神经网络在奥氏体钢设计中的应用

采用人工神经网络分别对奥氏体钢的相变临界点Ｍｓ、Ｍｅｓ，力学性能和化学成分间的关系建立了非线性网络模型，并通过试验数据验证了这些模型的正确性。此方法不同于以线性回归为基础来推导得到经验公式。它具有容错性好，通用性强等优点，神经网络的应用为材料的设计与应用提供了一种较为可靠的新途径。     

Release of Ciprofloxacin from Chondroitin 6-Sulfate-Graft-Poloxamer Hydrogel In Vitro for Ophthalmic Drug Delivery

The system was designed to use Poloxamer as a vehicle for ophthalmic drug delivery using in situ gel formation property. To enhance the wound healing and cell adhesion as well as transparency of Poloxamer hydrogel, chondroitin 6-sulfate (C6S) was introduced into Poloxamer. For this purpose, mono amine-terminated Poloxamer (MATP), which was end-capped with ethylene amine group only in one side of terminal hydroxyl groups of Poloxamer, was synthesized. Subsequently, C6S-graft-Poloxamer copolymer (C6S-g-Poloxamer) was prepared by reaction between the amine groups of MATP and carboxyl groups of C6S in the presence of 1-ethyl-3-(3-dimethylaminopropyl)-carboimide (EDC). The coupling of MATP with C6S was clarified by ¹H-NMR and FT-IR spectroscopy. The gelation temperature of graft copolymers was determined by measuring the temperature at which immobility of the meniscus in each solution was first noted. Release behavior of ciprofloxacin from C6S-g-Poloxamer hydrogel in vitro was investigated as a function of C6S content in the graft copolymer by a spectrophotometric assay at 287 nm using an UV spectrophotometer. Differences in the adhesion and morphology of human lens cell between Poloxamer- and C6S-g-Poloxamer-coated surfaces were also investigated. The gelation temperatures of C6S-g-Poloxamer copolymers were lowered with increasing of the concentration of the copolymer and decreasing of C6S content. The release of ciprofloxacin from the graft copolymer was sustained compared with Poloxamer itself and decreased with increasing the content of C6S in the copolymer due to the in situ gel formation of the copolymer and viscous properties of C6S. Human lens cells (B3) adhered to C6S-g-Poloxamer-coated surface were observed as transformed shapes after 2 days. The bioadhesive and thermally gelling of these graft copolymers will be expected to be an excellent drug carrier for the prolonged delivery to surface of the eye.     

Novel configurations of planar multilayer magic-T usingmicrostrip-slotline transitions

Novel configurations of microwave planar magic-T suitable for microwave integrated circuits (MICs) and monolithic MICs are described. They consist of microstrip and slotline T-junctions coupled by microstrip-slotline transitions. Since via-hole processing is not encountered, they are especially applicable to multilayer MICs. Derived equivalent network models are used efficiently for the design of the corresponding multilayer microstrip magic-T. Measured data and numerical simulations showing good amplitude and phase characteristics over an octave operating bandwidth validate the proposed configurations of planar magic-T     

Enhanced Electrochromism with Rapid Growth Layer‐by‐Layer Assembly of Polyelectrolyte Complexes

In this work, a facile method to deposit fast growing electrochromic multilayer films with enhanced electrochemical properties using layer‐by‐layer (LbL) self‐assembly of complex polyelectrolyte is demonstrated. Two linear polymers, poly(acrylic acid) (PAA) and polyethylenimine (PEI), are used to formulate stable complexes under specific pH to prepare polyaniline (PANI)/PAA‐PEI multilayer films via LbL deposition. By introducing polymeric complexes as building blocks, [PANI/PAA‐PEI]_n films grow much faster compared with [PANI/PAA]_n films, which are deposited under the same condition. Unlike the compact [PANI/PAA]_n films, [PANI/PAA‐PEI]_n films exhibit porous structure that is beneficial to the electrochemical process and leads to improved electrochromic properties. An enhanced optical modulation of 30% is achieved with [PANI/PAA‐PEI]₃₀ films at 630 nm compared with the lower optical modulation of 11% measured from [PANI/PAA]₃₀ films. The switching time of [PANI/PAA‐PEI]₃₀ films is only half of that of [PANI/PAA]₃₀ films, which indicates a faster redox process. Utilizing polyelectrolyte complexes as building blocks is a promising approach to prepare fast growing LbL films for high performance electrochemical device applications.     

