全文获取类型
收费全文 | 815篇 |
免费 | 33篇 |
国内免费 | 3篇 |
专业分类
电工技术 | 7篇 |
化学工业 | 205篇 |
金属工艺 | 45篇 |
机械仪表 | 39篇 |
建筑科学 | 17篇 |
能源动力 | 42篇 |
轻工业 | 77篇 |
水利工程 | 10篇 |
石油天然气 | 4篇 |
无线电 | 52篇 |
一般工业技术 | 176篇 |
冶金工业 | 72篇 |
原子能技术 | 12篇 |
自动化技术 | 93篇 |
出版年
2023年 | 14篇 |
2022年 | 20篇 |
2021年 | 22篇 |
2020年 | 24篇 |
2019年 | 16篇 |
2018年 | 28篇 |
2017年 | 27篇 |
2016年 | 32篇 |
2015年 | 26篇 |
2014年 | 34篇 |
2013年 | 67篇 |
2012年 | 41篇 |
2011年 | 44篇 |
2010年 | 33篇 |
2009年 | 33篇 |
2008年 | 29篇 |
2007年 | 19篇 |
2006年 | 35篇 |
2005年 | 19篇 |
2004年 | 11篇 |
2003年 | 14篇 |
2002年 | 25篇 |
2001年 | 13篇 |
2000年 | 16篇 |
1999年 | 9篇 |
1998年 | 19篇 |
1997年 | 14篇 |
1996年 | 24篇 |
1995年 | 8篇 |
1994年 | 8篇 |
1993年 | 6篇 |
1992年 | 12篇 |
1991年 | 5篇 |
1990年 | 10篇 |
1989年 | 6篇 |
1988年 | 4篇 |
1987年 | 6篇 |
1986年 | 6篇 |
1984年 | 8篇 |
1983年 | 6篇 |
1981年 | 6篇 |
1980年 | 4篇 |
1979年 | 8篇 |
1978年 | 4篇 |
1977年 | 5篇 |
1976年 | 7篇 |
1975年 | 6篇 |
1974年 | 4篇 |
1973年 | 4篇 |
1972年 | 3篇 |
排序方式: 共有851条查询结果,搜索用时 0 毫秒
21.
Ghayth Rigane Mohamed Bouaziz Nidhal Baccar Samira Abidi Sami Sayadi Ridha Ben Salem 《Journal of food science》2012,77(10):C1077-C1083
Abstract: A very simple method is proposed to produce hydroxytyrosol, a commercially unavailable compound with well‐known biological properties which justify a potential commercial application. The 2‐phase Chemlali olive pomace is selected as substrate for chemical treatment. Different conditions of chemical treatment, including concentration of acid and alkaline solutions, time and temperature, were assayed. A high amount of hydroxytyrosol (1360 mg/kg of fresh 2‐phase olive pomace) was obtained using water bath after treatment at 80 °C for 90 min with 1 M of H3PO4. However, treatment of 2‐phase Chemlali olive pomace using autoclave apparatus could produce a large amount of hydroxytyrosol (1993.60 and 1515.88 mg/kg of fresh alperujo, 1 M acid and basic catalyst, respectively). By taking into consideration practical and economic aspects, acid‐catalyzed treatment was more effective using autoclave conditions, whereas the alkali catalyzed conditions were not very suitable. This study could provide useful information for industry to produce the potentially bioactive compound. Practical Application: The 2‐phase Chemlali olive pomace is selected as substrate for chemical treatment. Treatment of “alperujo” using water bath or autoclave apparatus was carried out. A high amount of hydroxytyrosol was obtained using autoclave apparatus. 相似文献
22.
Kilicaslan M. Fatih Altaib Salaheddin Salem Vurdu Can Doğan 《Metals and Materials International》2019,25(6):1457-1466
Metals and Materials International - In this project the morphology and microstructure of both conventional cast and melt spun of Al–20Si–9Fe–1.2Nb and... 相似文献
23.
24.
