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71.
Renata Lubczak 《Polymer International》2013,62(8):1243-1249
3‐(9‐Carbazolyl)propane‐1,2‐diol was obtained in the reaction of 9‐(2,3‐epoxypropyl)carbazole with water. The obtained diol was further used for modification of unsaturated polyester resin to produce enhanced thermal and heat resistance in comparison with classic resins. The properties of polyesters and polyester resins modified with 3‐(9‐carbazolyl)propane‐1,2‐diol were studied in detail. When 3‐(9‐carbazolyl)propane‐1,2‐diol is used instead of propylene glycol the unsaturated polyester resins possess enhanced thermal stability.© 2013 Society of Chemical Industry 相似文献
72.
The objective of this work was to evaluate the influence of oil concentration and homogenization pressure on the emulsion and particle properties during the microencapsulation of basil essential oil by spray drying, using gum arabic as the wall material. Experiments were planned according a 22 rotational central composite design. The independent variables were oil concentration with respect to total solids (10–25%) and homogenization pressure (0–100 MPa). Emulsions were analyzed for droplet mean diameter, stability, and viscosity, and particles were analyzed for oil retention, moisture content, particle size, and morphology. Emulsion viscosity was not affected by any of the independent variables. The increase in the homogenization pressure from 0 to 100 MPa resulted in smaller emulsion droplet size (down to 0.40 µm) and, consequently, higher oil retention (up to 95%). On the other hand, higher oil loads (25%) resulted in poorer oil retention (51.22%). Microencapsulation of basil essential oil using gum arabic as the wall material proved to be a suitable process to obtain powdered basil essential oil, presenting great oil retention with the use of lower oil concentration and higher homogenization pressure. 相似文献
73.
Renata C.K. Kaminski Sandra H. Pulcinelli Celso V. Santilli Florian Meneau Stéphanie Blanchandin Valérie Briois 《Journal of the European Ceramic Society》2010,30(2):193-198
In this paper an unprecedent thermo-reversible sol–gel transition for titania nanoparticles dispersed in a solution of p-toluene sulfonic acid (PTSH) in isopropanol is reported. The sol formed by the thermo-hydrolysis at 60 °C of titanium tetraisopropoxide (Ti(OiPr)4) reversibly changes into a turbid gel upon cooling to room temperature. Turbidimetric measurements performed for samples containing different nominal acidity ratios (A = [PTSH]/[Ti]) have evidenced that the gel transformation temperature increases from 20 to 35 °C as the [PTSH]/[Ti] ratio increases from 0.2 to 2.0. SAXS results indicate that the thermo-reversible gelation is associated to a reversible aggregation of a monodisperse set of titania nanoparticles with average gyration radius of ≈2 nm. From the different PTSH species evidenced by Raman spectroscopy and TG/DTA of dried gels we proposed that the thermo-reversible gelation in this systems is induced by the formation of a supramolecular network, in which the protonated surface of nanoparticles is interconnected through cooperative hydrogen bonds between –SO3 groups of p-toluene sulfonic acid. 相似文献
74.
Renata Reisfeld Tsiala Saraidarov Gerard Panzer Viktoria Levchenko Michael Gaft 《Optical Materials》2011,34(2):351-354
In our search for efficient Luminescent Solar Concentrators (LSC) we have prepared polyvinyl pyrrolidone (PVP) films incorporated by ethylenediamine tetraacetic acid (EDTA) complex of europium and co-doped with silver nanoparticles (NPs). Steady state fluorescence was studied under weak and strong excitation. Dynamical study was performed by second harmonic of Nd laser. Under weak excitation the fluorescence of europium co-doped with silver plasmons increased by a factor of three and excited by continuous laser by a factor of 50. The lifetimes of films doped by the complex were 755 μs and co-doped with silver nanoparticles 946 μs. This is the first finding that the photon density accumulates the number of plasmons interacting with electronic states of europium increasing its transition probability resulting in the strong intensification of fluorescence. In dynamical measurements of lifetimes a single pulse does not provide enough energy to create such number of plasmons. 相似文献
75.
Federica Benvenuti Carlo Carlini Mario Marchionna Renata Patrini Anna Maria Raspolli Galletti Glauco Sbrana 《Journal of Inorganic and Organometallic Polymers》1997,7(3):183-201
The synthesis and structural characterization of a novel bidentate ligand such as bis(diphenylphosphino) methane bound to a cross-linked styrene/divinylbenzene resin and to linear poly(styrene) are reported. Moreover, the anchoring of palladium acetate to the above polymeric ligands is described and the structure of the heterogenized palladium(II) complexes obtained is proposed. 相似文献
76.
