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91.
为改善V2O5薄膜的电致变色性能,采用溶胶-凝胶法将具有高离子电导率并具有水溶性的聚环氧乙烷(PEO)直接嵌入V2O5层间,制备了PEO/V2O5纳米复合薄膜。采用标准三电极法从0.5mol/L LiClO4的PC电解质溶液向PEO/V2O5纳米复合薄膜注入锂离子,测量了纳米复合薄膜在注入不同数量锂离子时的可见光透射光谱以及对应的颜色变化,并运用循环伏安法测试其电化学性能。实验结果表明,PEO/V2O5纳米复合薄膜的循环伏安图出现了2对氧化还原峰,并且具有稳定的循环可逆性。随着应用电压的不同,薄膜呈现黄色、绿色和蓝色的多色可逆变化。PEO/V2O5纳米复合薄膜的电化学稳定性和机械性能都优于V2O5干凝胶薄膜,可以作为电致变色材料得到应用。X射线光电子能谱(XPS)成分分析表明PEO/V2O5纳米复合薄膜的电致变色效应与V、O的化合价和化学环境密切相关。 相似文献
92.
93.
Y. Y. Lee H. Y. Sun J. N. Reddy 《International journal for numerical methods in engineering》2006,65(1):45-61
A theoretical analysis is presented for the large amplitude vibration of symmetric and unsymmetric composite plates using the non‐linear finite element modal reduction method. The problem is first reduced to a set of Duffing‐type modal equations using the finite element modal reduction method. The main advantage of the proposed approach is that no updating of the non‐linear stiffness matrices is needed. Without loss of generality, accurate frequency ratios for the fundamental mode and the higher modes of a composite plate at various values of maximum deflection are then determined by using the Runge–Kutta numerical integration scheme. The procedure for obtaining proper initial conditions for the periodic plate motions is very time consuming. Thus, an alternative scheme (the harmonic balance method) is adopted and assessed, as it was employed to formulate the large amplitude free vibration of beams in a previous study, and the results agreed well with the elliptic solution. The numerical results that are obtained with the harmonic balance method agree reasonably well with those obtained with the Runge–Kutta method. The contribution of each linear mode to the maximum deflection of a plate can also be obtained. The frequency ratios for isotropic and composite plates at various maximum deflections are presented, and convergence of frequencies with the number of finite elements, number of linear modes, and number of harmonic terms is also studied. Copyright © 2005 John Wiley & Sons, Ltd. 相似文献
94.
Soil-cement blocks also known as compressed earth blocks or stabilised mud blocks are used for load bearing masonry. The paper focuses on the study of various characteristics of soil-cement blocks using highly sandy soils through an experimental investigation. Characteristics of soilcement blocks having three different cement contents (6%, 8% and 12%) have been examined. Paper reports results of influence of cement content on compressive strength, tensile strength, the initial rate of absorption (IRA), water absorption, rate of water absorption, surface porosity and pore size, stress-strain relationships and elastic properties of soil-cement blocks. The results indicate that there is 2.5 times increase in strength for doubling of cement content from 6%. IRA decreases drastically with the increase in cement content of the block. Saturated water content of the blocks is not sensitive to cement content, whereas rate of moisture absorption greatly depends on the cement content. Pore size decreases with increase in cement content of block, whereas surface porosity is independent of the cement content. Soil-cement block modulus varies between 2000 and 6000MPa. Elastic modulus increases by 2.5 times when the cement content is increased from 6 to 8%, whereas the increase in modulus is marginal when cement content goes from 8 to 12%. 相似文献
95.
This paper deals with the development of a neural computing system that can predict the cutting tool path length for milling an arbitrary pocket defined within the domain of a product design, in a computer numerically controlled (CNC) setting. Existing computer aided design and manufacturing systems (CAD/CAM) consume significant amounts of time in terms of data entry pertaining to the geometries and subsequent modifications to them. In the concurrent engineering environment, where even the designer needs information from the CAD/CAM systems, such time-consuming processes can be expensive. To alleviate this problem, a neural network system can be used to estimate machining time by predicting cost-dependent variables such as tool path length for the pocket milling operation. Pockets are characterized and classified into various groups. A randomized design is described so that the training samples that have been chosen represent the domain evenly. An appropriate network was built and trained with the sample pocket geometries. The analysis of the performance of the system in terms of tool path length prediction for new pocket geometries is presented. 相似文献
96.