Dimensional analyses and surface quality of pulsed UV laser micro-machining of STAVAX stainless steel mold inserts

Laser micro-machining is a new, precise, and very flexible process in micro-mold manufacturing, especially for difficult to machine material, i.e., hardened steel. The aim of the work reported in this paper was to utilize response surface methodology to optimize the dimensional accuracy and surface finish for STAVAX stainless steel mold inserts in the pulsed UV laser micro-machining. The influence of laser machining parameters on the ablated depth and surface roughness of the machined mold inserts have been experimentally investigated. The parameters of insert quality are analyzed under varying laser power, pulse frequency, hatched spacing, scan rate, and number of passes. The settings of the laser micro-machining parameters are determined by using design of experiments method. The analysis of variance, and regression analyses are employed to find the optimal levels and to analyze the effect of the parameters on the depth accuracy values and surface finish. Confirmation experiments with the optimal levels of micro-machining parameters are carried out in order to illustrate the effectiveness of the multi-optimization method. The validity of regression approach to process optimization is well established.     

无线网络虚拟化架构与关键技术

提出采用集中式和分布式的动态频谱管理技术来提升频谱资源利用效率,解决无线网络虚拟化中频谱资源难以高效分配与不易管理难题;认为为了构建一个稳定、灵活和开放的无线网络虚拟化架构,需要从虚拟网络的隔离、信令优化设计、通用接口设计、用户移动性管理等方面开展研究。     

Characterization of the Ultrathin HfO2 and Hf-Silicate Films Grown by Atomic Layer Deposition

The physical properties of HfO₂ and Hf-silicate layers grown by the atomic layer chemical vapor deposition are characterized as a function of the Hf concentration and the annealing temperature. The peaks of Fourier transform infrared spectra at 960, 900, and 820 cm_-1 originate from Hf-O-Si chemical bonds, revealing that a Hf-silicate interfacial layer began to form at the HfO₂/SiO ₂ interface after post deposition annealing process at 600 degC for 1 min. Moreover, the intensity of the peak at 750 cm^-1 can indicate the degree of crystallization of HfO₂. The formed Hf-silicate layer between HfO² and SiO² is also confirmed by X-ray photoelectron spectroscopy     

高氮奥氏体钢形变组织的晶体学特征

Ｆｅ－Ｍｎ－Ｃｒ－Ｍ奥氏体钢在低温下形变组织具有严格的晶体学特征。穿晶脆断刻面是｛１１１｝γ，刻面上滑移带相交成６０°，两相交大角度１０９°２８＇的｛１１１｝γ穿晶刻面上滑移带成对称状；沿形变孪晶界面脆断面为｛１１０｝面，相交形变孪晶夹角为７０°；滑移带在孪晶晶界处产生扭折，扭折角３５￣４０°；在任意的金相断面上，相交滑移带夹角是６０￣８０°。     

Validation of [13C]urea breath test for Helicobacter pylori using a simple gas chromatograph-mass selective detector

OBJECTIVE: Isotope ratio mass spectrometry (IRMS) is the accepted method for accurately measuring the 13CO2:12CO2 ratio in the non-invasive and non-radioactive [13C]urea breath test (13C-UBT) for Helicobactor pylori. The IRMS instrument, an expensive and highly specialized analyser, is rarely available. The objective of this project was to modify and validate the use of a simple bench-top gas chromatograph-mass selective detector (GC-MSD) for 13C-UBT. METHODS: Breath samples from 71 patients were taken at baseline and 30 min after ingestion of 100 mg [13C]urea. The breath samples were analysed using GC-MSD in the selected ion monitoring mode. The reference 13CO2:12CO2 ratio was from NBS19 obtained from the US National Institute of Standards and Technology. 13CO2:12CO2 ratios of the breath samples were determined. Excess delta per thousand (per mil, delta/thousand) of the 30 min sample over the baseline (deltadelta/thousand) of > or = 6deltadelta/thousand was considered H. pylori positive. Results from 13C-UBT and histology determined blind to each other were compared. RESULTS: The coefficient of variation of the reference 13CO2:12CO2 ratio was 0.06%. Using histology as the 'gold standard', the sensitivity (97.9%) and specificity (95.8%) of the GC-MSD 13C-UBT were comparable to those of other methods of H. pylori diagnosis. CONCLUSION: A gas chromatograph coupled to a mass selective detector that is available in many analytical and biomedical laboratories can be used for the 13C-UBT. This method will increase the availability and reduce the cost of this non-invasive, non-radioactive diagnostic test.