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Enzymatic Synthesis of l‐Ascorbyl Fatty Acid Esters Under Ultrasonic Irradiation and Comparison of Their Antioxidant Activity and Stability 下载免费PDF全文
A series of novel l ‐ascorbyl fatty acid esters were synthesized by catalization of Novozym® 435 under ultrasonic irradiation and characterized by infrared spectroscopy, electrospray ionization mass spectra, and nuclear magnetic resonance. Their properties especially antioxidant activity and stability were investigated. The results showed that the reducing power, the scavenging activity of hydroxyl radical and 2,2‐diphenyl‐1‐picrylhydrazyl radical were decreased with the increase of the number of carbon atoms in fatty acid. The hydroxyl radical scavenging activity and reducing power of l ‐ascorbyl saturated fatty acid esters were better than that of tert‐butylhydroquinone. The induction period in lipid oxidation of l ‐ascorbyl saturated fatty acid esters and tert‐butylhydroquinone were longer than that of l ‐ascorbyl unsaturated fatty acid esters and l ‐ascorbic acid both in soybean oil and lard. Besides, the l ‐ascorbyl fatty acid esters showed different stabilities in different conditions by comparing with l ‐ascorbic acid, and the l ‐ascorbyl saturated fatty acid esters were more stable than l ‐ascorbyl unsaturated fatty acid esters in ethanol solution. 相似文献
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Dominic Phelan Mark Reid Nicole Stanford Rian Dippenaar 《JOM Journal of the Minerals, Metals and Materials Society》2006,58(9):67-69
An in-situ laser-scanning confocal microscopy study has been undertaken on the phase transformations in highpurity titanium. Observations of the β-Ti to α-Ti were observed to proceed with a pronounced Widmanstätten plate morphology due to the large β-Ti grain size. An anomalous transformation was also observed, with the α-Ti growing with a defined ledge-like surface relief. The observed transformation morphologies are discussed with reference to the crystallography of the regions, analyzed using electron-backscatter diffraction. 相似文献
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Impact of coagulation and adsorption on DOC fractions of secondary effluent and resulting fouling behaviour in ultrafiltration 总被引:2,自引:0,他引:2
Membrane fouling by macromolecular dissolved organic compounds is still a fundamental drawback in low-pressure membrane filtration of secondary effluent. In this study, pre-treatment of secondary effluent by coagulation and/or adsorption was investigated in terms of removal of different dissolved organic carbon (DOC) fractions, especially macromolecular substances. DOC fractionation has been characterised by size exclusion chromatography. Adsorption tests using four commercially available activated carbons yielded a removal of small as well as larger organic compounds, revealing differences in the affinity towards macromolecules depending on the type of applied activated carbon. By contrast, coagulation removed predominantly larger molecules, i.e., biopolymers and humic substances. In terms of DOC reduction, the coagulant ferric chloride was superior to aluminium chloride. A combination of coagulation and adsorption resulted in the addition of individual removal efficiencies, suggesting that different fractions of organic compounds were involved in each of the processes. After removal of macromolecular organic compounds either by coagulation or by adsorption, a significant reduction of membrane fouling was observed in tests using two different types of ultrafiltration flat-sheet membranes in 20-h cross-flow filtration tests. 相似文献
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基于体素S因子计算个体化病例的三维剂量是目前核医学研究的一个重要方向.153Sm是目前骨转移治疗常用的核素之一.本文利用EGS4蒙特卡罗程序包构建了基于体素的三维吸收剂量分布模拟程序,计算了不同情况下153Sm的S因子,探讨了介质成分和物理密度对S因子的影响.结果表明:1)不同物理密度对S因子有明显影响;2)在相同物理密度的情况下,不同介质对S因子的影响相对较小.计算结果为基于体素S因子计算核素治疗的三维剂量提供了参考,明确了在不考虑介质和物理密度差异时S因子的误差. 相似文献
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Region-based fractal image compression 总被引:5,自引:0,他引:5
A fractal coder partitions an image into blocks that are coded via self-references to other parts of the image itself. We present a fractal coder that derives highly image-adaptive partitions and corresponding fractal codes in a time-efficient manner using a region-merging approach. The proposed merging strategy leads to improved rate-distortion performance compared to previously reported pure fractal coders, and it is faster than other state-of-the-art fractal coding methods. 相似文献
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Rian Van Staden 《Refocus》2001,2(8):45
The International Solar Energy Society has been experiencing an extraordinary period of change of late, in this article, Rian Van Staden, new Executive Director of ISES highlights current developments and initiatives at the organisation. 相似文献
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MA Dobbs M Lueker KA Aird AN Bender BA Benson LE Bleem JE Carlstrom CL Chang HM Cho J Clarke TM Crawford AT Crites DI Flanigan T de Haan EM George NW Halverson WL Holzapfel JD Hrubes BR Johnson J Joseph R Keisler J Kennedy Z Kermish TM Lanting AT Lee EM Leitch D Luong-Van JJ McMahon J Mehl SS Meyer TE Montroy S Padin T Plagge C Pryke PL Richards JE Ruhl KK Schaffer D Schwan E Shirokoff HG Spieler Z Staniszewski AA Stark K Vanderlinde JD Vieira C Vu B Westbrook R Williamson 《The Review of scientific instruments》2012,83(7):073113
A technological milestone for experiments employing transition edge sensor bolometers operating at sub-Kelvin temperature is the deployment of detector arrays with 100s-1000s of bolometers. One key technology for such arrays is readout multiplexing: the ability to read out many sensors simultaneously on the same set of wires. This paper describes a frequency-domain multiplexed readout system which has been developed for and deployed on the APEX-SZ and South Pole Telescope millimeter wavelength receivers. In this system, the detector array is divided into modules of seven detectors, and each bolometer within the module is biased with a unique ~MHz sinusoidal carrier such that the individual bolometer signals are well separated in frequency space. The currents from all bolometers in a module are summed together and pre-amplified with superconducting quantum interference devices operating at 4 K. Room temperature electronics demodulate the carriers to recover the bolometer signals, which are digitized separately and stored to disk. This readout system contributes little noise relative to the detectors themselves, is remarkably insensitive to unwanted microphonic excitations, and provides a technology pathway to multiplexing larger numbers of sensors. 相似文献