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1.
Using photo acoustic technique, the thermal properties of CdS thin films grown by spray pyrolysis are measured. Thermal diffusivity
and conductivity in these films decrease at least two orders compared with bulk. These results are compared with our study
on nano CdS and the other available literature. The comparison is good. The dependence of thermal diffusivity on the thickness
of the layer or the size of the particles on the glass substrate are analysed from the present measurement and discussed.
The dependence of thermal diffusivity on the thickness of the layer on the glass substrate is discussed. 相似文献
2.
Moisture sorption isotherms of EX-BORNO and SOSAT C88 millets at temperature range of 30–70 °C and water activity range of 0.07–0.98 were determined using the static gravimetric method. The sorption isotherms of both millet varieties decreased with increasing temperature, exhibited type II behaviour according to BET classification and hysteresis having loop size increasing with increasing temperature. This is as a result of the hard nature of the millet varieties. The moisture sorption and the data fitted well with Modified Henderson, Modified Halsey, Modified Oswin and Modified GAB models. The constants of the equations used in fitting were determined by non-linear regression analysis when the models were compared using the standard error of estimate, mean relative percent deviation, fraction explained variation and residual plots. The Modified Oswin model gave the best fit for the whole set of data. The study has provided information and data useful in large scale drying and processing of millet which have remained at the traditional level despite the importance of the drought resistance crop in poverty alleviation. 相似文献
3.
M. Auta U. Musa D. G. Tsado A. A. Faruq A. G. Isah S. Raji 《Chemical Engineering Communications》2018,205(6):789-796
Attention is presently drawn to the development of a new and green alternative technique for the extraction of essential oil from citrus plant materials. This study was aimed at the extracting essential oil from orange and lemon peels using solvent-free microwave method. This process uses microwave-assisted hydro-diffusion technique to extract essential oil from citrus peels. Response surface methodology was used to investigate the effect of microwave power (200–1,000?W) and extraction time (10–40?min) on the essential oil yield. The oil extracted was characterized using Fourier transform infrared radiation (FTIR) and Gas chromatography–mass spectrometry analysis to determine the functional groups and chemical components present, respectively. The optimum yield of extract from orange and lemon peels were 3.7 and 2.0%, respectively at corresponding power of 1,000?W and time of 10?min. The analysis of variance results showed that the resulting models for both orange and lemon peels were significant and microwave power had greater influence on the extraction processes at both linear and quadratic levels. The FTIR analysis revealed prominent functional groups of alkenes that majorly constitute limonene compound at 1,642 and 1,643?cm?1 for orange and lemon peels, respectively. The present process permits fast and efficient extraction, avoids water and solvent consumption, and allows substantial energy savings. 相似文献
4.
In this report, Cu0.5Ni0.5Fe2O4 nanoparticles were synthesized by solgel using eco-friendly aloe vera extract and citric acid separately and their properties were discussed. Structural, Functional, morphological, magnetic properties of the samples were characterized using X-ray diffraction (XRD), Fourier transform infrared (FT-IR), Transmission electron microscopy (TEM), Vibrating sample magnetometer (VSM). XRD exhibited the samples have single phase cubic spinel with average size of 46.4?nm and 35.45?nm. Two characteristics bands of ferrite were confirmed by FTIR. TEM indicated different morphology of the samples with some regularity. VSM data showed that higher coercivity for the sample prepared by aloe vera extract. 相似文献
5.
Gholamhossein Sodeifian Mojtaba Raji Morteza Asghari Mashallah Rezakazemi Amir Dashti 《中国化学工程学报》2019,27(2):322-334
SAPO-34 nanocrystals (inorganic filler) were incorporated in polyurethane membranes and the permeation properties of CO2, CH4, and N2 gases were explored. In this regard, the synthesized PU-SAPO-34 mixed matrix membranes (MMMs) were characterized via SEM, AFM, TGA, XRD and FTIR analyses. Gas permeation properties of PU-SAPO-34 MMMs with SAPO-34 contents of 5 wt%, 10 wt% and 20 wt% were investigated. The permeation results revealed that the presence of 20 wt% SAPO-34 resulted in 4.45%, 18.24% and 40.2% reductions in permeability of CO2, CH4, and N2, respectively, as compared to the permeability of neat polyurethane membrane. Also, the findings showed that at the pressure of 1.2 MPa, the incorporation of 20 wt% SAPO-34 into the polyurethane membranes enhanced the selectivity of CO2/CH4 and CO2/N2, 14.43 and 37.46%, respectively. In this research, PU containing 20 wt% SAPO-34 showed the best separation performance. For the first time, polynomial regression (PR) as a simple yet accurate tool yielded a mathematical equation for the prediction of permeabilities with high accuracy (R2 > 99%). 相似文献
6.
