Pressureless sintering of in-situ toughened Yb α-SiAlON ceramics by adding seed crystals prepared by combustion synthesis

Single-phase Yb α-SiAlON ceramics in-situ toughened by elongated grains were prepared by pressureless sintering, with the crystalline powder prepared by combustion synthesis used as seed crystals. The effects of seed addition on the densification, phase transformation, microstructure development, and mechanical properties of the samples were investigated in detail. From the experimental results, it was found that the added seed crystals could promote the phase transformation and facilitate the growth of elongated grains. By adding seed crystals the fracture toughness of the sintered α-SiAlON ceramics was considerably improved, with no obvious degradation in the bulk density and hardness at the same time.     

Natural frequencies of functionally graded plates by a meshless method

We use the global collocation method, the first and the third-order shear deformation plate theories, the Mori–Tanaka technique to homogenize material properties, and approximate the trial solution with multiquadric radial basis functions to analyze free vibrations of functionally graded plates. Frequencies computed by the present method are found to agree well with those from the analytical solution of Vel and Batra, and the numerical solution of Qian et al. based on the meshless local Petrov–Galerkin formulation.     

电力系统电流互感器饱和特性的柔性神经网络补偿法

电流互感器(CT)由于饱和使得副边电流变形,进而导致保护与测量应用中的许多问题。为此,提出一种补偿CT饱和特性的方法,以改善其测量性能。所提算法基于具有2个可变参数的sigmoid函数,构建了新型柔性神经网络,以估算CT励磁电流。实时地将估算所得励磁电流与扭曲的副边测量电流相加,即得补偿后原边电流。在学习过程中,所建补偿器的各柔性神经元柔性地改变其形状以适应各自的角色,高度柔性特点增强了网络学习能力,不但可减少网络节点数,而且可减少迭代学习时间。仿真研究中,应用一个900:5A的CT测试所提出的补偿器,测试时考虑了CT原边电流不同直流分量、CT剩磁大小与CT负载特性的影响。仿真结果验证了所提补偿方法的高精度,而且不受CT负载特性、CT剩磁情况及原边电流直流成分的影响。     

Nanostructured Ni-Co alloys with tailorable grain size and twin density

We present an experimental approach to systematically produce nanostructures with various grain sizes and twin densities in the Ni-Co binary system. Using electrodeposition with various applied current densities and organic additive contents in the deposition bath, we synthesize nanostructured fcc and hcp solid solutions with a range of compositions. Due to the low stacking fault energy (SFE) of these alloys, growth twins are readily formed during deposition, and by adjusting the deposition conditions, a range of twin boundary densities is possible. The resulting nanostructured alloys cannot be described by a single characteristic length scale, but instead must be characterized in terms of (1) a true grain size pertaining to general high-angle grain boundaries and (2) an effective grain size that incorporates twin boundaries. Analysis of Hall-Petch strength scaling for these materials is complicated by their dual length scales, but the hardness trends found in Ni-80Co are found to be roughly in line with those seen in pure nanocrystalline nickel.     

A high-density heat-sink-mounted inductor for automotive applications

Passive components, and inductors, in particular, contribute greatly to the overall volume of power electronic converters. These components are normally packaged individually with little concern for the overall system. For high-density switching power supplies it is imperative to minimize the volume to as great an extent as possible which implies that the passive component volume usage needs to be improved. This can be accomplished by applying suitable packaging and cooling techniques to these components. In this paper, two inductor structures finding application in a 2.1-kW synchronous automotive converter are described. The air-gap placement, losses, cooling methods, and thermal profiles are analyzed and verified experimentally with an inductor designed for operation at 85/spl deg/C ambient.     

Cryo-X-ray analysis-A novel tool to better understand the physicochemical reactions at the bioglass/biological fluid interface

The present study deals with the short-term physicochemical reactions at the interface between bioactive glass particles [55SiO(2)-20CaO-9P(2)O(5)-12Na(2)O-4MgO. mol%] and biological fluid (Dulbecco Modified Eagle's Medium (DMEM)). The physicochemical reactions within the interface are characterized by scanning transmission electron microscopy (TEM) (STEM) associated with Energy-dispersive X-ray spectroscopy (EDXS). Microanalysis of diffusible ions such as sodium, potassium, or oxygen requires a special care. In the present investigation the cryo-technique was adopted as a suitable tool for the specimen preparation and characterization. Cryosectioning is essential for preserving the native distribution of ions so that meaningful information about the local concentrations can be obtained by elemental microanalysis. The bioglass particles immersed in biological fluid for 24 h revealed five reaction stages: (i) dealkalization of the surface by cationic exchange (Na(+), Ca(2+) with H(+) or H(3)O(+)); (ii) loss of soluble silica in the form of Si(OH)(4) to the solution resulting from the breakdown of Si--O--Si bonds (iii); repolymerization of Si(OH)(4) leading to condensation of SiO(2)); (iv) migration of Ca(2+) and PO(4) (3-) to the surface through the SiO(2)-rich layer to form CaO-P(2)O(5) film; (v) crystallization of the amorphous CaO-P(2)O(5) by incorporating OH-- or CO(3) (2-) anions with the formation of three different surface layers on the bioactive glass periphery. The thickness of each layer is approximately 300 nm and from the inner part to the periphery they consist of Si--OH, which permits the diffusion of Ca(2+) and PO(4) (3-) ions and the formation of the middle Ca--P layer, and finally the outer layer composed of Na--O, which acts as an ion exchange layer between Na(+) ions and H(+) or H(3)O(+) from the solution.     

