Classification of acoustic emission signals collected during tensile tests on unidirectional ultra high molecular weight polypropylene fiber reinforced epoxy composites using principal component analysis

The objective of this study is to utilize a mathematical procedure for the evaluation of damage mechanism in ultra high molecular weight polypropylene/epoxy composite (UHMWPP/epoxy) specimen with different configuration based on the analysis of the AE signals of presented. Principal component analysis (PCA) is powerful tool, which utilized for the classification of the monitored AE transients. We worked on epoxy L160 resin, UHMWPP fiber bundle and UHMWPP/epoxy unidirectional specimens, subjected to tensile loading. Using model specimens exhibiting a predominant damage mechanism, correlations were established between the observed damage growth mechanisms and the AE parameter variances result in PCA. Outputs from this study revealed that the PCA is an effective tool for identifying damage modes such as matrix cracking, fibre/matrix debonding, fibre breakage and fibre pull-out in the UHMWPP/epoxy composites. The presence of damage modes in UHMWPP/epoxy composites was proven with scanning electron microscopy (SEM) images.     

9.7 GHz small-signal bandwidth of three-quantum well GaInNAs/GaAs laser diodes operating at 1.35 /spl mu/m

High frequency characterisation of three-quantum well GaInNAs/GaAs lasers operating at 1.35 /spl mu/m is reported. A relaxation frequency as high as 7.4 GHz and a 9.7 GHz small-signal bandwidth are demonstrated, indicating the potential for high bit rate (10 Gbit/s) direct modulation of these dilute nitrides on GaAs devices.     

Carbon-centered radicals in isolated soy proteins

ABSTRACT:  Solid-state electron paramagnetic resonance (EPR) spectroscopy of commercial samples of isolated soy proteins (ISP) revealed a symmetrical free-radical signal typical of carbon-centered radicals ( g = 2.005) ranging from 2.96 × 10¹⁴ to 6.42 × 10¹⁴ spins/g. The level of free radicals in ISP was 14 times greater than similar radicals in sodium caseinate, 29 times greater than egg albumin, and about 100 times greater levels than casein. Nine soy protein powdered drink mixes contained similar types of free radicals up to 4.10 × 10¹⁵ spins/g of drink mix, or up to 6.4 times greater than the highest free-radical content found in commercial ISP. ISP samples prepared in the laboratory contained trapped radicals similar to the levels in commercial ISP samples. When ISP was hydrated in 2.3 mM sodium erythorbate or 8.3 mM L-cysteine, frozen and dried, the level of trapped free radicals increased by about 17- and 19-fold, respectively. The ESR spectrum of defatted soybean flakes contained overlapping signals from the primary free-radical peak ( g = 2.005) and a sextet pattern typical of manganese-II. The manganese signal was reduced in the laboratory ISP and very weak in the commercial ISP.     

Novel composite nanofibers based on polyamide 66/graphene oxide- grafted aliphatic- aromatic polyamide: preparation and characterization

New polyamide 66/graphene oxide (GO)-grafted aliphatic-aromatic polyamide (polyamide-imide) (PAI) (PA66/GOF) composites nanofibers were successfully prepared via electrospinning method for the first time. An polyamide imide (PAI) was synthesized using polycondensation reaction from a dicarboxylic acid and a diamine based on 4,4′-(4,4′-isopropylidenediphenyl-1,1′-diyldioxy) dianiline, and characterized by ¹HNMR and FTIR. Morphological, structural, thermal and mechanical characteristics of the nanocomposite fibers were investigated by means of SEM, TEM, WAXD, DMTA and TGA techniques. Composites nanofibers of PA66/GO, PA66/PAI and PA66/GOF with smooth surface, uniform structure as well as with diameter ranging from 195 to 784 nm were obtained. The GO incorporation caused a reduction in the nanofibers diameters. The TEM images showed that the GO was well dispersed in the PA66 nanofibers without significant aggregation. An approximately 10 °C temperature increase in the glass transition temperature of PA66 was achieved by addition of 0.5 wt% of PAI, resulting from aliphatic-aromatic structure of PAI. By the TGA results, an increase about 40 °C was observed in the thermal stability of PA66/PAI composite nanofibers in comparison with that of pure PA66 nanofibers.     

