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961.
Solidus temperatures of the B2 NiAl phase have been determined by high-temperature differential thermal analysis for binary
melt compositions NixAl100−x
(45<x<57) and for ternary alloys FeyNi50−yAl50 (0≤y≤50). It was shown that the melting temperature of the stoichiometric Ni50Al50 phase is 1681 °C, which is 43 K higher than some literature data. The solidus line at the Ni-rich side of the Ni-Al phase
diagram exhibits a steeper slope than that reported previously. Substituting Fe for Ni, the decrease of solidus temperature
along the isoplethal section with 50 at.% Al of the ternary Ni-Fe-Al phase diagram exhibits a steep initial slope of −13 K/at.%
Fe for small Fe-fractions, which changes into a nearly linear decrease with an average slope of −8.5 K/at.% Fe. 相似文献
962.
Poly(N-methylaniline) (PNMA) coatings have been electropolymerized on 304 stainless steel alloy by potentiodynamic, galvanostatic and potentiostatic synthesis techniques from aqueous solutions of 0.1 M N-methylaniline (NMA) and 0.3 M oxalic acid. Characterization of PNMA coatings was carried out by cyclic voltammetry, UV-Vis and FTIR spectroscopy techniques. Corrosion behavior of PNMA coated stainless steel electrodes was investigated using linear anodic potentiodynamic polarization, Tafel test, chronoamperometry and electrochemical impedance spectroscopy (EIS) techniques in 0.5 M aqueous HCl solutions. Corrosion test results showed that PNMA coatings possessed protection to uncoated stainless steel against corrosion. 相似文献
963.
Chang-Seog?Kang Si-Young?Chang Sung-Kil?HongEmail author 《Metals and Materials International》2003,9(5):439-445
An attempt has been made to measure the temperature dependence of dynamic Young’s modulus together with the related variation
of internal friction in polycrystalline copper. A mechanical spectroscopy study was employed using a standard servo hydraulic
fatigue testing machine equipped with a scanning laser extensometer. Dynamic Young’s modulus and internal friction were measured
over a temperature range of 298 to 873 K at very low frequencies of 0.1, 0.05, and 0.01 Hz. One internal friction peak was
observed over the ranges 450 to 700 K, together with marked decreases in the dynamic Young’s modulus in the same temperature
range. From a quantitative analysis of the experimental data with the relaxation strength, relaxation time, and activation
energy, it is concluded that the peak phenomenon is due to grain-boundary sliding relaxation. 相似文献
964.
Joo-Youl?HuhEmail author Sang-Uk?Han Chang-Yong?Park 《Metals and Materials International》2004,10(2):123-131
The effect on the growth kinetics of the intermetallic compounds (IMCs) in solder/Cu joints, caused by adding Bi to eutectic
Sn-3.5Ag solder alloy, was examined at the aging temperatures of 150°C and 180°C. The Cu6Sn5 layer growth was significantly enhanced, but the Cu3Sn layer growth was slightly retarded by the addition of Bi, resulting in significant growth enhancement of the total (Cu6Sn5+Cu3Sn) IMC layer with increasing Bi addition. The IMC layer growth in the Bi-containing solder joints was accompanied by the
accumulation of Bi ahead of the Cu6Sn5 layer that resulted in the formation of a liquid layer at the Cu6Sn5/solder interface. A kinetic model was developed for the planar growth of the Cu6Sn5 and Cu3Sn layers in the solder joints, accounting for the existence of interfacial reaction barriers. Predictions from the kinetic
model showed that the experimental results could be well explained by the hypothesis that the formation of a Bi-rich liquid
layer at the Cu6Sn5/solder interface reduces the interfacial reaction barrier at the interface. 相似文献
965.
Young?Ah?JeonEmail author Kwang?Soo?No Jong?Sung?Kim Young?Soo?Yoon 《Metals and Materials International》2003,9(4):383-387
ZnO films for electronic applications were deposited by radio-frequency (rf) sputtering onto various metal bottom electrodes
(Pt/Ti, W, Ni) to investigate such structural properties as crystallinity and surface morphology. The crystallinity, surface
morphology and composition of the as-deposited films were studied using X-ray diffraction (XRD), scanning electron microscopy
(SEM) and Rutherford back-scattering spectrometry (RBS), respectively. The preferred orientation and surface morphologies
were strongly influenced by the type of bottom electrodes. The ZnO films with (200) texturing deposited on Pt/Ti/SiO2/Si showed a smoother and smaller grain size than those deposited on W and Ni. The ZnO films on Pt and W electrodes exhibited
compressive residual stress.