Renata Braga Araújo Guilherme Henrique Trielli Ferreira Gustavo Henrique Orair Wagner Meira Jr. Renato Antônio Celso Ferreira Dorgival Olavo Guedes Neto Mohammed Javeed Zaki 《International journal of parallel programming》2008,36(2):226-249
Analyzing gene expression patterns is becoming a highly relevant task in the Bioinformatics area. This analysis makes it possible
to determine the behavior patterns of genes under various conditions, a fundamental information for treating diseases, among
other applications. A recent advance in this area is the Tricluster algorithm, which is the first algorithm capable of determining
3D clusters (genes × samples × timestamps), that is, groups of genes that behave similarly across samples and timestamps.
However, even though biological experiments collect an increasing amount of data to be analyzed and correlated, the triclustering
problem remains a bottleneck due to its NP-Completeness, so its parallelization seems to be an essential step towards obtaining
feasible solutions. In this work we propose and evaluate the implementation of a parallel version of the Tricluster algorithm
using the filter-labeled-stream paradigm supported by the Anthill parallel programming environment. The results show that
our parallelization scales well with the data size, being able to handle severe load imbalances that are inherent to the problem.
Further more, the parallelization strategy is applicable to any depth-first searches. 相似文献
77.
Lodi A. Cappelli A. Bocchi M. Mucci C. Innocenti M. De Bartolomeis C. Ciccarelli L. Giansante R. Deledda A. Campi F. Toma M. Guerrieri R. 《Solid-State Circuits, IEEE Journal of》2006,41(1):85-96
In the nanometer era, the increase in nonrecurring engineering costs is a challenge for SoCs that can be faced through a standardization process. Hardware specialization of a standard platform to a given application can be achieved by exploiting reconfigurable technology. This paper presents a XiSystem SoC, which integrates two different field-programmable devices to provide application-specific computing blocks and IOs. A XiRisc reconfigurable processor is exploited to achieve more than one order of magnitude speed-up and energy consumption reduction vis-a/spl grave/-vis a DSP-like processor, while an eFPGA is integrated in the system in order to make it flexible enough to support various IO ports and protocols. The reconfigurable IO device is also utilized for pre/post data processing and implementation of some standard computational blocks. 相似文献
78.
Mrcia A. F. S. Neves Fernanda M. B. Coutinho Marcos L. Dias Renata A. Simo Carlos A. Achete 《应用聚合物科学杂志》2002,84(3):541-551
Macroporous poly(styrene‐co‐divinylbenzene) and poly(divinylbenzene) beads were synthesized by modified suspension polymerization in the presence of different mixtures of toluene and heptane as porogen agent. Through atomic force microscopy, it was possible to identify the microspheres and the channels between them that constitute the bead pores. It was also possible to make a comparison with the results obtained by nitrogen desorption, a traditional technique used to determine the porosity of macroporous copolymers in the dry state. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 84: 541–551, 2002; DOI 10.1002/app.10290 相似文献
79.
Renata Cardoso Magagnin Maria Solange Gurgel de Castro Fontes Rosio Fernandez Baca Salcedo 《土木工程与建筑:英文版》2014,(12):1567-1574
This paper presents an assessment of the spatial quality of a pedestrian street located in downtown Bauru, S~o Paulo State, Brazil, from the application of some urban sustainability indicators. Multi-method was used to evaluate the thermal comfort quality of users, urban accessibility and preservation of architectural heritage. The results show that the sustainability indicators, apart from being effective tools in identifying problems, can assist local managers in decision making, planning and monitoring of pedestrian public space. These indicators contribute to a broad diagnosis of the pedestrian street and also the formulation of programs, projects and municipal policies, aimed at providing a better life quality for pedestrians. 相似文献
80.
Nogueira IR Carneiro G Yoshida MI de Oliveira RB Ferreira LA 《Drug development and industrial pharmacy》2011,37(9):1083-1089
Topical chemotherapy with paromomycin (PA) has been used as an alternative for the treatment of cutaneous leishmaniasis; however, poor skin penetration of this drug limits the efficacy of formulations. The objective of this work was to study the ability of the PA free base to form ion pairing with organic acids, as well as evaluate the effect of these compounds on the topical delivery of PA. PA permeation across intact skin was low, while drug penetration into skin from PA ion pairing was the higher than that observed for the PA base. Data obtained on the stripped skin, a damaged skin model, clearly showed that the ion pairing presented a potential to improve PA skin permeation. 相似文献