Vijaya L. Manugula Koteswararao V. Rajulapati G. Madhusudhan Reddy R. Mythili K. Bhanu Sankara Rao 《Metallurgical and Materials Transactions A》2017,48(8):3702-3720
The effects of tool rotational speed (200 and 700 rpm) on evolving microstructure during friction stir welding (FSW) of a reduced activation ferritic-martensitic steel (RAFMS) in the stir zone (SZ), thermo-mechanically affected zone (TMAZ), and heat-affected zone (HAZ) have been explored in detail. The influence of post-weld direct tempering (PWDT: 1033 K (760 °C)/ 90 minutes + air cooling) and post-weld normalizing and tempering (PWNT: 1253 K (980 °C)/30 minutes + air cooling + tempering 1033 K (760 °C)/90 minutes + air cooling) treatments on microstructure and mechanical properties has also been assessed. The base metal (BM) microstructure was tempered martensite comprising Cr-rich M23C6 on prior austenite grain and lath boundaries with intra-lath precipitation of V- and Ta-rich MC precipitates. The tool rotational speed exerted profound influence on evolving microstructure in SZ, TMAZ, and HAZ in the as-welded and post-weld heat-treated states. Very high proportion of prior austenitic grains and martensite lath boundaries in SZ and TMAZ in the as-welded state showed lack of strengthening precipitates, though very high hardness was recorded in SZ irrespective of the tool speed. Very fine-needle-like Fe3C precipitates were found at both the rotational speeds in SZ. The Fe3C was dissolved and fresh precipitation of strengthening precipitates occurred on both prior austenite grain and sub-grain boundaries in SZ during PWNT and PWDT. The post-weld direct tempering caused coarsening and coalescence of strengthening precipitates, in both matrix and grain boundary regions of TMAZ and HAZ, which led to inhomogeneous distribution of hardness across the weld joint. The PWNT heat treatment has shown fresh precipitation of M23C6 on lath and grain boundaries and very fine V-rich MC precipitates in the intragranular regions, which is very much similar to that prevailed in BM prior to FSW. Both the PWDT and PWNT treatments caused considerable reduction in the hardness of SZ. In the as-welded state, the 200 rpm joints have shown room temperature impact toughness close to that of BM, whereas 700 rpm joints exhibited very poor impact toughness. The best combination of microstructure and mechanical properties could be obtained by employing low rotational speed of 200 rpm followed by PWNT cycle. The type and size of various precipitates, grain size, and evolving dislocation substructure have been presented and comprehensively discussed. 相似文献
97.