A new laser Doppler flowmeter prototype for depth dependent monitoring of skin microcirculation

Laser Doppler flowmetry (LDF) is now commonly used in clinical research to monitor microvascular blood flow. However, the dependence of the LDF signal on the microvascular architecture is still unknown. That is why we propose a new laser Doppler flowmeter for depth dependent monitoring of skin microvascular perfusion. This new laser Doppler flowmeter combines for the first time, in a device, several wavelengths and different spaced detection optical fibres. The calibration of the new apparatus is herein presented together with in vivo validation. Two in vivo validation tests are performed. In the first test, signals collected in the ventral side of the forearm are analyzed; in the second test, signals collected in the ventral side of the forearm are compared with signals collected in the hand palm. There are good indicators that show that different wavelengths and fibre distances probe different skin perfusion layers. However, multiple scattering may affect the results, namely the ones obtained with the larger fibre distance. To clearly understand the wavelength effect in LDF measurements, other tests have to be performed.     

Effects of ozonized water and heat treatment on the papaya fruit epidermis

This study examined the effects of O₃ and hot water treatments on the epidermis of Golden papaya fruit. Heat treatments were applied in a hot water brushing (HWB) system. Papayas were brushed under a pressurized hot water rinse stage at 45, 55 and 65 °C for 60 s. In the HWB treatment, 4 ppm ozone was applied to the papayas for 1 or 2 min. The results show that ozone applications did not affect the fruit's cuticular surface, while heat treatments allowed natural fissures on the fruit epidermis to recover. Several crystalloid forms were identified on the epidermis of the papayas after the heat treatments. The predominant crystalloid forms on papayas are tubular and there is a positive response to temperature; the higher the temperature, the larger and more frequent the tubular crystalloids.     

Salmonella in eggs: From shopping to consumption—A review providing an evidence-based analysis of risk factors

Nontyphoidal salmonellae are among the most prevalent foodborne pathogens causing gastrointestinal infections worldwide. A high number of cases and outbreaks of salmonellosis are associated with the consumption of eggs and egg products, and several of these occur at the household level. The aim of the current study is to critically evaluate the current status of knowledge on Salmonella in eggs from a consumer's perspective, analyzing the hazard occurrence and the good practices that should be applied to reduce salmonellosis risk. Following a HACCP (Hazard Analysis and Critical Control Point) based approach, some steps along the food journey were identified as Critical Consumer Handling (CCH)—steps in which consumers, through their behavior or choice, can significantly reduce the level of Salmonella in eggs and egg products. From shopping/collecting to consumption, each of these steps is discussed in this review to provide an evidence-based overview of risk factors of human salmonellosis related to egg consumption. The main message to consumers is to choose Salmonella-free eggs (those that some official entity or producer guarantees that does not contain Salmonella), when available, especially for dishes that are not fully heat treated. Second, as guaranteed Salmonella-free eggs are only available in a few countries, refrigerated storage from the point of collection and proper cooking will significantly reduce the risk of salmonellosis. This will require a revision of the actual recommendations/regulations, as not all ensure that eggs are maintained at temperatures that prevent growth of Salmonella from collection until the time of purchasing.     

The transaction costs theory in international business research: a bibliometric study over three decades

Transaction costs theory (TCT) has long been an important conceptual lens for examining International Business (IB) phenomena and perhaps especially relevant for the study of multinational corporations, entry mode choices and location selection. In this paper we examine the extent to which TCT been used and has impacted IB research. Methodologically, we conduct a bibliometric study of the articles published on nine top journals for publishing IB-related research. We use Jean-François Hennart’s research as the key marker for TCT in IB research given that Hennart’s work has been a hallmark in the discipline. On a sample of 377 articles published between 1982 and 2010, and using the works rather than the authors as the unit of analysis, we analyze citations, co-citations and a spatial visualization of the intellectual research themes delved into. Our analyses provide insights on the influence of Hennart but more broadly of TCT on IB research over the past three decades. We conclude that the TCT has a pervasive influence on a large array of IB research and that Hennart’s work is boundary-spanning, connecting several research themes.