Rajangam Vinodh Prem Jyoti Sing Rana Chandu VV Muralee Gopi Zongmin Yang Raji Atchudan Kandan Venkatachalam Hee‐Je Kim 《Polymer International》2019,68(5):929-935
We successfully synthesized 13X zeolite using a hydrothermal method. Then, composites of polyaniline (PANI) with 13X zeolite and PANI–13X with platinum were prepared by chemical oxidative polymerization and chemical reduction, respectively. Field emission scanning electron microscopy, X‐ray diffraction, Raman spectroscopy and Brunauer–Emmett–Teller techniques were used to characterize the PANI–Pt and PANI–Pt–13X composites. Further, the electrocatalytic activity towards methanol oxidation of the synthesized catalysts was explored using cyclic voltammetry in 1 mol L?1 CH3OH + 0.5 mol L?1 H2SO4 solution. From the obtained results, PANI–Pt–13X shows superior performance compared to PANI–Pt towards methanol oxidation and electrical conductivity. Hence, the 13X zeolite‐incorporated PANI–Pt composite could be an efficient catalyst for direct methanol fuel cell applications. © 2019 Society of Chemical Industry 相似文献
7.
Sekar Karthi Raji Govindan Ajithkumar Gangadharan Gamage Chamath Dannangoda Karen S. Martirosyan Dhiraj K. Sardar Santhosh Chidangil Easwaradas Kreedapathy Girija 《Journal of the American Ceramic Society》2019,102(5):2558-2568
Luminomagnetic nanostructured Nd3+ doped fluorapatite (FAP) coated Fe3O4 nanoparticles were produced by hydrothermal method. X-ray diffraction analysis indicates that the prepared nanoparticles contain both FAP and Fe3O4 phases. Electron microscope analysis shows the formation of nanoparticles of Fe3O4 encased in rod shaped FAP nanoparticles of average length 40 nm. Magnetic measurements confirm the room temperature superparamagnetic nature of the nanoparticles with saturation magnetization value up to 7.8 emu/g. The prepared nanoparticles display strong near infrared (NIR) emission at 1060 nm under 800 nm excitation. Cell viability studies for 72 hour demonstrate the survival rate of over 84% with 500 μg/mL concentration indicating the good cytocompatibility of the prepared materials. The present Nd3+ doped FAP coated Fe3O4 nanostructure provides an excellent multifunctional platform for diagnostics and therapeutic applications. 相似文献
8.
Igor Jerković Marina Rajić Zvonimir Marijanović Mate Bilić Stela Jokić 《分离科学与技术》2016,51(18):2925-2931
Supercritical (SC) CO2 extraction of dried Immortelle flowers was performed at different process parameters. The optimal extraction conditions related to the yield were determined by response surface methodology (yield 4.09% at 20 MPa and 52°C). The extracts were analyzed by GC-MS and tremetone derivatives dominated: bitalin A, 12-acetoxytremetone, gnaphaliol, 1-[2-(2-methyl-2,3-dihydroxypropyl)-2,3-dihydro-1-benzofuran-5-yl]ethanone, isobutyl bitalin A, and 1-[2-(acetylprop-1-en-2-yl)-3-hydroxy-2,3-dihydro-1-benzofuran-5-yl]ethanone. Striking differences were found among the essential oil and SC-CO2 extracts composition. The major oil compounds were γ-curcumene, α-pinene, β-selinene, α-selinene, and limonene. Mono- and sesquiterpene were found among minor constituents of the extracts. Neryl acetate was present in the extracts and essential oil. 相似文献
9.
Sidharth Kumar Sethi Rupesh Raina Shyam Bihari Bansal Anvitha Soundararajan Maninder Dhaliwal Veena Raghunathan Meenal Kalra Kritika Soni Samit Kumar Mahato Ananya Vadhera Dinesh Kumar Yadav Timothy Bunchman 《Hemodialysis international. International Symposium on Home Hemodialysis》2023,27(3):308-317
10.
Sarkar S. Soundararajan P. 《IEEE transactions on pattern analysis and machine intelligence》2000,22(5):504-525
Perceptual organization offers an elegant framework to group low-level features that are likely to come from a single object. We offer a novel strategy to adapt this grouping process to objects in a domain. Given a set of training images of objects in context, the associated learning process decides on the relative importance of the basic salient relationships such as proximity, parallelness, continuity, junctions, and common region toward segregating the objects from the background. The parameters of the grouping process are cast as probabilistic specifications of Bayesian networks that need to be learned. This learning is accomplished using a team of stochastic automata in an N-player cooperative game framework. The grouping process, which is based on graph partitioning is able to form large groups from relationships defined over a small set of primitives and is fast. We statistically demonstrate the robust performance of the grouping and the learning frameworks on a variety of real images. Among the interesting conclusions is the significant role of photometric attributes in grouping and the ability to form large salient groups from a set of local relations, each defined over a small number of primitives 相似文献