Previous studies have indicated that milrinone, a specific type III phosphodiesterase inhibitor, may be able to induce chloride secretion in cystic fibrosis (CF) tissues. We have now assessed the effect of this agent in vivo on the nasal epithelium of CF mutant mice and also in the nose and lungs of human subjects with CF. Wild-type mice showed a small hyperpolarization of the nasal potential difference (PD) in response to milrinone (100 microM, 1.6 +/- 0.6 mV, n = 8, P < 0.05). In contrast, CF mice carrying either the most common human mutation of the gene for the CF transmembrane regulator (CFTR), DeltaF508 (protein mislocalized), or the G551D mutation (protein normally localized) failed to demonstrate this response. Milrinone perfused alone had no significant effect on the baseline nasal PD of human subjects without CF (14.7 +/- 4.0 mV preperfusion; 15.3 +/- 4.6 mV postperfusion), but significantly (P < 0.05) augmented the hyperpolarization induced by a subsequently perfused low-chloride solution (with milrinone, 36.8 +/- 3.0 mV, n = 6; without milrinone, 18.1 +/- 2.2 mV, n = 19). In contrast, in human subjects with CF (n = 6), milrinone alone significantly (P < 0. 05) altered the nasal baseline PD (52.2 +/- 3.3 mV preperfusion; 57. 4 +/- 4.2 mV, postperfusion) but not the subsequent responses to the low-chloride solution (with milrinone, 1.1 +/- 2.2 mV, n = 4; without milrinone, 0.6 +/- 0.5 mV, n = 28) or to isoproterenol (100 microM). In a separate study in subjects (n = 6) with the DeltaF508 mutation, nasal coadministration of milrinone with isoproterenol produced no effect in the presence of amiloride and a low-chloride solution (-0.8 +/- 0.5 mV). This was also the case in the nasal epithelium of CF subjects (n = 4) carrying at least one G551D allele (-0.3 +/- 0.8 mV). Similarly, milrinone did not hyperpolarize the PD of either the tracheal (n = 6) or segmental (n = 6) airways of CF subjects (DeltaF508) when applied topically in vivo in the presence of amiloride, isoproterenol, or adenosine triphosphate (all 100 microM) in a low-chloride solution. These data do not support the use of milrinone to induce chloride secretion in CF airways in vivo. 相似文献
98.
Sampath Kumar Puttapati Venkataramana Gedela Vadali V S S Srikanth M V Reddy Stefan Adams B V R Chowdari 《Bulletin of Materials Science》2018,41(2):53
Unique reduced graphene oxide named solar reduced graphene oxide (SRGO) was found to be an excellent anode material in Li ion battery. SRGO exhibited first cycle discharge- and charge-capacities as high as 1480 and 880 mAh \(\hbox {g}^{-1}\), respectively. Moreover, the columbic efficiency was found to be >95% and the specific capacity retention even after 60 cycles was >500 mAh \(\hbox {g}^{-1}\). 相似文献
99.
Alzheimer’s disease (AD) is one of the most common forms of neurodegeneration, defined by reduced cognitive function, which is caused by the gradual death of neurons in the brain. Recent studies have shown an age-dependent rise in the levels of voltage-dependent anion channel 1 (VDAC1) in AD. In addition, we discovered an aberrant interaction between VDAC1 and P-TAU in the brains of AD patients, which led to abnormalities in the structural and functional integrity of the mitochondria. The purpose of our study is to understand the protective effects of reduced VDAC1 against impaired mitochondrial dynamics and defective mitochondrial biogenesis in transgenic TAU mice. Recently, we crossed heterozygote VDAC1 knockout (VDAC1+/−) mice with transgenic TAU mice to obtain double-mutant VDAC1+/−/TAU mice. Our goal was to evaluate whether a partial decrease in VDAC1 lessens the amount of mitochondrial toxicity in transgenic Tau (P301L) mice. We found that mitochondrial fission proteins were significantly reduced, and mitochondrial fusion and biogenesis proteins were increased in double-mutant mice compared to TAU mice. On the basis of these discoveries, the current work may have significance for the development of reduced-VDAC1-based treatments for individuals suffering from AD as well as other tauopathies. 相似文献
100.
M. Reddy D. D. Lofgreen K. A. Jones J. M. Peterson W. A. Radford J. D. Benson S. M. Johnson 《Journal of Electronic Materials》2013,42(11):3114-3118
HgCdTe dual-band mid-wave infrared/long-wave infrared focal-plane arrays on CdZnTe are a key component in advanced electrooptic sensor applications. Molecular beam epitaxy (MBE) has been used successfully for growth of dual-band layers on larger CdZnTe substrates. However, the macrodefect density, which is known to reduce the pixel operability and its run-to-run variation, is larger when compared with layers grown on Si substrate. This paper reports the macrodefect density versus size signature of a well-optimized MBE dual-band growth and a cross-sectional study of a macrodefect that represents the most prevalent class using focused ion beam, scanning transmission electron microscopy, and energy-dispersive x-ray spectroscopy. The results show that the macrodefect originates from a void, which in turn is associated with a pit on the CdZnTe substrate. 相似文献