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31.
The effect of the reaction conditions on the grafting parameters during grafting of 2‐acrylamido‐2‐methyl‐1‐propanesulfonic acid onto sodium carboxymethylcellulose using H2O2/Fe+2 redox pair are studied at 30°C. The grafting ratio, add on, and conversion initially increase with the H2O2 concentration in the range of (10.0–15.0) × 10?2 mol dm?3. Thereafter, these parameters decrease with the H2O2 concentration. The grafting ratio, add on, and conversion increase when increasing the ferrous ion concentration from (0.5 to 4.0) × 10?2 mol dm?3 and decrease with a further increase in the concentration. It is observed that the grafting ratio and add on increase with the monomer concentration, whereas the conversion decrease. The hydrogen ions seem to be facilitating the grafting reaction up to a certain concentration and after this concentration seem to be retarding the process. The grafting ratio, add on, and conversion decrease with the sodium carboxymethylcellulose concentration. When increasing the time period from 60 to 90 min, the grafting parameters increase but decrease thereafter. Similarly, when increasing the temperature from 25 to 30°C, the grafting parameters increase and decrease thereafter. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 100: 4819–4825, 2006 相似文献
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33.
Guttamindapalli A. Ravi Feridoon Azough Robert Freer Robert J. Cernik Anthony M. T. Bell 《Journal of the American Ceramic Society》2007,90(12):3947-3952
Mixed-oxide prepared Ca0.7 Ti0.7 La0.3 Al0.3 O3 (CTLA) ceramics (≈96% dense), grain size 6–7 μm, with dielectric properties (at 4 GHz) of ɛr ≈46, Q × f ≈38 000 GHz, and τf +13 ppm/°C, were studied at 25°–1300°C using synchrotron X-ray powder diffraction. At room temperature, CTLA exhibits a distorted orthorhombic structure, with two tilt systems: a =5.40383 (4) Å, b =5.41106 (6) Å, and c =7.64114 (7) Å with space group Pbnm . At 1050°±25°C, there is a transition from orthorhombic ( Pbnm ) to tetragonal ( I 4/ mcm ), with a simpler tilt arrangement. The lattice parameters at 1100°C were: a =5.44285 (4) Å and c =7.68913 (8) Å. 相似文献
34.
[60]Fullerene (C60) was mono-substituted with well-defined poly(methyl methacrylate) (PMMA-b-C60) using the atom transfer radical polymerization (ATRP) technique. The self-assembly behaviors of PMMA-b-C60 in ethyl acetate (EA) and decalin mixtures were studied using laser light scattering (LLS) and transmission electron microscopy (TEM). Homogeneous solutions of PMMA-b-C60 can be obtained in the solvent mixtures containing more than 40 wt% EA, where the molar ratio of decalin to EA is close to 1. For each solvent mixture, unimers coexist with micelles and large aggregates. The sizes of PMMA-b-C60 micelles and aggregates are independent of polymer concentration, confirming that they are produced via the closed association mechanism. For the various solvent mixtures, the weight-averaged molecular weights, Mw of the PMMA-b-C60 aggregates range from 4.1×107 to 12.5×107 g/mol. The hydrodynamic radii of the large aggregate, Rh, vary from 90 to 136 nm, while the z-averaged radii of gyration, Rg, range from 210 to 311 nm. The Rg/Rh value for each solvent mixture is ∼2.3, which is independent of decalin contents in the mixed solvents. The morphological study using the transmission electron microscope suggests that the large aggregates are composed of porous large compound micelles (LCM) in solution. 相似文献
35.
