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71.
Xiang‐Dan Li Zhen‐Xin Zhong Sang‐Hoon Han Seung Hee Lee Myong‐Hoon Lee 《Polymer International》2005,54(2):406-411
From chloromethylated polyimide, a useful starting material for modification of aromatic polyimides, a thermocurable transparent polyimide having acrylate side groups was prepared. In the presence of 1,8‐diazabicyclo[5,4,0]undec‐7‐ene, chloromethylated polyimide was esterified with acrylic acid to synthesize poly(imide methylene acrylate). The polymer was soluble in organic solvent, which makes it possible to prepare a planar film by spin coating. The polymer film became insoluble after thermal treatment at 230 °C for 30 min. Optical transparency of the film at 400 nm (for 1 µm thickness) was higher than 98 % and not affected by further heating at 230 °C for 250 min. Adhesion properties measured by the ASTM D3359‐B method ranged from 4B to 5B. Preliminary results of planarization testing showed a high degree of planarization (DOP) value (>0.53). These properties demonstrate that poly(imide methylene acrylate) could be utilized as a thermocurable transparent material in fabricating display devices such as TFT‐LCD. Copyright © 2004 Society of Chemical Industry 相似文献
72.
Wang Xuegang Yan Fengjie Yan Qian Li Xingeng 《Frontiers of Materials Science in China》2007,1(2):225-227
An iron-based amorphous foil (FeNiCrSiB) was used as an interlayer for the amorphous diffusion bonding of low carbon steel
pipes under argon flux. The microstructure and mechanical properties of the joint were analyzed using an electron probe micro-analyzer
(EPMA), tensile test, bending test and impact test. The results show that the joint microstructure resembles that of the base
metal and no precipitates form at the joint. Melting point depressants (B, Si) diffuse far away from the joint and the base
metal element is homogenous across the joint. The joint impact toughness is greater than the base metal toughness and the
mechanical properties of the joint are similar around the pipe. 相似文献
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Xiaojun Xie Yonghong Cheng Hong Wang Qian Wang Xiaolin Chen Caixin Sun 《Ceramics International》2008,34(4):689-693
In the ideal A2B2O6O′ pyrochlore structure, the x-value of O atom position is a variable parameter. In Bi1.5ZnNb1.5−xTaxO7 (BZNT) cubic pyrochlores, the x-values alter with the different compositions of Nb/Ta. In this work, a series of initial models for BZNT were established by analyzing X-ray diffraction data. Then three structure modifying methods, including Rietveld refinement, Rietveld refinement with energy and geometry optimization based on quantum mechanics, were employed to obtain the precise models using Materials Studio. Moreover, the reflectivities of BZNT were computed by quantum mechanical simulation based on the refined models. Comparing the simulation results from different modifying models with the experimental results, it is found that Rietveld refinement with energy optimization is the most accurate method for BZNT pyrochlores. According to the simulation results, the different reflectivities correspond well with various x-values of O atom positions in BZNT pyrochlores. 相似文献
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美国著名未来学家阿尔温托夫勒曾经预言:“电脑网络的建立与普及将彻底地改变人类生存及生活的模式,而控制与掌握网络的人就是人类未来命运的主宰。谁掌握了信息,控制了网络,谁就将拥有整个世界。”信息技术通过信息交换网络渗透到社会各个领域,将导致社会资源配置方式、企业生产及 相似文献
79.
The present study is an investigation on the behaviors of concrete-filled thin-walled steel tubular members subjected to combined loading, such as compression and torsion, bending and torsion, compression, bending and torsion. ABAQUS software is used in this paper for the finite element analysis (FEA). A comparison of results calculated using this modeling shows generally good agreement with test results. The FEA modeling is then used to investigate the influence of important parameters that determine the ultimate strength of the composite members under combined loading, such as compression and torsion, bending and torsion, compression, bending and torsion. The parametric studies provide information for the development of formulae for calculating the ultimate strength of the composite members subjected to combined loading. 相似文献
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