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121.
A new technique for the preparation of CuI nanoparticles from CuSO4 and KI ethanol solutions has been developed. Preparation conditions were optimized through a series of experiments. Under
these conditions, the yield of CuI reached 95.39%. The product was characterized and the reaction kinetics was studied. The
results show that the product takes a roughly spherical shape with an average particle size of less then 50 nm. The activation
energy of the formation of CuI is found to be E
a = 0.58 × 102 kJ/mol, and the preexponential factor in the Arrhenius equation is k
0 = 7.43 × 1016 mol/(l s).
The text was submitted by the authors in English. 相似文献
122.
针对信息技术和工业控制技术的飞速发展,为适应现代化发电企业的信息建设需求,提高企业自动化水平和管理水平,提出了电厂模块结构的数字化仪表墙(digitalwall)系统概念,并对电厂模块结构的数字化仪表墙系统的结构、显示平台、控制平台等整体的集成方案及设计选型等进行简要叙述。 相似文献
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124.
腐败是与政府行政权力相伴生的痼疾,既是一个历史现象又是一个国际现象。贪污腐败和寻租腐败是委托一代理模型中最典型的腐败方式,文章在此基础上对贪污腐败和寻租腐败进行成本一收益分析和市场均衡分析,并探讨治理行政权力腐败的有效途径。 相似文献
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127.
The combination of the chemical aggressivity of water and lead piping, as is well known, can cause severe cases of lead poisoning in those who consume such water. After a great number of observations and epidemiological studies which have strongly incriminated this metal in a wide range of pathologic conditions, other materials have been gradually substituted for lead; however, the problem remains.In compliance with a European Directive to survey the risk of lead poisoning (Council Directive, 1977), a random sample of 321 residents was selected from the Vosgian Mountains of France. This region is noted for its high incidence of cases of lead poisoning: 150 reported during 8 months in 1983 (Barbier et al., 1983).During the course of a health evaluation, a blood sample was taken from each subject for lead analysis. At the same time, a sample of tap-water (after running for 5 s) was taken from each subject home. Both lead analyses (blood and water) were performed by electrothermal atomization-atomic absorption spectrophotometry. Because of the log-normality of the distributions of the blood lead levels and the concentrations of lead in the drinking water, a logarithmic transformation was performed so that the results are expressed as the geometric mean, which for the amount of lead in the drinking water of our sample was found to be 0.16 mg l?1.Among the subjects of this study, 28% are served by water containing more than 0.10 mg l?1 of lead (the standard for France) and 48% by water containing more than 0.05 mg l?1 (the European and WHO standard). In concurrence with numerous authors, our study indicates that, among our subjects, the blood lead level is much higher in men than in women (geometric means 22.9 and 15.0 μg dl?1 respectively); this difference is highly significant (t-test:P < 0.001). Table 1 summarizes the results, by sex, obtained in this region compared with those from a study (Huel, 1982) concerning an urban French population whose geometric mean blood lead levels were 15.9 μg dl?1 for men and 11.4 μg dl?1 for women. The irrespective of sex, is highly significant (P < 0.001). Table 2 shows the significance of the relation between these subjects, high blood lead levels and the concentration of lead in their drinking water, while Fig. 1 shows that for contamination levels up to 0.02 mg l?1 of lead in water, the blood lead level remains relatively stable, while above this apparent “threshold” value, the blood lead level begins to increase finally reaching quite high values in response to high contamination levels, suggesting a direct translation of increases in the water above the 0.02 mg l?1 level to increases in the blood. 相似文献
128.
Xinying. Lu Kaiming. Liang Shouren. Gu Yankang. Zheng Hongsheng. Fang 《Journal of Materials Science》1997,32(24):6653-6656
The effect of oxygen vacancy on the stability of phase structures and phase transformation of zirconia at low temperatures
was studied using an electrochemical technique. It is suggested that the decrease of oxygen vacancies decreases the stability
of metastable tetragonal zirconia and promotes its transformation to the monoclinic phase.
This revised version was published online in November 2006 with corrections to the Cover Date. 相似文献
129.
130.
研究了电子束、离子束作用于Al2O3表面时成分的变化,表明无论电子束或离子束都能使Al2O3发生分解,产生导电的元素Al。实验在PHI610·SAM上进行,电子束轰击下(3keV,O.5μA,入射角60°)10s就有元素Al分解出来,2min以后就达到饱和,分解析出量随时间成a(1-e-bt)的关系。离子束轰击下同样发生元素Al的分解,但当Ei>3keV时,由于剥离速率加大,溅射5min时表面Al峰反而比1min时要弱。这时表面Al含量处于分解析出与溅射剥离的动态平衡中。实验还发现了Al2O3的解析与表面成分有关(如碳的含量)。最后讨论电子束与离子束的解析机理。 相似文献