Geoffrey Lawrence Arun V Baskar Mohammed H El-Newehy Wang Soo Cha Salem S Al-Deyab Ajayan Vinu 《Science and Technology of Advanced Materials》2015,16(2)
Three-dimensional cage-like mesoporous FDU-12 materials with large tuneable pore sizes ranging from 9.9 to 15.6 nm were prepared by varying the synthesis temperature from 100 to 200 °C for the aging time of just 2 h using a tri-block copolymer F-127(EO106PO70EO106) as the surfactant and 1,3,5-trimethyl benzene as the swelling agent in an acidic condition. The mesoporous structure and textural features of FDU-12-HX (where H denotes the hydrothermal method and X denotes the synthesis temperature) samples were elucidated and probed using x-ray diffraction, N2 adsorption, 29Si magic angle spinning nuclear magnetic resonance, scanning electron microscopy and transmission electron microscopy. It has been demonstrated that the aging time can be significantly reduced from 72 to 2 h without affecting the structural order of the FDU-12 materials with a simple adjustment of the synthesis temperature from 100 to 200 °C. Among the materials prepared, the samples prepared at 200 °C had the highest pore volume and the largest pore diameter. Lysozyme adsorption experiments were conducted over FDU-12 samples prepared at different temperatures in order to understand their biomolecule adsorption capacity, where the FDU-12-HX samples displayed high adsorption performance of 29 μmol g−1 in spite of shortening the actual synthesis time from 72 to 2 h. Further, the influence of surface area, pore volume and pore diameter on the adsorption capacity of FDU-12-HX samples has been investigated and results are discussed in correlation with the textural parameters of the FDU-12-HX and other mesoporous adsorbents including SBA-15, MCM-41, KIT-5, KIT-6 and CMK-3. 相似文献
25.
A. F. Salem 《Journal of Superconductivity and Novel Magnetism》2014,27(12):2707-2711
We have used the AC susceptibility for MgAlB2 samples to investigate the grain boundary effects and the Al-doping effects on the critical current density. The Cole-Cole plots were used to obtain the grain boundary effects on the critical current density. We found that the grain boundaries are highly transparent to current flow and have virtually no effects on the critical current density in MgB2pure and Al-doped samples. Moreover, the lower critical field H c1 is found to be enhanced with Al doping. The highest H c1 value is achieved with the 4.5 % concentration of Al. 相似文献
26.
Freestanding fiber mats of zeolitic imidazolate framework 7 via one‐step,scalable electrospinning 下载免费PDF全文
Seongpil An Ji Sun Lee Bhavana N. Joshi Hong Seok Jo Kirill Titov Jong‐San Chang Chul‐Ho Jun Salem S. Al‐Deyab Young Kyu Hwang Jin‐Chong Tan Sam S. Yoon 《应用聚合物科学杂志》2016,133(32)
We demonstrated the fabrication of freestanding zeolitic imidazolate framework 7 (ZIF‐7) nanofiber (NF) mats by means of one‐step, scalable electrospinning. The formation of ZIF‐7 nanoparticles embedded in polymer fibers was unambiguously pinpointed via X‐ray diffraction, transmission electron microscopy, and adsorption studies. The NF mats exhibited excellent characteristics, with an average diameter of 245 nm, in the adsorption and desorption of carbon dioxide (CO2); this makes them attractive candidates for gas separation and other selective filtration applications. This excellent property of the ZIF‐7 mats was explained by the gate‐opening phenomenon of ZIF‐7, which yielded a stepwise increase in the overall CO2 uptake capacity. The mechanical strength of the NF mats was also obtained via large‐strain uniaxial tensile deformation, which enabled preliminary assessment of the mat's suitability for textiles and membranes in targeting separation and filtration applications with large‐area permeability. © 2016 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2016 , 133, 43788. 相似文献
27.