Using the red-near infrared spectral to estimate ground cover based on vegetative indices

Rapid and accurate estimation of Ground Cover (GC) at regional and global scales for agricultural management application is only possible by using remote sensing (RS). In this study, two Vegetation Indices (VIs) including the Perpendicular Vegetation Index (PVI) and Normalized Difference Vegetation Index (NDVI) were used for estimating GC. Since the parameters of the bare soil line have an important role in calculating GC based on PVI, this line was extracted based on the red-NIRmin (minimum near infrared) method with different intervals (0.0001, 0.0005, and 0.0010). In addition to traditional statistics such as Root Mean Square Error (RMSE), the sensitivity analysis (S) was also used to sharpen the accuracy of the models' estimations. The results indicated that the PVI-based method, in contrast to the NDVI-based approach, had a better performance in estimating GC of wheat. The highest correlation between the observed GC and the estimated GC based on PVI method was achieved in interval length of 0.0005 (R2 = 0.91) with RMSE equal to 8.82. This regression line (GCEST = -3.47 + 0.96 GCOBS) was not significantly different from the 1:1 line. As expected, the best estimation was achieved when the sensitivity of estimated GC based on PVI (length of the interval: 0.0005) was almost constant and low compared to the other models.     

Thermally stable cellular poly(vinylidene) ferroelectrets: Optimization of CO2 driven inflation process

Electrically charged cellular ferroelectrets can show excellent thermally stable piezoelectric activity and are therefore progressively used in electrochemical transducers. Given that an optimized cellular structure is a key for improving charge density and the associated piezoelectric properties in this material, we investigated the influence of CO₂ inflation treatment using various gas diffusion expansion or inflation procedures on the piezoelectric d₃₃ coefficient and thermal stability of cellular poly(vinylidene) ferroelectrets and compare with the results (partially) obtained by N₂ inflation as reported in our previous study (Jahan, Mighri, Rodrigue, Ajji, J. Appl. Polym. Sci. 2019, 136, 47540). Samples were prepared using the conventional extrusion–stretching–inflation–corona charging method. Maximum d₃₃ coefficient for CO₂-inflated samples is found to be around 30% higher than that of N₂-inflated samples (327 pC/N compared to 251 pC/N) by stepwise pressure application method. The key parameters addressed in the inflation procedures are the changes in sample thickness, morphology, and the void-height distribution in both gas treatments. The ferroelectrets show excellent thermal stability for up to 4 days at 90, 110, and 120 °C in both treatments with a slightly improved performance in CO₂ gas. The higher activation energy of CO₂-inflated samples (0.52 eV) than the N₂-inflated ones (0.43 eV) further confirms the stability data. © 2019 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2019 , 136, 47929.     

Multipolar Graviton in the Hydrogen Atoms

We derive multipolar gravitational radiation in the framework of quantum field theory in which the atomic states are treated nonrelativistically, and the gravitational waves are quantized. By relaxing the constraint e^ik·x ≈ 1, the multipolar transition rate is calculated when one graviton is emitted. As a consistency check, we recover the semiclassical result in the dipole approximation regime. Besides, we show that the dynamical mechanism that gives rise to spontaneous graviton emission by an atom, has a profound consequence on the lifetime of the atomic electron.     

Swallow: Resource and Tag Recommender System Based on Heat Diffusion Algorithm in Social Annotation Systems

Social annotation systems (SAS) allow users to annotate different online resources with keywords (tags). These systems help users in finding, organizing, and retrieving online resources to significantly provide collaborative semantic data to be potentially applied by recommender systems. Previous studies on SAS had been worked on tag recommendation. Recently, SAS‐based resource recommendation has received more attention by scholars. In the most of such systems, with respect to annotated tags, searched resources are recommended to user, and their recent behavior and click‐through is not taken into account. In the current study, to be able to design and implement a more precise recommender system, because of previous users' tagging data and users' current click‐through, it was attempted to work on the both resource (such as web pages, research papers, etc.) and tag recommendation problem. Moreover, by applying heat diffusion algorithm during the recommendation process, more diverse options would present to the user. After extracting data, such as users, tags, resources, and relations between them, the recommender system so called “Swallow” creates a graph‐based pattern from system log files. Eventually, following the active user path and observing heat conduction on the created pattern, user further goals are anticipated and recommended to him. Test results on SAS data set demonstrate that the proposed algorithm has improved the accuracy of former recommendation algorithms.     

On the measurement of friction coefficient utilizing the ring compression test

The main objective of this research was to investigate whether generalized friction calibration curves, as recommended in the literature for use with ring compression tests, are applicable to all types of materials and test conditions. Specifically, the effects of material properties, strain-rate sensitivity, and “barreling” on the behavior of friction calibration curves were investigated. To this end, a series of ring compression tests were conducted in order to determine the magnitude of the friction coefficient, μ, as well as the corresponding calibration curves for two types of modeling materials, white and black Plasticine. The experiments were first conducted using the Physical Modeling Technique (PMT) and then simulated via an elastic–plastic finite element code (ABAQUS). In contrast to the results available in the literature, where the same friction calibration curves are recommended for all types of materials and test conditions, the results of this investigation showed that friction calibration curves are indeed affected by the material properties and test conditions and every material possesses its own distinctive friction calibration curve.