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101.
以丙烯酸(AA)、顺丁烯二酸酐(MA)、2-丙烯酰胺-2-甲基丙磺酸(AMPS)和苯乙烯(St)为单体,通过自由基聚合反应,制备得到了具有两亲结构的聚合物分散剂.将该聚合物分散剂应用于钛白粉在水中的分散,考察了其对钛白粉悬浮稳定性、Zeta电位和粘度性能等的影响.同时,还对该聚合物的结构进行了FT-IR、TGA和XRD分析.结果表明,此聚合物能显著地改善钛白粉在水中的分散情况. 相似文献
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103.
Polymer/carbon nanotube nanocomposites have attracted high interest for a wide spectrum of applications, including antistatic packaging used to protect electronic devices against electrostatic discharge. Polytrimethylene terephthalate (PTT)/maleic-anhydride-grafted PTT (PTT-g-MA)/acrylonitrile butadiene styrene (ABS) blend-based multiwall carbon nanotubes (MWCNTs) nanocomposites were prepared through extrusion. It was conducted chemical functionalization on the MWCNTs by oxidation using nitric acid to introduce functional groups. The effect of the amount (0.5 or 1.0 wt%) and functionalization of MWCNTs on the nanocomposites was investigated. Despite the poor barrier properties of PTT/PTT-g-MA/ABS/MWCNT nanocomposites due to the presence of voids confirmed by scanning electron microscopy (SEM), the nanocomposites with functionalized MWCNT (MWCNTf) showed excellent barrier properties, indicating that the functionalization process improved the interaction between the MWCNTs and the matrix. The addition of MWCNTs into PTT/PTT-g-MA/ABS blend decreased the electrical resistivity by eight orders of magnitude. The use of MWCNTf may still disrupt the electrical network pathway and slightly decreasing the electrical resistivity, but the nanocomposites present the desired properties required for antistatic packaging. 相似文献
104.
CHENG Bei YU Xiaoxiao YU Jiaguo ZHAO Xiujian 《稀有金属(英文版)》2006,25(4):382-388
BaCO3 whiskers exhibiting different morphologies were fabricated by a simple precipitation reaction of barium ch/oride with sodium carbonate in the absence and presence of poly-(styrene-alt-maleic acid) (PSMA) as a crystal growth modifier at room temperature. The as-prepared products were characterized by scanning electron microscopy (SEM), transmission electron microscopy (TEM), and X-ray diffraction (XRD). The influences of experimental parameters on the size and morphology of BaCO3 whiskers were investigated and discussed. It was found that the as-prepared BaCO3 whiskers are single crystals with diameter ranging from 100 to 300 run, and grow along the crystallographic a-axis or [100] direction. BaCO3 whiskers with different morphologies, such as branching and dendritic structure, can be obtained depending on the experimental conditions. With increasing PSMA concentration, the diameter of BaCO3 whiskers decreases. 相似文献
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106.
Leonardo Roberto da Silva Eduardo Carlos Bianchi Ronaldo Yoshinobu Fusse Rodrigo Eduardo Catai Thiago Valle Frana Paulo Roberto Aguiar 《International Journal of Machine Tools and Manufacture》2007,47(2):412-418
The quality of machined components is currently of high interest, for the market demands mechanical components of increasingly high performance, not only from the standpoint of functionality but also from that of safety. Components produced through operations involving the removal of material display surface irregularities resulting not only from the action of the tool itself, but also from other factors that contribute to their superficial texture. This texture can exert a decisive influence on the application and performance of the machined component. This article analyzes the behavior of the minimum quantity lubricant (MQL) technique and compares it with the conventional cooling method. To this end, an optimized fluid application method was devised using a specially designed nozzle, by the authors, through which a minimum amount of oil is sprayed in a compressed air flow, thus meeting environmental requirements. This paper, therefore, explores and discusses the concept of the MQL in the grinding process. The performance of the MQL technique in the grinding process was evaluated based on an analysis of the surface integrity (roughness, residual stress, microstructure and microhardness). The results presented here are expected to lead to technological and ecological gains in the grinding process using MQL. 相似文献
107.
108.
用倒极图法研究了含0.3%Ce对Fe-Cr合金在高温下氧化膜(Cr_2O_3)择优取向的作用。加Ce的主要取向为(10110)⊥、(1014)⊥,(1126)⊥;不加的主要取向为(1014)⊥,(1126)⊥,(0112)⊥。 实验证明,Ce富聚于氧化膜和基体(α-Fe)的界面,起着增强和保持氧化膜择优取向的作用,从而改善合金的抗氧化性能。 相似文献
109.
测定了Fe-15Cr-4Al合金在500℃的时效脆化动力学,利用内耗,TEM,EPMA和SEM等手段研究了合金在时效后的组织变化和断裂行为。结果表明,时效脆化第一阶段(0-100h)主要是碳化物在α相晶界析出的作用,它损害界面结合,降低断裂应力,使塑性在时效0.25h后消失;第二阶段(100-1000h)主要是富Cr-α'相均匀析出的作用,它通过强化基体引起二次脆化。含0.2和0.4%的Fe-15 相似文献
110.
We consider an initial-boundary-value problem for a time-fractional diffusion equation with initial condition u0(x) and homogeneous Dirichlet boundary conditions in a bounded interval [0, L]. We study a semidiscrete approximation scheme based on the pseudo-spectral method on Chebyshev–Gauss–Lobatto nodes. In order to preserve the high accuracy of the spectral approximation we use an approach based on the evaluation of the Mittag-Leffler function on matrix arguments for the integration along the time variable. Some examples are presented and numerical experiments illustrate the effectiveness of the proposed approach. 相似文献