This article is based on a presentation made in the 2002 Korea-US symposium on the “Phase Transformations of Nano-Materials”,
organized as a special program of the 2002 Annual Meeting of the Korean Institute of Metals and Materials, held at Yonsei
University, Seoul, Korea on October 25–26, 2002. 相似文献
966.
Jae?H.?KimEmail author Jung?M.?Lee Ho?C.?Shin Young?H.?Paik 《Metals and Materials International》2003,9(6):593-597
It is known that oxide inclusions in liquid metal carry mostly positive charges on their surfaces. In an electrostatic field,
therefore, such charged particles suspended in a liquid metal experience forces and accumulate in the region of the negatively
charged surface, resulting in the separation of oxide inclusions from the liquid metal. In this study, this principle was
experimentally demonstrated for the case of a capacitor cell by the imposition of a d.c. potential on electrodes. The capacitor
cell consisted of a dielectric container of Pyrex tube, a high voltage d.c. source, and two electrodes, which were symmetrically
attached onto the outer surface of the Pyrex. tube. Experiments were carried out for suspensions of liquid tin/metal oxides,
such as SnO2, WO3, and PbO under an applied potential of up to 12 kV. All experimental results were in good agreement with the theoretical
prediction and showed that the degree of separation was significantly increased with the applied potential. 相似文献
967.
Hybrid Model of High Speed Machining Centre Headstock 总被引:1,自引:0,他引:1
A hybrid high-speed machining centre headstock model based on two computation methods: the finite element method and the finite difference method is presented. The model allows one to calculate precisely the headstock's indices on the basis of which its optimal operating characteristics can be determined. The presented modelling methods allow one to evaluate a design from thermal, stiffness and durability points of view. By way of illustration, the behaviour of three machining centre headstocks with: an electrospindle on rolling bearings, a conventional spindle and an electrospindle on aerostatic bearings are modelled using the hybrid model. 相似文献
968.
Cold-rolled and annealed ultra-high strength sheet steels with good ductility accompanied by TRIP of retained austenite have
received considerable attention in recent years. This paper discusses the effect of silicon content and annealing temperature
on the formation of retained austenite and the mechanical properties in Fe-0.34%C-1.7% Mn steels whose structure consists
of ferrite, bainite and retained austenite. Silicon inhibited the cementite formation in bainite during isothermal holding
and partitioned carbon from bainite to austenite, resulting in an increase in retained austenite content. When the silicon
content was increased to 1.0 wt.% or higher, the amount of retained austenite markedly increased leading to good mechanical
properties. 0.34%C-1.03%Si-1.7%Mn steel showed a high tensile strength of 1,030 MPa and a total elongation of 34.5% when annealed
at 780°C for 5 min followed by isothermal holding at 400°C for 5 min. In this case, the amount of retained austenite was about
25%. The variation in tensile strength-elongation combination had good correlation with that in the amount of retained austenite
with both annealing temperature and silicon content. The most retained austenite was obtained in the steel annealed at just
above AC1 temperature. The annealing temperature which gives the most retained austenite was decreased with decreasing the silicon
content. 相似文献
969.
970.
Setsuo?TakakiEmail author Toshihiro?Tsuchiyama Koichi?Nakashima Hideyuki?Hidaka Kenji?Kawasaki Yuichi?Futamura 《Metals and Materials International》2004,10(6):533-539
The microstructure development during plastic deformation was reviewed for iron and steel which were subjected to cold rolling
or mechanical milling (MM) treatment, and the change in strengthening mechanism caused by the severe plastic deformation (SPD)
was also discussed in terms of ultra grain refinement behavior. The microstructure of cold-rolled iron is characterized by
a typical dislocation cell structure, where the strength can be explained by dislocation strengthening. It was confirmed that
the increase in dislocation density by cold working is limited at 1016m−2, which means the maximum hardness obtained by dislocation strengthening is HV3.7 GPa. However, the iron is abnormally work-hardened
over the maximum dislocation strengthening by SPD of MM because of the ultra grain refinement caused by the SPD. In addition,
impurity of carbon plays an important role in such grain refinement: the carbon addition leads to the formation of nano-crystallized
structure in iron. 相似文献