Musarat Amina Touseef Amna Mallick Shamshi Hassan Nawal Musayeib Al Musayeib Salem Slayyem Salem Al-Deyab Myung-Seob Khil 《Korean Journal of Chemical Engineering》2016,33(11):3169-3174
Pure water is the fundamental requisite for human life. The water has been recycled naturally but not in an adequate amount for consumption. Nanotechnology with extraordinary applications provides competent ways for the decontamination of contaminated water. In the present study MnWO4 nanoflowers endorsed with inherent antibacterial activity were successfully synthesized by facile hydrothermal approach. XRD, SEM, EDX spectroscopy and UVDRS were used to characterize the as-synthesized nanoflowers. Gram negative Escherichia coli ATCC 52922 bacterium was used as model organism to test antibacterial activity of as-synthesized MnWO4 nanoflowers. This study was conducted to optimize minimum concentration of MnWO4 nanoflowers and maximum contact time required to achieve complete inactivation of bacteria present in contaminated water. Minimum inhibitory concentration (MIC) of MnWO4 nanoflowers was found to be 10 μg/ml. The assessment and interpretation of bacterial viability was done using dual fluorescent staining. The synthesized 3D-nanoflowers were found as potent bactericides. Thus, MnWO4 nanoflowers emerged to be very good future material for disinfection of biological pollutants present in the contaminated water reservoirs and as an anti-biofouling agent. 相似文献
28.
Differential thermal analysis (DTA) and thermogravimetry (TG) methods have been developed to evaluate the thermal and thermooxidation stability of different lubricating oils. Measurements are carried out either by heating the oil sample at a constant rate (direct programme) or by keeping it at a fixed high temperature (isothermal programme). Oxygen at a constant flow rate is used for thermooxidation measurements. Tested samples included different viscosity grades: neutral base oils, unadditivated lubricating oil blends, and industrial oils. The mechanism of thermal decomposition for ZDDP and the estimation of its optimum concentration was also considered. 相似文献
29.
Christiane L. Ojaimi Julieta A. Ferreira Adilson L. Chinelatto Raphael E. P. Salem Adriana S. A. Chinelatto Eliria M. J. A. Pallone 《International Journal of Applied Ceramic Technology》2020,17(4):1619-1628
Composites of Al2O3/ZrO2 (containing 25, 50, and 75 vol% ZrO2) were prepared by mixing Al2O3 and ZrO2 suspensions. The microstructural control via two-step sintering (TSS) was the main objective of this work. For this purpose, different sintering curves were constructed, aiming to achieve the best temperature combination for the sintering steps that provides higher density and finer microstructure. The results were compared with single-step sintering (SSS). Furthermore, microhardness and fracture toughness were measured for the best TSS specimens under each composition. The results showed that the high densities were obtained, and the reduction of grain size was greater than 40% for two-step sintered specimens, compared to SSS ones. Consequently, microhardness values increased. However, fracture toughness values remained unchanged. 相似文献
30.
M. Shamshi Hassan Touseef Amna Faheem A. Sheikh Salem S. Al-Deyab Kyung Eun Choi I.H. Hwang Myung-Seob Khil 《Ceramics International》2013
The objective of this study was to develop a new class of bimetallic ZnO/Ag embedded polyurethane multi-functional nanocomposite by a straightforward approach. Bimetallic nanomaterials, composed of two unlike metal elements, are of greater interest than the monometallic materials because of their improved characteristics. In the present study the bimetallic composite was prepared using sol–gel via the facile electrospinning technique. The utilized sol–gel was composed of zinc oxide, silver and poly(urethane). The physicochemical properties of as-spun composite mats were determined by X-ray diffraction pattern, field emission scanning electron microscopy, energy dispersive X-ray spectroscopy and transmission electron microscopy. The antibacterial activity was tested using Escherichia coli as model organism. The antibacterial test showed that ZnO:Ag/polyurethane composite possesses superior antimicrobial activity than pristine PU and ZnO/PU hybrids. Furthermore, our results illustrate that the synergistic effect of ZnO and Ag resulted in the advanced antimicrobial action of bimetallic ZnO/Ag composite mat. The viability and proliferation properties of NIH 3T3 mouse fibroblast cells on the ZnO:Ag/polyurethane composite nanofibers were analyzed by in vitro cell compatibility test. Our results indicated the non-cytotoxic behavior of bimetallic ZnO:Ag/polyurethane nanofibers towards the fibroblast cell culture. In summary, novel ZnO:Ag/polyurethane composite nanofibers which possess large surface to volume ratio with excellent antimicrobial activity were fabricated. The unique combination of ZnO and Ag nanoparticles displayed potent bactericidal effect due to a synergism. Hence the electrospun bimetallic composite indicates the huge potential in water filtration, clinical and biomedical applications. 相似文献