beneficial role of Mo were discussed by taking account of inherent susceptibility of metal elements to corrosion, possible effects of Mo on surface films, and Mo-induced change in microstructure and microhardness.     

奔驰重卡转向节挤压锻造复合工艺的有限元分析

奔驰重型卡车的转向节挤压锻造工艺，分为镦粗、挤压、预锻和终锻4个工步。针对汽车转向节的挤压锻造进行的有限元分析。模拟软件采用Deform 3D，锻件采用刚塑性材料模型，成形过程看作为等温成形。报告给出了毛坯形状和尺寸、锻件形状变化，成形等效应变分布以及载荷——行程曲线等。实验表明，模拟结果和实际成形过程吻合良好。     

Numerical simulation of gas metal arc welding temperature field

The infrared camera is used to investigate the temperature field of gas metal arc welding.The results show that the temperature distribution of weld pool and adjacent area appears cone shape.A new heat source model combined by Gaussian distribution heat source of the arc and conical distribution heat source of the droplet is set up based on the experimental results, and with the combined boundary conditions,the temperature field of gas metal arc welding is simulated using finite element method.According to the comparison between the results of experiment and simulation in temperature field shows that the new combined heat source model is more accurate and effective than the Gauss heat source model.     

Size and pressure effects on solid transition temperatures of ZrO2

Transition temperatures between tetragonal and monoclinic polymorphs of ZrO₂ nanoparticles, thin films and nanostructured materials are calculated by considering energetic contributions of surface (interface) energy and surface stress on total Gibbs free energy. The transition temperatures drop as the size of the nanocrystals decreases, which is consistent with available results.     

焊接工艺参数对奥氏体不锈钢焊接接头腐蚀行为的影响

通过草酸腐蚀和硫酸-硫酸铁腐蚀实验，研究了奥氏体不锈钢焊接接头腐蚀与焊接热输入的关系。结果表明，随着焊接线能量的增加，其焊接接头腐蚀越严重。随着焊接线能量的增大，腐蚀率增大且有加速趋势。     

弛豫铁电体Pb(Mg1/3Nb2/3)O3-PbTiO3的相变

测量了(1-x％)镁铌酸铅-x％钛酸铅(1≤X≤11)(简称PMNTx)陶瓷样品的介电常数、内耗和Young’s模量．观测到在Tm温度附近，即在介电常数达到最大值时，出现一个内耗峰，并且模量发生软化．这反映了极化纳米微畴的弛豫．对于PMNTx(5≤x≤11)的样品，在Tm温度以下的某个温度出现附加的内耗峰和Young’s模量的异常，表明样品中发生了自发的弛豫铁电到铁电(简称R-F)的相变，对R-F相变的机制进行了讨论．     

电磁无接触成形过程熔体形状的数值模拟及实验研究

应用有限元方法模拟计算了电磁约束成形过程中感应器结构、固／液界面位置、熔体上顶面位置、电流频率及熔体种类对熔体形状的作用规律。结果表明：喇叭形内壁的感应器中熔体可获得侧面基本垂直的理想形状；固／液界面、熔体上顶面位置对熔体形状有明显的影响：电流频率的变化对熔体成形形状的影响很小：在感应器结构、固／液界面及熔体上顶面位置等确定后，合金种类对熔体形状几乎没有影响。同时对电磁成形规律进行了研究，表明实验与模拟计算的结果取得了很好的吻合。用电磁成形方法完成了Al合金、TiAl化合物和Ni基高温合金的无接触成形，制备出了样件，并对组织实现了定向控制。     

板料拉深成形过程中的变压边力技术

压边力是板料成形过程中的重要参数之一。在概述压边力在生产中的主要用途和意义的基础上，从压边力的加载模式、理论模型、实验研究变压边力技术与拉延筋、人工智能技术的交叉应用等方面，比较全面的综述了压边力技术的研究现状及存在问题，并探讨压边力技术的研究方向。     

残余奥氏体对20Mn2SiVB钢的疲劳裂纹扩展的影响

研究了残余奥氏体对20Mn2SiVB钢疲劳裂纹扩展的影响。结果表明,在贝氏体铁索体中有残余奥氏体膜的存在,残余奥氏体膜可起到提高断裂韧性的作用;在应力强度因子较高的范围内,疲劳裂纹扩展速率受钢的断裂韧性影响,断裂韧性高,裂纹扩展速率低。