Scanning Electron Microscopic (SEM) studies were carried out on the failure surface of syntactic foam material tested in a short beam three point bend test (SBT) by employing 21 × 15 × 3 mm3 dimension bearing specimens. The syntactic foams were fabricated using glass microballoons in epoxy binder. The failure of the tensile, compression, and shear dominated regions were studied by SEM at different magnifications. The tensile region had characteristic features, such as partial debonding of the microballoons from the matrix and cracking of glass microballoons, apart from matrix cracking and some river pattern features. The compression side was characterized by crushing and collapsing of microballoons, resulting in accumulation of debris with no apparent river pattern for matrix‐rich regions. The midway positions of the SBT failed surface comprised of deformation bands in the matrix and occasional debonding of microballoons. The morphology recorded in the tensile and compression regions corroborated well with the results obtained on these foam samples in those specimens that were subjected to pure uniaxial tension and compression, respectively. © 2005 Wiley Periodicals, Inc. J Appl Polym Sci 98: 673–679, 2005 相似文献
36.
Anbarasi A. Ravi S. Vaishnavi J. Matla S. V. Suresh Babu 《Multimedia Tools and Applications》2021,80(14):21409-21424
Multimedia Tools and Applications - The significance of mitral valve (MV) treatment is increasing recently because of an aging population. The computer vision-based acquisition and quantification... 相似文献
37.
38.
Surface reconstruction for incremental forming 总被引:1,自引:0,他引:1
A. Erman Tekkaya Ravi Shankar Gerd Sebastiani Werner Homberg Matthias Kleiner 《Production Engineering》2007,1(1):71-78
In spite of extensive efforts being made with regard to virtual process optimization technology, the production of prototype
parts is still a necessity. With respect to the production of sheet metal parts in low quantities, incremental sheet metal
forming (ISMF) is a highly interesting process. ISMF allows the production of complex parts with drastically reduced costs
in tooling and machinery compared to conventional processes like deep drawing. However, ISMF, with it’s incremental nature,
introduces the need for generating a tool path considering both final geometry and process-induced deviations or constraints.
Consequently, for the generation of the tool path a (tool path) surface, with an adequate offset, is necessary. That is why,
within the scope of extensive research work at the Institute of Forming Technology and Lightweight Construction (IUL), a special
correction module has been developed, determining this offset e.g. depending on the workpiece geometry. This paper presents
the algorithm, the application, and the effect on the produced parts. Furthermore, a concept for an extension regarding further
constraints like elastic workpiece behavior is presented. 相似文献
39.
Y.S Wong M Rahman H.S Lim H Han N Ravi 《Journal of Materials Processing Technology》2003,140(1-3):303-307
Similar to EDM, in micro-EDM, intense heat is generated between the workpiece and tool electrode by the discharge through a dielectric medium to result in the formation of a microcrater that is much smaller in size. In this study, a single-spark generator has been developed to study the erosion characteristics from the microcrater size. Using a simple heat transfer model, the efficiency at different discharge condition is also deduced. It is found that at lower-energy (<50 μJ) discharges, the energy required to remove the unit volume of material, defined as the specific energy, is found to be much less than that at higher-energy discharges. Additionally, the ratio of the standard deviation to the measured microcrater size is found to be lower at lower discharge energy, indicating greater consistency in shape and size when the discharge occurs at lower energy. The fundamental erosion mechanism of material is discussed by considering melting and evaporation phenomena using theoretical modeling. The average efficiency of erosion, when estimated to be due primarily to melting or evaporation alone, is found to be up to an order of magnitude higher at lower-energy discharges than that at higher-energy discharges. 相似文献
40.
Hualong Li Emilie Hsu Jerzy Szpunar Ravi Verma Jon. T. Carter 《Journal of Materials Engineering and Performance》2007,16(3):321-326
In order to determine the deformation modes in AZ31 magnesium alloy at room temperature, computer simulations of deformation
texture development and calculation of formability have been carried out. The simulation results were compared with the measured
texture results. Based on agreement between the experiments and simulations the active deformation modes were determined.
A Visco Plastic Self Consistent model was employed for the simulation of plastic deformation. Simulations and experiments
were performed for different initial textures. The goal of the study was to develop the understanding of deformation texture
evolution and its effects on mechanical properties of magnesium, with an ultimate goal of improving room temperature formability
of magnesium alloys.
This article was presented at Materials Science & Technology 2006, Innovations in Metal Forming symposium held in Cincinnati,
OH, October 15-19, 2006. 相似文献